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931.
932.
Qinghua Duan Yong Zhang Jinqiang Jiang Kuilin Deng Taoyi Zhang Ping Xie Rongben Zhang Pengfei Fu 《Polymer International》2004,53(1):113-120
A fully ethoxy‐terminated ladder‐like polymethylsilsesquioxane oligomer (EtO‐Me‐T) has been synthesized and characterized for the first time using an effective transient catalyst (tetramethylammonium hydroxide, TMAH) via the dehydration alcoholysis reaction of hydroxy‐terminated ladder‐like polymethylsilsesquioxane (HO‐Me‐T) prepared by a modified stepwise coupling polymerization approach. Compared with the common acidic or basic catalysts, use of the transient catalyst TMAH can not only make the HO‐Me‐T molecules fully ethoxy‐terminated but also enables the catalyst to be readily and thoroughly removed after completion of the alcoholysis reaction. It is noteworthy that the common acidic or basic catalysts widely used in the dehydration alcoholysis reaction are clearly unsuitable for the preparation of EtO‐Me‐T oligomer because the latter would be hydrolyzed unavoidably back to the parent HO‐Me‐T during the washing process. In addition, preliminary exploration indicates that, when compared with the tetraethyl orthosilicate (Si(OEt)4) generally used as a crosslinking agent for the room‐temperature vulcanization of silicone rubber (RTV‐SR), the oligomer EtO‐Me‐T is a promising replacement which can greatly improve the mechanical properties of RTV‐SR Copyright © 2003 Society of Chemical Industry 相似文献
933.
In an attempt to extend past goal setting research, the present study examined the influence of goal-performance discrepancies (GPDs), causal attributions, and temporal factors on the process of dynamic self-regulation. Goal revision processes were examined longitudinally in a sample of 100 varsity-level college track and field athletes over the course of an 8-week competitive season. The results indicate that an individual's GPD significantly predicted the amount of goal revision engaged in by the athletes, such that participants were more likely to lower their competition (proximal) and season (distal) goals when they failed to reach these goals and their respective GPDs were large. However, as hypothesized, this relationship was moderated by stability attributions and the temporal location of the individual with respect to the time period allotted for goal attainment. Implications for future research in the area of goal setting and dynamic self-regulation are discussed. (PsycINFO Database Record (c) 2010 APA, all rights reserved) 相似文献
934.
935.
Practice variability has been shown to enhance transfer of training. The purpose of the present study was to examine the role of self-efficacy generality as a motivational mechanism in explaining the relationship between practice variability and transfer. Undergraduate students (N = 82) were randomly assigned to 1 of 2 training conditions (constant or variable) for a computer decision-making task. Measures of self-efficacy (intensity and generality) and transfer (near and far) were assessed. The results provided support for some of the hypothesized relationships. Specifically, practice variability led to increased self-efficacy generality. Both self-efficacy intensity and generality influenced far transfer performance, although only self-efficacy generality served as a mediator between practice variability and far transfer. (PsycINFO Database Record (c) 2010 APA, all rights reserved) 相似文献
936.
937.
余伟 《稀有金属材料与工程》2007,24(3):32-35
对自焙电极在大型钛渣电炉中的运用进行了讨论,介绍了电极糊的组成、自焙电极的焙烧、电极壳结构,以及自焙电极与石墨电极进行比较和自焙电极的硬断和软断及处理办法。 相似文献
938.
储层分析中的自组织映射分析是通过直接分析未知数据体来进行的,特别在勘探早期,可用于储层预测约束的井位很少,借助于原数据体中存在的聚类关系,可大大提高钻井的成功率。 相似文献
939.
940.
纳米TiO2薄膜制备技术研究进展 总被引:10,自引:0,他引:10
对纳米TiO2薄膜的各种制备技术,包括基于溶胶一凝胶的涂层技术、电沉积、化学气相沉积、物理气相沉积、自组装制膜等技术的研究进展进行了综述。并对纳米TiO2薄膜制备的研究方向提出建议。 相似文献