Development of High Thermal Conductivity Aluminum Nitride Ceramic

AIN ceramics with densities varying from 3.18 to 3.30 g/cm³ and room-temperature thermal conductivities varying from 88 to 193 W/m K were produced. Different sintering conditions, packing powders, AIN powder sources, carbon additive, and sintering times were evaluated, and the key processing parameters which cause the differences in density and thermal conductivity were identified. SEM, TEM, and EDS were used to characterize the correlation between thermal conductivity, microstructure, and processing parameters. The important parameters which control the thermal conductivity of AIN ceramics are discussed.     

环冷机卸矿槽料位自动控制技术的改进

针对烧结过程中环冷卸矿槽料位存在周期性变化的特点。提出了一种改进的控制思路和解决方案。该方案在太钢三烧450m^2烧结机上采用后，取得了较好的效果。     

多缝式烧嘴点火器在攀钢烧结生产中的应用

多缝式烧嘴点火器具有燃烧效率高，火焰长度易调，炉膛温度分布合理等优点，经工业试验证明，该点火器能满足攀钢烧结点火工艺要求，并有明显节能效果。     

Processing and properties of zirconia-toughened alumina ceramics

Al₂O₃:ZrO₂ ceramics have been prepared from physically mixed pure oxide powders. The results indicate that careful processing of the starting powders and a two-stage sintering process can avoid expensive processing methods like hot pressing/hot isostatic pressing used for achieving high densification. The mechanical properties were measured and the resultant microstructure studied to explain the toughening behaviour of this material.     

优化锰铁高炉配矿结构

介绍了通过优化高炉锰铁烧结矿原料结构，改善了烧结矿性能，使锰铁冶炼取得了增产、节焦、降成本的明显效果。     

添加CaF2-YF3的AlN陶瓷的热导率

用CaF2和YF3做添加剂，在1750℃制备了热导率高于170W/m.K的的AlN陶瓷，并用XRD和SEM研究了AlN陶瓷在烧结过程中的相组成，微结构以及晶格参数的变化，并讨论了其对热导率的影响，研究发现，当使用CaF2-YF3做添加剂时，微结构差异对AlN陶瓷热导率的影响很小，AlN陶瓷的热导率主要由AlN晶格氧缺陷浓度决定，由于CaF2-YF3能有效降低AlN颗粒表面的氧含量，从而有利于获得高的热导率。     

钨钼活化烧结机理

主要介绍了添加少量Ｎｉ－Ｃｏ时钨，钼的低温烧结特性，对比了纯钨，Ｗ－Ｃｏ，Ｗ－Ｎｉ，Ｗ－Ｎｉ－Ｃｏ，纯钼，Ｍｏ－Ｃｏ，Ｍｏ－Ｎｉ，Ｍｏ－Ｎｉ－Ｃｏ烧结体系，测算了这些体系的烧结活化能，研究了其低温烧结机理，发现Ｎｉ－Ｃｏ对钨，钼的烧结具有最好的活化效果，说明镍与钴的共同加入对钨，钼的烧结具有协同活化作用。     

Fabrication and properties of PLZT ceramics from spray-dried aqueous solution

PLZT ceramics with the composition of 9/62/38 (La/Zr/Ti) were fabricated from spraydried aqueous solution. Complete crystallization of the spray-dried powder is achieved after 1 hr calcination at 650‡ C as compared to 800‡ C, 1 hr for conventional mixedoxide method. Sintering environment plays an important role in the densification of PLZT ceramics. Densities of the atmosphere sintered samples are much higher than those of normal sintered ones. PLZT ceramics derived from spray-dried powders have properties comparable to those derived from sol-gel ones. The spray-dried method presents a less expensive and more effective approach in the synthesis of PLZT ceramics.     

反应烧结法制备MgAlON的合成机理及烧结行为的研究

通过对以Al2 O3、MgO和AlN为起始原料 ,在氮气气氛中反应烧结合成MgAlON材料合成机理的研究发现 :在 12 0 0℃以前 ,MgO与Al2 O3反应生成镁铝尖晶石 ,此后 ,随着温度的升高 ,Al2O3不断向所形成的尖晶石中固溶 ;在 130 0℃以前 ,AlN基本上不参与反应 ,而在更高的温度下 ,AlN开始向尖晶石中固溶形成MgAlON ,约在 15 5 0℃时形成单一的MgAlON相。用热膨胀仪检测了试样的线变化率随温度和时间的变化 ,用最小二乘法回归分析了试样线变化率的实验数据 ,并根据烧结理论对MgAlON材料烧结初期的动力学进行了探讨。结果表明 ,MgAlON材料烧结初期的烧结机理以体积扩散为主     

大比例配用进口粉矿的烧结试验及生产

安钢烧结厂为应对原料条件的变化，就烧结配加进口粉矿进行了试验。以试验结果指导生产，顺利地实现了原料结构的改变，以及工艺参数的优化和生产指标的改善。