锇(Ⅷ)-N-(8-喹啉基)-N’-苯甲酰基硫脲(QBTU)络合物吸附波的1.5次微分极谱研究

于0.025mol/LNaOH溶液中,Os(Ⅷ)-QBTU体系产生—明晰的极谱波,其1.5次微分峰电流与浓度在1.0×10~(-7)～4.0×10~(-5)mol/L范围内呈线性关系。研究了极谱电流的性质、反应机理及电极过程等后确认:络合物的组成为[OsO_4(OH)_2·QBTU]·Na_2并吸附于滴汞电极表面,配体QBTU在不离解出的情况下发生电还原,获得络合物吸附波,电极过程不可逆,[OsO_4(OH)_2·QBTU]~(2-)离子的条件稳定常数8.5×10~5。     

DCPTA合成新方法的研究

ＤＣＰＴＡ是近年来新发现的一种植物生长调节剂。对农作物具有明显的增产增质效果。文中就其新的合成方法进行了研究。     

ST-102C式NaI(Tl)晶体中KX射线逃逸率的计算

本文对ST-102C式NaI(Tl)晶体中碘原子K层X射线的五种主要成分K_(α1)、K_(α2)、K_(β1)、K_(β2)和 K_(β3)的逃逸率分别进行了计算,然后根据五种 X 射线的相对强度进一步计算了加权平均逃逸率。计算中所选用的初始入射 X 射线能量在33.5—1000keV 之间。     

Short fibre elastomer composites: effect of fibre length,orientation, loading and bonding agent

A series of short fibre reinforced styrene butadiene rubber (SBR) composites were prepared by incorporating sisal fibres of different lengths and different concentrations. The vulcanization behaviour and the properties of the vulcanizates were measured by the relevant ASTM procedures. The processing characteristics such as green strength and mill shrinkage were improved by the addition of fibres. The properties like tensile strength, tear strength, moduli at 10% and 20% elongations were found to be maximum for composites containing longitudinally oriented fibres of length 6 mm. Mixes containing 35 phr loading of fibres and bonding agent showed better mechanical performance than others. The failure behaviour of tensile and tear specimens have been analysed by scanning electron microscopy techniques. Paper presented at the poster session of MRSI AGM VI, Kharagpur, 1995     

^125I,^131I诱发小鼠精子畸形发生率比较

本文选用 ICR 雄性小鼠,经腹腔分别注射不同剂量的~(125)I 及~(131)I,观察并比较它们对小鼠精子畸形发生率的影响及染毒后睾丸中放射性活度的变化。实验结果表明:(1)~(125)I 染毒后4—5周,0、185、370和555 kBq 各组精子畸形发生率分别为9.00‰、9.57‰、11.6‰及13.9‰;~(131)I 染毒后4—5周,上述各组精子畸形发生率分别为8.50‰、12.5‰、14.7‰和15.5‰;在相同注入量下,~(125)I 与~(131)I 诱发小鼠精子畸形发生率的差异各组均不显著(X~2检验,p>0.05)。(2)~(125)I、~(131)I 染毒后2h 至7天内,两者在睾丸中的放射性活度及变化规律相似,即在染毒后2h 达最高值,每克睾丸中~(125)I 和~(131)I 的放射性活度分别占初始注入量(370 kBq)的0.72％和0.50％,然后迅速下降,至一周时,仅分别占初始注入量的0.035％和0.011％。     

Electrosynthesis and impedance studies on zinc selenide

Electrochemical impedance measurements have been used to characterize zinc selenide films prepared by electrochemical co-deposition at a platinum rotating disk electrode. Estimations of capacitance and polarization resistance of variously prepared electrodeposits have been carried out to determine charge carrier density and corrosion rates.     

MAXIMUM ENTROPY DECONVOLUTION OF XPS PEAK

Necessity of XPS spectrum,deconvolution,disadvantages of the traditional Fast Fourier Tranderm decon-volution method(FFT),princtple,method and advantage ofMaximum Entropy Deconvolution Method (MEM) are de-scribed.Criteria for determing the number of data points sam-pled in MEM are the main point disccussed in the paper,someXPS deconvolution applications of our MEM software showthat the MEM makes XPS deconvolution much easier than thetraditional FFT method.     

天然糖甙类化合物^13C—NMR位移范围规律的计算机解析方法

本文从糖甙类化合物的数据特点出发,用较严格的数学推导总结出原则上适用于任何类型的~(13)C-NMR 图谱化学位移范围规律计算机自动解析的方法,并从多方面说明了该方法的研究及实现对实际的~(13)C-NMR 图谱解析工作的意义和重要作用。     

Machine translation of non-literary texts: Some Canadian experiences

A survey was carried out of past and current Canadian experiences with machine-aided translation (MAT) systems of non-literary texts in one government institution and three industrial settings. Each organization requires a great deal of translation and had conducted several experiments in the use of MAT. The survey supports positive conclusions about the prospects for expanded use of computers in translation.The authors express their thanks to all those who helped in the preparation of this paper. We are particularly grateful to the staff of the translation departments of the organizations mentioned in the paper for their kind cooperation and their willingness to answer our questions: Chantal Delorme ofIBM Canada, Lorraine Desmarais and Mr. Plamondon of Bell Canada, Pierre Tellier of the Department of the Secretary of State, Maria Russo and Raymond Lapointe of the Xerox Corporation. Furthermore we thank Prof. Graeme Hirst for helpful discussion.     

基于TMS320C6x实现多载波QPSK信号全数字化整体解调

提出并证明了一种群路FDMA/QPSK(频分多址/正交相移键控)信号全数字化整体解调的新方法,该方法根据信道构成特点和信号调制方式,将直接分路法和常规多相FFT(快速傅里叶变换)分离法相结合,构成了一种简化的等效多相FFT分路方法,再将输出的数字信号送到数字式解调器,实现了多载波信号的全数字化整体解调,其特点是软件和硬件结构简单、系统计算量小,且易于DSP实时实现,现已用该算法进行了32路FDMA/QPSK信号整体解调的计算机仿真实验,结果表明该方法是可行的.