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1.
《Journal of the European Ceramic Society》2020,40(10):3577-3584
In this work, the grain boundaries composition of the polycrystalline CaCu3Ti4O12 (CCTO) was investigated. A Focused Ion Beam (FIB)/lift-out technique was used to prepare site-specific thin samples of the grain boundaries interface of CCTO ceramics. Scanning transmission electron microscopy (STEM) coupled with energy dispersive X-ray spectrometry (EDXS) and Electron Energy Loss Spectroscopy (EELS) systems were used to characterize the composition and nanostructure of the grain and grain boundaries region. It is known that during conventional sintering, discontinuous grain growth occurs and a Cu-rich phase appears at grain boundaries. This Cu-rich phase may affect the final dielectric properties of CCTO but its structure and chemical composition remained unknown. For the first time, this high-resolution FIB-TEM-STEM study of CCTO interfacial region highlights the composition of the phases segregated at grain boundaries namely CuO, Cu2O and the metastable phase Cu3TiO4. 相似文献
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Alena Yarysheva Dmitry Strel'tsov Sergey Malakhov Olga Arzhakova Larisa Yarysheva Alexandr Volynskii 《Polymer International》2020,69(7):627-634
This work addresses the phenomenon of the development of a patterned surface relief on polymer films via different modes of environmental crazing. Commercial films of semicrystalline poly(tetrafluoroethylene) (PTFE) and amorphous glassy poly(ethylene terephthalate) (PET) were subjected to tensile drawing in the presence of physically active liquid environments (carbon tetrachloride or aliphatic alcohols). The structure parameters and wettability of the modified films were studied by AFM, SEM, profilometer measurements and contact angle measurements. Environmental intercrystallite crazing of PTFE is accompanied by the development of an unstable structure with a high free surface, which experiences marked strain recovery upon unloading. As a result of the relief formation, PTFE hydrophobicity is enhanced (the water contact angle increases by 25°). Classical environmental crazing of PET films is accompanied by the formation of an anisotropic surface relief which is an assembly of crazes oriented perpendicular to the direction of tensile drawing, thus leading to the phenomenon of anisotropic wetting. The proposed approach for structural surface modification makes it possible to use the advantages of surface instability and spontaneous self‐organization of the polymer towards the development of a unique surface microrelief. © 2020 Society of Chemical Industry 相似文献
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在目标信号检测模块的基础上增加了测有计算模块,构成一种新型的单脉冲雷达点迹提取器,显著提高了雷达系统潜在的处理能力。 相似文献
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W. Shang B. Robrahn F. Golding M. H. J. Koch 《Nuclear instruments & methods in physics research. Section A, Accelerators, spectrometers, detectors and associated equipment》2004,530(3):513-520
A data acquisition system for time resolved X-ray scattering experiments using linear, quadrant or area gas proportional detectors with delay line readout based on commercially available hardware (National Instruments) is described. The system can easily be configured for recording data from point detectors (e.g. photomultipliers and photodiodes) and/or ancillary data only. Applications involving measurements with two different types of time to digital converters illustrate the features and performances of the system. 相似文献
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D. M. Suckling R. W. Peck L. M. Manning L. D. Stringer J. Cappadonna A. M. El-Sayed 《Journal of chemical ecology》2008,34(12):1602-1609
Disruption of Argentine ant trail following and reduced ability to forage (measured by bait location success) was achieved
after presentation of an oversupply of trail pheromone, (Z)-9-hexadecenal. Experiments tested single pheromone point sources and dispersion of a formulation in small field plots. Ant
walking behavior was recorded and digitized by using video tracking, before and after presentation of trail pheromone. Ants
showed changes in three parameters within seconds of treatment: (1) Ants on trails normally showed a unimodal frequency distribution
of walking track angles, but this pattern disappeared after presentation of the trail pheromone; (2) ants showed initial high
trail integrity on a range of untreated substrates from painted walls to wooden or concrete floors, but this was significantly
reduced following presentation of a point source of pheromone; (3) the number of ants in the pheromone-treated area increased
over time, as recruitment apparently exceeded departures. To test trail disruption in small outdoor plots, the trail pheromone
was formulated with carnuba wax-coated quartz laboratory sand (1 g quartz sand/0.2 g wax/1 mg pheromone). The pheromone formulation,
with a half-life of 30 h, was applied by rotary spreader at four rates (0, 2.5, 7.5, and 25 mg pheromone/m2) to 1- and 4-m2 plots in Volcanoes National Park, Hawaii. Ant counts at bait cards in treated plots were significantly reduced compared to
controls on the day of treatment, and there was a significant reduction in ant foraging for 2 days. These results show that
trail pheromone disruption of Argentine ants is possible, but a much more durable formulation is needed before nest-level
impacts can be expected.
Electronic supplementary material The online version of this article (doi:) contains supplementary material, which is available to authorized users. 相似文献
10.
本文介绍了磁电机点火系统的点火提前角测量原理。对点火系统的点火信号和触发信号进行采集、调理,再用单片机进行处理,最后用LabVIEW进行点火提前角数据存储和显示。 相似文献