Thermal Hydrolysis Synthesis and Characterization of Monoclinic Metahewettite CaV_6O_(16)·3H_2O

Monoclinic metahewettite CaV 6 O 16 ·3H 2 O has been fabricated via thermal hydrolysis of calcium vanadate(Ca 10 V 6 O 25). High purity calcium vanadate precipitate, featuring column structure with surface area of 8.61 m2/g, can be obtained by reacting sodium orthovanadate(Na 3 VO 4) with calcium oxide at 90 ℃ for 2 h. By acidifi cation of calcium vanadate in hot water at pH of 1.0-3.0, the monoclinic metahewettite crystals with uniform particle distribution, layered structure and nonporous structure can be fabricated. With the well crystallized layered structure, CaV 6 O 16 ·3H 2 O may be a potential cathode material for secondary batteries as well as super capacitor materials.     

Direct reduction of carburized pre-reduced pellets by microwave heating简

A new iron-making process using carburized pre-reduced iron ore pellets and microwave heating is investigated. The pre-reduced pellets, with a porous structure, and fine particles are carburized homogeneously at 400-650 ℃ in a CO atmosphere. The carburized carbon not only acts reaction as a reduction agent, but also absorbs microwave in the reduction process. Hence, the carburized pre-reduced pellets can be rapidly reduced by microwave heating. There are three procedures involved in the process, namely, gas-based pre-reduction, low-temperatttre carburization and deep reduction by microwave heating. Carburized pre-reduced iron ore pellets show a rapid temperature rise that is twice as fast as the results for pre-reduced pellets in the laboratory. This not only improves the efficiency of the microwave heating, but also accelerates the reduction of iron oxides. The temperature of the pre-reduced pellets rises to 1050 ℃ in 45 min when the carburization rate is 2.02%, and the metallization rate and compressive strength reach 94.24% and 1725 N/pellet, respectively.     

满堂扣件式钢管脚手架应力传递规律试验研究

满堂扣件式钢管脚手架在混凝土工程模板施工中有着广泛的应用,具有拆装方便、周转次数多、经济效益显著等诸多优点。本文通过3×3跨的满堂式扣件钢管脚手架加载实验,在施加不同荷载的情况下,研究脚手架某一立杆扣件处的应力传递规律。采用数值模拟和现场监测等分析方法,分析在不同的荷载作用下,架体内部钢管立柱的应力传递规律,其结论和研究方法可为研究类似架体的受力性能提供借鉴和参考,同时为现场关键点监控和远程安全预警系统开发提供相应的理论依据。     

高校数字图书馆海量信息存储系统架构研究

高校数字图书馆改变了传统图书馆的存在和服务方式,结合校园网络平台,实现用户对图书馆文献检索和数据共享网络化和图书馆办公自动化。本文结合主流的海量信息存储技术DAS （直接附加存储）、NAS （网络附加存储）、SAN （存储区域网络）和云存储,设计数据资源分级分布存储的高校数字图书馆网络信息存储系统架构。满足了数字图书馆存储系统的高容量、易扩容和数据资源安全可靠性等方面需求。     

基于嵌入式的电网自动调度信息分级采集系统设计

传统系统在电网调度信息采集的过程中,未对其进行分级,导致系统采集数据误差较大,准确度较低.为了提高电网自动调度信息分级采集能力,提出基于嵌入式的电网自动调度信息分级采集系统.构建电网自动调度信息的大数据挖掘模型,结合嵌入式调度方法,实现电网自动调度信息分级采集和优化检索.仿真结果表明,电网自动调度信息分集采集的准确度较高,自适应性较好,具有一定可行性,数据准确性满足系统设计需要,达到实用效果.     

面向不平衡补偿的三相四桥臂并网逆变器控制策略研究

针对微网中大量接入不对称负载且日益增多的现状,引起的三相电压不平衡问题,提出基于三相四桥臂逆变器的多状态分层协同补偿策略.利用四桥臂并网逆变器三相输出独立的特点,采用双同步坐标系解耦软件锁相准确跟踪微网相位,根据电网三相电压值的大小,对发电装置发出的电源进行三相功率分配,对低电压相进行功率补偿以实现微电网电压的平衡.利用MATLAB/Simulink进行建模仿真,并对个别状态进行了试验.结果 表明,对于微电网中可能存在的电压不平衡情况,所提出的补偿控制策略可以有效改善电压不平衡的问题,并对其进行补偿.     

涡流法检测铝硅合金显微组织的误差分析

当采用涡流法检测铝硅合金活塞显微组织级别时，合金的含硅量、变质剂的加入量以及温度变化都将影响分级结果的准确性。分析了由以上因素引起的显微组织的分级误差，确定了含硅量不同时的修正因子，变质剂的加入量以及温度变化时的校核方式，并采用数理统计方法分析了测试的可靠性，最后得出该涡流检测的分级准确率可迭99％。     

贾沟矿区破碎系统改造及其效果

由于贾沟矿区铝土矿矿床赋存条件，使采出的矿石含泥量较大，矿仓下料口易堵塞，放矿困难，使成列车皮不能同时装车。在破碎流程中增设筛分设施，使地矿与粉矿分开，块矿进仓，粉发矿送到露天堆场，防止矿仓堵矿，放矿顺利，并做到铝土矿分级供矿，取得较好的经济效益。     

Plasma spray forming of functionally graded materials mould

A new technology of functionally graded materials(FGM) mould fabricated by plasma spraying and arc spraying was developed. According to applied characteristic of plastic mould, the reasonable coatings of FGM were designed and their microstructures were analyzed. At the same time, some key problems were solved including spray mould fabricating, FGM forming and demoulding, etc. The results show that the service performance of the FGM mould is much more excellent than the one composed of the traditional materials, and the life span can also be greatly increased. The technology will have a significant influence on materials development in mould industry.     

铸造Al-Si-Cu-Mg合金分级热处理工艺及对力学性能的影响

通过示差热分析及对Al-7.0Si-2.5Cu-0.5Mg合金热处理工艺参数的研究发现为了防止合金中低熔点共晶物在固溶处理过程中熔化,同时提高Q、Al2Cu等相在合金中的溶解度,应选择分级固溶的方式进行.一级固溶在500 ℃固溶3 h后,可使合金中低熔点共晶物完全溶解,此时合金的熔点为540 ℃;综合各因素,该合金较好的热处理工艺为500 ℃×3 h、530 ℃×14 h;175 ℃×6 h,此时,合金的力学性能可以达到σb≥385 MPa,δ5≥5.0%.