稀土棕红色陶瓷颜料的制备

在低温下,采用溶胶均匀共沉淀法合成了含少量稀土氧化物CeO2的棕色陶瓷颜料,并应用颜色测定、SEM及XRD分析等手段对颜料的颜色、粒度及结晶构造进行了表征。同时,将合成的颜料应用于陶瓷釉料中,表明该颜料可以应用于1320℃的高温环境下。     

Study on Effect of Flux on CeMgAl11O19：Tb^3＋ Phosphor

High calcination temperature is an important factor in the preparation process of CeMgAl11O19:Tb^3 . To decrease the temperature, different fluxes (H3BO3, MgF2 and AlF3) were tested in order to compare their influence on the luminescence property and particle size distribution of CeMgAl11O19: Tb^3 . The result shows that when the content of MgF2 is 0.1 mol/mol, the intensity of luminescence can attain a maximum. Furthermore, MgF2 can improve the particle size quality of the phosphor. So MgF2 can take the place of the conventional flux H3BO3 to prepare high quality CeMgAl11O19:Tb^3 phosphor. In addition, the relation between phosphor property and content of AlF3 was also studied. The crystal structure of the phosphor was analyzed by XRD method. The phase composition analysis shows that the reason of decrease of the brightness of CeMgAl11O19:Tb^3 phosphor is the emergence of TbAlO3 and α-Al2O3 during the preparation process.     

Effect of Y2O3, CeO2 on Sintering Properties of Si3N4 Ceramics

The effect of rare earth oxides Y203 or Ce02 on sintering properties of Si3N4 ceramics was studied and the mechanism of assisting action during sintering was analyzed. The results in dicate that the best sintering properties appear in Si3N4 ceramics with 5% Y203 or 8% CeO2. Secondary crystallites are formed at grain boundaries after heat treatment,which decreases the amount of glass phase and contributes to the improvement of high-temperature mechanical properties of silicon nitride.     

稀土的应用

我国是稀土资源大国，又是稀土生产大国，随着稀土金同冶炼技术的发展，各种稀土产品相继生产，稀土应用不断开拓新的领域，已渗入到冶金工业、石油化工、玻璃陶瓷、电子技术、农业、医疗等各个领域，在高技术新材料上，如磁性材料、萤光材料、贮氢材料等，稀土有着不可磨灭的功绩。1996年国内稀土应用达14530t，备领域构成的消费比例，冶金工业占34．1％，石油化工占24．l％，玻璃陶瓷占9．6％，新材料占11．0％，其他行业（农业、轻纺等）占21．2％。1＃土在钢铁及合全中的应用在冶金工业中，稀土被称为金属材料的“维生素”，其特点是加…     

复混肥料综述（上）

简单介绍了我国复混肥料的概况、生产条件、生产工艺、配方及施用效果。并介绍了专用肥、微肥、稀土肥料的配方、工艺和施用效果。     

磁六极透镜场分布的测定

本文介绍一种用于电镜透镜球差矫正系统中的磁六极透镜的磁场分布实验测定原理及方法,并给出较详细的测量数据。测量结果说明这种透镜内磁场分布是以3θ为宗量的正弦和余弦规律,随r的变化是二次方规律。