Determination of Analytical Wavelength in Derivative Spectrophotometry

Abstract

The work presents two methods for preliminary determination of analytical wavelength when a binary system is analysed by derivative spectrophotometry. “The method of disturbing effect” involves the recording of derivative spectra of a series of two-component solutions where the concentration of one component of the mixture remains unchanged, whereas the concentration of the other changes. “The method of sixteen solutions” involves the recording of derivative spectra of a series of 16 solutions, in which to four concentrations of the one component correspond four different concentrations of the other component of the mixture.     

基于整车性能的液压减振器虚拟调校

为使减振器对车辆具有最佳减振效果,利用Rebrouck建模方法,建立了反映液压减振器阀系特性的参数化动力学模型,并将该减振器动力学模型以S-Function的形式嵌入到CarsimTM的某E-Class整车模型中。以整车动力学性能为优化目标,使用NSGA-II多目标优化算法,在扫频工况下,对车辆前、后轴减振器的阻尼力特性进行了虚拟调校。计算结果表明,经调校以后的液压减振器阻尼特性使得整车的动力学性能得到了较大程度的改善。     

具有温度补偿的FBG电流传感器研究

采用双光纤Bragg光栅(FBG)和2种不同的解调方法实现对基于电磁力的FBG电流传感的温度补偿,对2种解调方法进行比较。实验结果表明:采用光谱分析仪(OSA)进行波长解调,测量范围为0.35～2.5 A,灵敏度为0.93 nm/A;采用滤波调谐进行光强解调,测量范围为0.30～0.70 A,灵敏度可达到9.6 nW/mA。     

模糊自适应PID控制器参数整定的研究

主要研究了模糊自适应PID控制器参数整定方法,给出了预估计PID参数值的经验公式和方法。用MATLAB软件对PID控制、模糊自适应PID控制的控制性能分别进行了仿真研究,结果表明参数模糊自整定PID控制具有良好的稳态精度和自适应能力。     

基于变量纯度的波长选择方法在近红外光谱分析中的应用

提出了一种基于光谱纯度值的变量选择方法。对光谱中各变量计算其纯度值后,按降序将相应变量排列,采用PLS交互检验按前向选择法选择最佳变量子集。用本方法对3组分混合物体系及烟草样品的近红外光谱进行变量选择,并与全谱变量建模的结果进行了比较。结果表明本实验给出的波长变量优选方法是一种比较有效和实用的变量筛选方法,通过变量筛选,可极大地减少光谱信息重叠,从而提高定量校正模型的预测精度和建模效率。     

3,5-二硝基水杨酸测定古尼虫草中多糖含量方法

根据蔗糖标准溶液做吸收曲线，作K(mg/A)值图选择标准糖含量线性范围和确定分析波长为520nm.,古尼虫草中的多糖转化成还原糖测定多糖含量。     

White organic light-emitting diodes from three emitter layers

Three-wavelength white organic light-emitting diodes (WOLEDs) were fabricated using two doped layers, which were obtained by separating the recombination zones into three emitter layers. A sky blue emission originated from the 4,4′-bis(2,2′-diphenylethen-1-yl)biphenyl (DPVBi) layer. A green emission originated from a tris(8-quinolinolato)aluminum (III) (Alq₃) host doped with a green fluorescent 10-(2-benzothiazolyl)-1,1,7,7-tetramethyl-2,3,6,7-tetrahydro-1H,5H,11H-[1]benzopyrano [6,7,8-ij]-quinolizin-11-one (C545T) dye. An orange emission was obtained from the N,N′-bis(1-naphthyl)-N,N′-diphenyl-1,1′-biphenyl-4,4′-diamine (NPB) host doped with a red fluorescent dye, 4-(dicyanomethylene)-2-tert-butyl-6-(1,1,7,7-tetramethyljulolidyl-9-enyl)-4H-pyran (DCJTB). A white light resulted from the partial excitations of these three emitter layers by controlling the layer thickness and concentration of the fluorescent dyes in each emissive layer simultaneously. The electroluminescent spectrum of the device was not sensitive to the driving voltage of the device. The white light device showed a maximum luminance of approximately 53,000 cd/m². The external quantum and power efficiency at a luminance of approximately 100 cd/m² were 2.62% and 3.04 lm/W, respectively.     

电流型变频器中调节器参数的计算方法

根据电流型变频器的结构特点,结合工程实例,介绍了电流调节器和电压调节器参数的计算方法。     

光分组交换中的波长变换器配置研究

首先对波长变换器的功能及分类进行详细的论述,然后,对波长变换器的配置进行分析,总结出两种波长变换器配置方法,即独占式配置方法和共享式配置方法.针对独占式配置方法,本文使用仿真实验的方法研究了在不同类型的波长变换器下交换节点丢包性能的差异.本文还对独占式配置方法和共享式配置方法进行对比研究.