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71.
A multifunctional thiophene-based covalent triazine framework (TTPATTh) with triphenylamine as core is synthesized by Friedel–Crafts reaction of cyanuric chloride with thienyl derivative for the first time. The yield of TTPATTh (99.59%) is far higher than that of the carbazole-based CTF (TTPATCz, 47.03%). TTPATTh and TTPATCz possess high BET surface areas with 1235 and 2501 m2 g–1 as well as high pore volumes with 1.60 and 2.23 cm3 g–1, respectively. TTPATTh and TTPATCz have high thermal stability with high thermal decomposition temperatures of 514 and 598 °C in nitrogen atmosphere. With the introduction of triazine rings, the fluorescence sensing sensitivities of TTPATTh and TTPATCz to picric acid and iodine are improved significantly. Especially for TTPATTh, the Ksv values reach 5.95 × 105 and 1.61 × 104 L mol–1, and LODs reach 1.02 × 10–12 and 1.86 × 10–12 mol L–1. To the best of the knowledge, this is the most sensitive value among thiophene-based porous organic polymers to PA and I2. Furthermore, TTPATTh and TTPATCz can also adsorb iodine in vapor phase, cyclohexane solution and aqueous solution, and release iodine by heating or in ethanol solution. The efficiency of controlling the release of iodine is higher than that in ethanol. 相似文献
72.
《中国稀土学报(英文版)》2022,40(11):1785-1793
Developing and exploring organic–inorganic hybrid multi-lanthanide (Ln) implanted heteropolyoxometalates (HPOMs) has bloomed into an emerging research field. In this article, two neoteric d-gluconic acids (H6GA) concatenating multi-LnIII implanted heteropolytungstates K14H10[Ln4(H2O)4W6(H2GA)4O12(B-α-TeW9O33)4]·60H2O (Ln = La3+ (1), Pr3+ (2)) were obtained in acidic aqueous system. Attractively, in the polyanion structure of 1 and 2, six WVI and four LnIII centers are connected by four flexible H2GA4? ligands via carboxyl and hydroxyl groups, resulting in the heterometallic [Ln4(H2O)4W6(H2GA)4O12]8+ cluster and then the heterometallic cluster is surrounded by four [B-α-TeW9O33]8– segments. Electrochemical measurements for the 1@CFMCN/GCE sensor (CFMCN = carboxyl-functionalized multiwalled carbon nanotube; GCE = glass carbon electrode) demonstrate that 1@CFMCN/GCE shows benign recognition response to detecting noradrenaline (NDA). This research expands the structural diversity of Ln-implanted HPOMs and presents an electrochemical platform of recognizing NDA in the field of biosensors. 相似文献
73.
压缩感知及其图像处理应用研究进展与展望 总被引:2,自引:0,他引:2
压缩感知理论(Compressed sensing,CS)通过少量的线性测量值感知信号的原始结构,并通过求解最优化问题精确地重构原信号.该理论减少了数字图像及视频 获取时的存储及传输代价,也为后续的图像处理及识别的研究提供了新的契机,促进了理论和工程应用的结合. 阐述了CS的基本原理,综述了其关键技术稀疏变换、观测矩阵 设计、重构算法的一系列最新理论成果和发展,深入分析和比较了CS理论应用到图像处理领域的研究和发展状况,总结了其中存在的问题,并对未来的应用前景进行了展望. 相似文献
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76.
一种适用于降压DC-DC的改进型电流检测电路 总被引:2,自引:0,他引:2
基于电流模式控制能够较好地改善DC-DC的性能,设计一种适用于降压DC-DC的改进型电流检测电路,所提出的电流检测电路提高了电流感应的速度和精度。通过对电路的理论分析与设计,采用SMIC 0.18μm CMOS工艺模型,利用Cadence工具对电路进行仿真验证,所提出的电流检测电路在负载电流为50 mA~500 mA时都能够达到96%的效率以及小于40 ns的建立时间。在开关频率为2 MHz时,输入电压范围为2.5 V~4.2 V,所需电感值为4.7μH,电容值为10μF,输出电压纹波小于18 mV。 相似文献
77.
This paper proposes a tactile display providing both shear and normal feedback to the fingertip for generating three-axis tactile feedback during teleoperation of a surgical robot. The display is composed of five balloons actuated by controlling the pneumatic pressure. The implemented display is 18?mm?×?18?mm?×?15?mm. This size is suitable for mounting the display onto the master controls of a surgical robot. The maximum normal and shear displacements are 2 and 1.3?mm, respectively. The proposed tactile display may provide perceivable stimuli to a human finger pad in all five directions: normal, distal, proximal, radial, and ulnar. This paper also reports on the results of psychophysical measurement of the minimum perceivable movement of the developed tactile display for each of the five directions. 相似文献
78.
《Robotics and Autonomous Systems》2014,62(4):422-435
In recent years, autonomous robots have increasingly been deployed in unknown environments and required to manipulate or categorize unknown objects. In order to cope with these unfamiliar situations, improvements must be made both in sensing technologies and in the capability to autonomously train perception models. In this paper, we explore this problem in the context of tactile surface identification and categorization. Using a highly-discriminant tactile probe based upon large bandwidth, triple axis accelerometer that is sensitive to surface texture and material properties, we demonstrate that unsupervised learning for surface identification with this tactile probe is feasible. To this end, we derived a Bayesian nonparametric approach based on Pitman–Yor processes to model power-law distributions, an extension of our previous work using Dirichlet processes Dallaire et al. (2011). When tested against a large collection of surfaces and without providing the actual number of surfaces, the tactile probe combined with our proposed approach demonstrated near-perfect recognition in many cases and achieved perfect recognition given the right conditions. We consider that our combined improvements demonstrate the feasibility of effective autonomous tactile perception systems. 相似文献
79.
80.
为了降低信号重构算法的复杂度,实现对稀疏度未知信号的重构,提出了一种基于一次投影子空间追踪(OPSP)的信号重构方法。首先根据约束等距性质确定信号稀疏度的上下界,并将最接近上下界中值的整数作为稀疏度的估计值;然后在子空间追踪(SP)算法的框架下,去掉了迭代中观测向量在支撑集上的投影过程,降低了算法的复杂度。为了更准确地衡量算法的重构性能,提出用完整信号的重构概率作为衡量算法重构性能的指标。与传统的SP算法相比,所提算法可以重构稀疏度未知的信号,且重构时间短,重构概率高。仿真结果验证了该算法的有效性。 相似文献