磁性Fe-Cr纤维的长期稳定性和热稳定性

以Cu-Fe-Cr原位复合丝材萃取得微米级、亚微米级的Fe-Cr纤维,并研究了变形量、长期储存条件和热处理对Fe-Cr纤维样品结构和磁性能的影响。采用X射线衍射(XRD)和扫描电镜(SEM)分析了样品的结构和形貌,采用振动样品磁强计(VSM)测试了样品的磁性,并利用热重差热分析(TGA-DTA)比较了不同变形量的Fe-Cr纤维在空气中的热稳定性。结果表明:随着变形量的增大和Fe-Cr纤维的细化,纤维的饱和磁矩基本恒定(约140 A.m2/kg),而剩磁和矫顽力则逐渐增加;Fe-Cr纤维在无水乙醇和空气中储存一年以上,磁性基本保持不变;Fe-Cr纤维在空气中经300℃以上加热1 h后,逐渐由铁磁性的-(αFe,Cr)(BCC结构)固溶体转变为顺磁性的(Fe,Cr)2O3(六角晶系),饱和磁化强度显著下降;且随着变形量的增大,较细Fe-Cr纤维的热稳定性较差。     

铝板热轧机的液压AGC控制

介绍了铝板热轧机液压AGC系统的控制原理,以及AGC的几种控制方式。     

累积叠轧焊法制备超细晶纯铝的研究

采用累积叠轧焊方法在室温下对1060纯铝进行剧烈塑性变形，并分析1060纯铝变形前后内部微观组织结构的演变和力学性能的变化。实验结果表明，随着累积叠轧道次的增加，层界面复合越来越紧密，5道次后出现母材基体的相互渗透；材料的抗拉强度和硬度得到大幅度提高，伸长率在1道次时急剧下降，然后基本保持不变；晶粒尺寸急剧细化，等效真应变为6．4的条件下得到了平均晶粒尺寸为400nm的超细晶组织。     

Mechanical strength of PET fibers treated in cold plasma and thermal exposed

As a followup to previous work, experiments with argon and oxygen Radio Frequency plasma treated polyethylene terepthalate (PET) exposed to 100 °C after cold plasma treatment were performed. Tensile tests results in monofilaments treated in oxygen and argon plasma for 5 s, 20 s, 30 s, and 100 s showed a decrease in the average tensile strength compared with the untreated fibers. It was also observed that the reduction in mechanical strength is more significant for argon plasma and very sensitive to the treatment time for oxygen plasma. Experimental data obtained from tensile tests in samples thermal exposed to 100 °C after plasma treatments indicate the same influence of treatment times on mechanical strength, as observed for cold plasma treated fibers. Furthermore, an increase in tensile strength when compared with the samples unexposed to 100 °C was observed. Scanning electron microscopy, used to analyze effects of cold plasma treatment on fibers surfaces, indicates differences in roughness profiles depending on the type of treatment. The distance of roughness interval, D_ri, was a parameter introduced to relate the fibers surface condition and average tensile strength. Statistical analysis of experimental data was performed to explain influences of treatment time, and environmental and temperature effects on mechanical properties.     

镁合金超塑性研究

镁合金在室温下的塑性比较差，但在高温时塑性会有很大程度的改善。AZ31、AZ61、AZ91等合金在较高的温度和较慢的拉伸速率下具有超塑性。最新研究表明镁合金能够在低温和高变形速率下实现超塑性，因而具有工业化应用的可能。综述了镁合金超塑性研究领域的主要成果，分析了该领域研究中尚存在的一些问题，就今后的研究课题及发展方向进行展望。     

模锻成形过程中金属变形流动的测试方法

利用此方法对叶轮锻件成形过程中两个典型截面上4条流线及其轴向应变进行了测量分析,并定量给出该复杂锻件成形过程中变形及应变分布规律。因而该方法是测试模锻成形过程中金属塑性变形流动较为有效的实验手段。     

三辊联合穿轧工艺及变形区刚塑性有限元分析

三辊联合穿轧机将穿孔和轧管工序集于一体，实现一道次可获得各种精度的钢管生产新工艺，本文介绍了这种工艺的方法，对变形区的刚塑性进行了有限元分析。     

Evolution of patinas on copper exposed in a suburban area

Copper plates were exposed under sheltered outdoor conditions for up to one year, starting in September 2001 in Musashino City, Tokyo, a suburban area. Following various periods of exposure, the patinas on the plates were characterized to investigate their evolution by using X-ray fluorescence analysis, X-ray diffraction, field emission scanning electron microscopy, and glow discharge optical emission spectroscopy. The difference in the roles of sulfur and chlorine in the early stages of copper patination were identified by analyzing the depth profiles of these two elements. Sulfur was found on top of the patina as cupric sulfates such as posnjakite (Cu₄SO₄(OH)₆ · H₂O) or brochantite (Cu₄SO₄(OH)₆). Brochantite appeared only after 12 months of exposure. In contrast, chlorine was found on the surface after only one month of exposure. It gradually penetrated the patina as the exposure period lengthened, forming copper chloride complexes. Chloride ions accumulated at the patina/copper interface, forming nantokite (CuCl), which promoted corrosion.     

光磁共振实验最佳扫场参数的确定和抽运信号图分析

用光磁共振实验测定铷原子的g因子和地磁场，并对实验得到的数据进行分析并确定测定g因子的最佳扫场幅度。从理论上对各种抽运信号图形的产生进行了分析。     

时效析出相在强变形过程中的室温回归现象

利用透射电镜和硬度测量实验手段，研究了多相Al-Zn-Mg-Cu合金在强烈塑性变形中的组织和性能变化，特别是析出相的改变。结果发现：强烈塑性变形加工可引起析出相变形、碎化，然后溶入基体形成过饱和固溶体。这种合金在重新时效处理时可再次沉淀析出。提出了析出相回溶现象的“畸变自由能”观点。认为因品格畸变导致析出相自由能显著升高，当高于基体相的自由能时，便会发生析出相室温溶解的自发过程，称此过程为应变回归以区别于由热处理时加热引起的回归。