缺失数据下m相依样本的大样本性质

讨论了缺失数据在随机补充方式下均值的估计,证明了估计的相合性和渐进正态性,并给出了经验似然比统计量的渐进分布．     

住宅设计原理——“住”的思考

居住类建筑一直是建筑设计人员关注的重点,关于"住"的思考人们也从未停歇过,将结合一些流行的住宅设计观点展开对于"住"的思考.     

平面盘形凸轮轮廓曲线统一建模的研究

将从动件的直线往复移动和定点往复摆动用虚拟摆动统一表示,采用单参数包络曲线理论建立直动和摆动从动件平面盘形凸轮轮廓的统一数学表达式。根据统一的数学表达式可以开发出一套适合于各类平面盘形凸轮机构的CAD软件包。     

一般均质地面承载力现场试验

为了评判施力盘作用下地面的承载安全,进行了一般均质地面承载力静态与动态荷载现场试验.采用平板载荷静态加载方法进行了模拟施力盘静态荷载的平板载荷试验,根据相似准则π定理进行了缩比施力盘动载试验.在现场试验的基础上研究了静载条件下沉降量随时间变化的S-t曲线,不同尺寸承载板在相应载荷作用下的地面土体沉降量之间关联关系的P-S/D曲线及动、静荷载下载荷与沉降量关系的P-S曲线以及动静载荷对比的P-S曲线.分析结果表明:对于进行现场试验的均质地面,S-t曲线表明静态加载方法合理;P-S/D曲线在极限载荷内呈线性比例关系;动载下的沉降量S远远小于静载条件下的沉降量S,动载下的土体变形刚度较静载下的变形刚度高,瞬间动态荷载造成的地面沉降可忽略.     

The role of charcoal on DTA curves of organo-clay complexes: an overview

DTA of organo-clay complexes supplemented by other thermal analysis methods supplies information on the thermal reactions, properties and stability of the complex, the amount and properties of the adsorbed water in the organo-clay and on the bonding between the organic species and the clay. It is used to identify the mineral to differentiate between various complexes composed of the same clay and the same organic ligand and to establish their composition. During the gradual heating in oxidizing atmospheres the adsorbed organic material is oxidized, giving rise to significant exothermic peaks. DTA curves of organo-clays are divided into three regions: (1) the dehydration of the clay, (2) the thermal oxidation of the organic material and (3) the dehydroxylation of the clay. The exothermic oxidation reaction occurring during the gradual heating of the sample takes place in two steps, in the range 200–500 °C, oxidation of organic hydrogen and formation of water and charcoal, and 400–750 °C, oxidation of charcoal and formation of CO₂. The exothermic peak temperatures depend on the mineral and on the organic compound and on the types of bonding between these two components of the organo-clay complex. The present communication concentrates in the role of the combustion of charcoal in the study of the fine structure of the complex and of the type of associations between the organic compound and the clay.     

The Mechanical Behaviour of Polyimide/Copper Laminates Part 2: Peel Energy Measurements

The mechanical peel behaviour of laminates consisting of polyimide films adhered to copper foil using a modified acrylic adhesive has been studied over a wide range of test rates and temperatures. The laminates were prepared from polyimide films which had been subjected to either a “high-thermal history” or a “low-thermal history” treatment during the production of the film. The measured peel energies of the laminates could be superimposed to give a master curve of peel energy versus the reduced rate of peel test, Ra_T, where R is the rate of peel test and a_T is the time-temperature shift factor. The appropriate shift factors were a function of the test temperature and were mainly deduced from tensile tests conducted on the bulk adhesive. The “high-thermal history” laminates gave higher peel energies and the locus of failure of the laminates was mainly by cohesive fracture through the adhesive layer. At low values of log₁₀ Ra_T, i.e. Low rates of peel and high test temperatures, the “low-thermal history” laminates also failed in the adhesive layer and possessed similar peel energies to those measured for the “high-thermal history” laminates. However, at high log₁₀ Ra_T values, the peel energies measured for the “low-thermal history” laminates were lower and showed a wider scatter. These arose from a different locus of failure occurring in these “low-thermal history” laminates when tested under these conditions. Namely, it was found that most of these laminates failed in a weak boundary layer in the outer regions of the “low-thermal history” polyimide film.     

50000m3外浮顶储罐施工方法探讨

本文根据我公司在新疆油田公司油气储运公司承建的50000m~3外浮顶储罐建设工程实践,借鉴国内外大型储罐建造技术,结合我公司成熟的储罐建造经验,探讨建造大型外浮顶储罐的一种施工方法——外脚手架正装法,同时介绍工厂预制和现场自动化焊接技术,并结合工期控制等问题论述该施工方法的特点。     

Activation of Ni/A12O3 catalysts through modification of the Al2O3 support

The effect of alumina pretreatment on the performance of alumina supported nickel catalysts was demonstrated in gas phase hydrogenation of toluene to methylcyclohexane. The state of the alumina was changed from pure to pure phase through various heat treatments in air. The catalysts were prepared from vapor phase by saturating the accessible binding sites on the pretreated alumina with the nickel precursor. The highest number of active sites for hydrogenation was observed for catalysts prepared on alumina having an incomplete phase transition and a / alumina phase ratio between 0.5 and 10. Results from temperature programmed desorption (TPD) studies revealed that a maximum in weakly chemisorbed hydrogen as well as in total amount of desorbed hydrogen was found for the same catalysts. By hydrogen chemisorption studies the total hydrogen uptake was found to correlate with the observed hydrogenation maximum. It is suggested that both the chemical and physical properties of the alumina influence the activity. An optimal metal-support interaction and structural defects on the alumina due to the phase transition can explain the observed maximum in the number of active sites and in hydrogen uptake.     

Implementing optimized pairings with elliptic nets

In this paper,we use elliptic nets to implement the optimized Ate pairings and optimal pairings on the Barreto-Naehrig curves with embedding degree 12.In order to do the arithmetic of elliptic curves over finite fields with elliptic nets,we first give some basic properties of elliptic nets associated to elliptic curves over finite fields and the expression of Miller function in terms of elliptic nets.Then we give formulae to compute some optimized pairings with elliptic nets,which is a new method to implement pairings.This method with elliptic nets has time complexity comparable to Miller’s algorithm and it can be optimized.     

Interfacial adhesion reaction of polyethylene and starch blends using maleated polyethylene reactive compatibilizer

The interfacial reaction of the polyethylene (PE)/starch blend system containing the reactive compatibilizer maleated polyethylene (m‐PE) was directly characterized by Fourier transform infrared (FTIR) spectroscopy. A significant amount of anhydride groups on m‐PE existed as hydrolyzed forms, resulting in a large amount of carboxyl groups. Using a vacuum‐heating‐cell designed in the laboratory, the carboxyl groups were successfully transformed into the dehydrolyzed state (i.e., anhydride group). This result enabled the direct spectroscopic observation of chemical reaction occurring at the interface. For the PE/starch blend system containing m‐PE, the chemical reaction at the interface was verified by the evolution of ester and carboxyl groups in the FTIR spectra. The effect of the reactive compatibilizer on the interfacial morphology was also examined by scanning electron micrography (SEM). Enhanced interfacial adhesion was clearly observed for the blend system containing reactive compatibilizer. Tensile strengths of blend systems containing m‐PE also increased noticeably compared with the corresponding system without compatibilizer. A similar observation was made for the breaking elongation data. © 2002 Wiley Periodicals, Inc. J Appl Polym Sci 83: 767–776, 2002