Preparation and sintering of nano Fe coated Si3N4 composite powders

Fe/Si₃N₄ composite powder was synthesized by the heterogeneous precipitation-thermal reduction process, and then pressed into flakes under a pressure of 10 MPa. Flakes were sintered by pressureless and hot-pressing at 1 600 °C under 0.1 MPa N₂. The chemical composition, phases and microstructure of composite powder and sintered flakes were investigated by energy dispersive spectroscopy (EDS), X-ray diffraction (XRD), scanning electron microscopy (SEM) and transmission electron microscopy (TEM). The results show that the structure of composite powders is Si₃N₄ coated by nano Fe. The crystal phases of sintered flakes by pressureless are Fe(Si) compound, SiC and Si₃N₄. The crystal phases of the sintered samples by hot-pressing are Fe, Fe(Si) compound and Si₃N₄. It is found that crystal phases flakes obtained by pressureless and hot-pressing are very different. Foundation item: Project(50804016) supported by the National Natural Science Foundation of China     

Zn掺杂对GdMnO体系的晶体结构影响

系统研究了Gd（1-x）ZnxMnO3（x=0,0.2,0.4,0.6,0.8,1.0）体系的结构。结果表明,实验样品具有正交对称性结构。当Zn掺杂浓度x≤0.4时,随着Zn掺杂浓度的增加,晶格常数b、c减小,而晶格常数a增大,晶胞体积逐渐减小;当掺杂浓度x≥0.6时,Zn掺杂浓度的增加,晶格常数b、c增大,而晶格常数a减小,晶胞体积逐渐增大。计算表明Gd（1-x）ZnxMnO3系列化合物的容忍因子在0.76~0.92范围,可以形成稳定的钙钛矿结构。     

Prevention and forecasting of rock burst hazards in coal mines

Rock bursts signify extreme behavior in coal mine strata and severely threaten the safety of the lives of miners, as well as the effectiveness and productivity of miners. In our study, an elastic-plastic-brittle model for the deformation and failure of coal/rock was established through theoretical analyses, laboratory experiments and field testing, simulation and other means, which perfectly predict sudden and delayed rock bursts. Based on electromagnetic emission (EME), acoustic emission (AE) and microseism (MS) effects in the process from deformation until impact rupture of coal-rock combination samples, a multi-parameter identification of premonitory technology was formed, largely depending on these three forms of emission. Thus a system of classification for forecasting rock bursts in space and time was established. We have presented the intensity weakening theory for rock bursts and a strong-soft-strong (3S) structural model for controlling the impact on rock surrounding roadways, with the objective of laying a theoretical foundation and establishing references for parameters for the weakening control of rock bursts. For the purpose of prevention, key technical parameters of directional hydraulic fracturing are revealed. Based on these results, as well as those from deep-hole controlled blasting in coal seams and rock, integrated control techniques were established and anti-impact hydraulic props, suitable for roadways subject to hazards from rockbursts have also been developed. These technologies have been widely used in most coal mines in China, subject to these hazards and have achieved remarkable economic and social benefits.     

蜂窝陶瓷型La0．8Sr0.2MnO3催化剂VOCs催化燃烧反应活性

以堇青石(CH)为第一载体,六铝酸盐(HA)为第二载体(washcoat),La0.8Sr0.2MnO3(LSM)为活性物种,制备了LSM/HA/CH催化剂.XRD表征发现,LSM具有完善的钙钛矿晶型.SEM观察表明,活性物种在涂层表面分散均匀.通过对苯、甲苯、二甲苯、乙酸乙酯、丙酮和乙醇六种有机物的性能测试,发现LSM/HA/CH对上述六种有机物均具有很好的催化活性,特别是对乙酸乙酯等含氧有机物表现出更好的燃烧性能,在10000 h-1空速下,反应温度为240℃时即可将含氧有机物完全燃烧.     

城市三维快速建模及浏览的研究与实现

随着计算机图形技术的发展,三维GIS成为城市规划的重要手段之一。如何实现三维场景快速构建以及实时浏览成为三维GIS研究及应用的热点。江苏省镇江市的城市三维可视化快速建模与浏览系统的研究与建立,可为相关应用提供借鉴经验和参考方案。     

MOTOMAN-HP3型机器人运动学建模

根据MOTOMAN-HP3型机器人具体结构特点,建立机器人的运动学模型,求出正逆解.并在机器人运动学建模过程中,对关节运动范围的转换规律进行了研究.为机器人运动分析、离线编程、轨迹规划等打下了基础.     

数控加工三维场景几何建模技术研究

讨论了基于构件技术的数控加工三维场景建模技术,并以OpenGL和Visual C++6.0为开发平台,开发出一个基于STL文件格式的建模系统.     

基于嵌入式农田信息采集系统的研究

基于嵌入式系统的农业数据采集系统采用先进的无线通信技术、GPS定位技术和嵌入式技术来解决农业数据的远程采集问题．论文以嵌入式系统为核心,提出和分析了实现系统的关键技术．采用无线通信GPRS网络将现场采集到的有关经纬度、高程、时间以及农田环境数据等信息进行分析和处理,并传送到远程管理中心,为农业生产提供决策支持．它能够解决农业的远程数据采集和传输问题．     

基于STL的楔横轧模具三维建模系统

采用Delphi语言开发了楔横轧模具三维建模系统。系统依据参数化的楔横轧模具数据,采用STL文件格式,自动输出楔横轧模具三维图形,提高了楔横轧模具的设计效率。由于大多数的CAM系统都可以读取STL文件,应用该系统能够提高模具的数控加工的效率。     

三维声纳频域波束形成算法的优化及实现

为了对三维声纳频域波束形成算法进行优化,提出了一种算法的优化方法。利用声纳回波信号的位移矢量分解与合成原理,推导出波束强度与相应方向角的数学关系式,进而使算法得到优化,并对优化的波束形成算法进行了仿真。同时,给出了实现此算法的两种数据通路,并对其内存需求量和计算量进行了分析。最终在XilinxISE环境下,在现场实现可编程门阵列(FPGA)上对该两种数据通路进行了仿真,并列出了相应的资源利用情况。优化后的算法不仅可以得到与传统算法相同的波束强度矩阵结果,而且减少了存储相移参数所需的内存空间。