等离子体熔融钛与羟基磷灰石混合粉颗粒的形态和相组成

利用等离子喷涂设备将Ti与羟基磷灰石（HA）的混合粉末喷射入水，采用扫描电子显微镜和X射线衍射仪研究了Ti HA入水颗粒的形态和相组成，结果表明，经等离子熔融喷射入水后，钛粒子的尺寸小于HA粒子，主要原因之一是HA内形成了空心结构，空心结构的形成是由于HA在熔融时生成气相P2O5和H2O，它们在颗粒内聚集形成气泡，入水Ti HA粒子主要是由晶相和非晶相HA，分角相磷酸三钙（TCP）和磷酸四钙（TTCP）以及Ti的化合物所组成，由于与Ti的混合，HA的分解加剧，而Ti与HA粒子的融合及元素的扩散在飞行过程中已经发生。     

Mechanical alloying of Mo—Si—Fe powders

Mechanical milling behavior of Mo-Si-Fe powders was investigated u sing XRD, SEM and TEM techniques. The mixtures of elemental molybdenum (>99%), s ilicon (>99%) and iron (>98%) powders with a stoichiometry of Mo5-xFe xSi3 (x=0.5, 1, 2) were milled in a planetary mill for up to 195 h. For all three powder mixt ures, high-energy milling of 60h led to formation of the Mo(Fe, Si) supers aturated solid solution (Moss); and to a remarkable expansion of the solub ility of Fe, Si in molybdenum. The transformation of Moss to an amorphous phase was identified after longer time milling. In the milling process, the grain size of Mo (Fe, Si) decreased gradually and the internal stress increased linearly. After 40 h milling, the grain size was reduced to about 11 nm. SEM analysis of milled powders showed that the particle size increased initially with milling time. After 195 h milling, particles exhibited a spherical morphology and the particle size were reduced to about 100 nm.     

30MnCrNiMoB低合金钢绝热剪切带的形成机制与微结构

研究了３０ＭｎＣｒＮｉＭｏＢ低合金钢在穿甲弹冲击下绝热剪切带（ＡＳＢ）的形成机制。指出在高速变形（冲击）条件下ＡＳＢ的形成是应变硬化、热软化和位错动态发时导致的应变软化等因素相互耦合产生的塑性失稳现象。进一步确认ＡＳＢ内具有周期性微观结构，并说明ＡＳＢ中周期性开裂与微结构的关系。     

Exploring thermal spray gray alumina coating pore network architecture by combining stereological protocols and impedance electrochemical spectroscopy

Complex multiscale pore network architecture characterized by multimodal pore size distribution and connectivity develops during the manufacture of ceramic thermal spray coatings from intra- and interlamellar cracks generated when each lamella spreads and solidifies to globular pores resulting from lamella stacking defects. This network significantly affects the coating properties and their in-service behaviors. De Hoff stereological analysis permits quantification of the three-dimensional (3D) distribution of spheroids (i.e., pores) from the determination of their two-dimensional (2D) distribution estimated by image analysis when analyzing the coating structure from a polished plane. Electrochemical impedance spectroscopy electrochemically examines a material surface by frequency variable current and potential and analyzes the complex impedance. When a coating covers the material surface, the electrolyte percolates through the more or less connected pore network to locally passivate the substrate. The resistive and capacitive characteristics of the equivalent electrical circuit will depend upon the connected pore network architecture. Both protocols were implemented to quantify thermal spray coating structures. Al₂O₃-13TiO₂ coatings were atmospherically plasma sprayed using several sets of power parameters, are current intensity, plasma gas total flow rate, and plasma gas composition in order to determine their effects on pore network architecture. Particle characteristics upon impact, especially their related dimensionless numbers, such as Reynolds, Weber, and Sommerfeld criteria, were also determined. Analyses permitted identification of (a) the major effects of power parameters upon pore architecture and (b) the related formation mechanisms. This article was originally published inBuilding on 100 Years of Success, Proceedings of the 2006 International Thermal Spray Conference (Seattle, WA), May 15–18, 2006, B.R. Marple, M.M. Hyland, Y.-Ch. Lau, R.S. Lima, and J. Voyer, Ed., ASM International, Materials Park, OH, 2006.     

电脉冲改善金属材料组织的应用现状

综合评述了电脉冲作用下金属凝固过程、非晶结构的纳米晶化以及金属快速再结晶等方面的研究进展,着重介绍了电脉冲在材料加工过程中的作用机理.     

不同参数脉冲电流对不锈钢Cr18Ni9Ti凝固组织的影响

采用储能电容为1200μF的脉冲电源，在不同的脉冲电压下，对奥氏体不锈钢1Crl8Ni9Ti进行脉冲电流处理。实验结果表明：脉冲电流能够细化奥氏体不锈钢的凝固组织，使奥氏体一次枝晶长度缩短，二次枝晶间距减小。在一定范围内，脉冲电压升高和脉冲重复率增大都有利于奥氏体不锈钢凝固组织的细化和改善。     

系统失效的分支-界限分析法及其在桁架可靠性分析中的应用

本文首先介绍了系统失效的分支-界限分析法，然后以空间桁架系统为例用分支-界限分析法进行了可靠性分析。系统失效的分支-界限分析法直观、明了，适合对实际工程中的复杂系统进行可靠性分析。     

复合材料微波快速抢修技术在某重型 战机抢修中的应用

我国空军多架现役重型战斗机的结构损伤（裂纹）经用复合材料微波快速抢修技术修复。本文以此为例，详细推介了这一我国独创的快速抢修技术。     

A porosity formation and flattening model of an impinging molten particle in thermal spray coatings

Thermal spray coatings have porosity; however, reasons for the production of porosity during the coating process are not known. This paper proposes a physical and mathematical model for the production of porosity by considering deformation of a molten particle during thermal spray coating processes. The theoretical model shows that the impinging velocity, the ambient gas pressure, the particle diameter, and the molten material viscosity contribute to producing porosity. This paper also proposes that there is a porosity distribution along the splat radius and that most of the porosity exists in the periphery of the splat. Also, a flattening model proposed in this work agrees well with the results of Engel (Ref 1).     

铸铁件电弧冷焊熔合区白口组织的控制

进行了冷焊条件下控制铸铁件焊补区白口组织的试验．结果表明，采用Ｓｉ－Ｃａ－Ａｌ－Ｂｉ系合金粉层对焊补熔合区进行集中强石墨化孕育处理及焊前在缺陷表面形成Ｎｉ基合金粉末喷涂层，均可消除熔合区白口