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61.
In view of the importance for CoxOy,-MoO3/-Al2O3 hydrodesulphurization (HDS) catalysts, the reactivity of cobalt oxide layers towards cobalt aluminate formation was investigated on both MoO3-covered and bare -Al2O3 substrates. Co3O4/MoO3/-Al2O3 and Co3O4/-Al2O3 systems were prepared by vapour-deposition of MoO3 (12 × 1015 Mo atoms/cm2) and Co (400 × 1015 Co atoms/cm2) layers onto a -Al2O3 substrate, followed by oxidation of the Co layer to Co3O4. After annealing at 800°C for 40 h, the interfacial reaction to cobalt aluminate was assessed using Rutherford backscattering spectrometry. The presence of molybdenum oxide appeared to enhance cobalt aluminate formation. The Mo atoms, which spread out over the entire cobalt-containing layer, presumably caused a high defect density, which explains the observed higher reaction rate. The amount of MoO3 was much too low to stabilize all cobalt atoms by cobalt molybdate formation. 相似文献
62.
通过轻骨料混凝土LC30,LC40与普通混凝土C30,C40的对比试验,研究了同等强度等级下轻骨料混凝土与普通混凝土的力学性能;得出了不同强度等级的轻骨料混凝土的应力应变关系曲线.将试验结果与规程模型进行对比,分析其差异,进一步给出下降段的应力应变曲线方程. 相似文献
63.
主要针对7.63m特大型焦炉砌筑施工技术,从工程实践效果分析其施工技术在质量、工期、成本等方面收到良好的经济效益和社会效益,现对7.63m特大型焦炉施工技术作简要介绍。 相似文献
64.
钱永江 《延边大学学报(自然科学版)》2009,35(3):207-210
讨论了缺失数据在随机补充方式下均值的估计,证明了估计的相合性和渐进正态性,并给出了经验似然比统计量的渐进分布. 相似文献
65.
居住类建筑一直是建筑设计人员关注的重点,关于"住"的思考人们也从未停歇过,将结合一些流行的住宅设计观点展开对于"住"的思考. 相似文献
66.
将从动件的直线往复移动和定点往复摆动用虚拟摆动统一表示,采用单参数包络曲线理论建立直动和摆动从动件平面盘形凸轮轮廓的统一数学表达式。根据统一的数学表达式可以开发出一套适合于各类平面盘形凸轮机构的CAD软件包。 相似文献
67.
The mechanical peel behaviour of laminates consisting of polyimide films adhered to copper foil using a modified acrylic adhesive has been studied over a wide range of test rates and temperatures. The laminates were prepared from polyimide films which had been subjected to either a “high-thermal history” or a “low-thermal history” treatment during the production of the film. The measured peel energies of the laminates could be superimposed to give a master curve of peel energy versus the reduced rate of peel test, RaT, where R is the rate of peel test and aT is the time-temperature shift factor. The appropriate shift factors were a function of the test temperature and were mainly deduced from tensile tests conducted on the bulk adhesive. The “high-thermal history” laminates gave higher peel energies and the locus of failure of the laminates was mainly by cohesive fracture through the adhesive layer. At low values of log10 RaT, i.e. Low rates of peel and high test temperatures, the “low-thermal history” laminates also failed in the adhesive layer and possessed similar peel energies to those measured for the “high-thermal history” laminates. However, at high log10 RaT values, the peel energies measured for the “low-thermal history” laminates were lower and showed a wider scatter. These arose from a different locus of failure occurring in these “low-thermal history” laminates when tested under these conditions. Namely, it was found that most of these laminates failed in a weak boundary layer in the outer regions of the “low-thermal history” polyimide film. 相似文献
68.
The effect of alumina pretreatment on the performance of alumina supported nickel catalysts was demonstrated in gas phase hydrogenation of toluene to methylcyclohexane. The state of the alumina was changed from pure to pure phase through various heat treatments in air. The catalysts were prepared from vapor phase by saturating the accessible binding sites on the pretreated alumina with the nickel precursor. The highest number of active sites for hydrogenation was observed for catalysts prepared on alumina having an incomplete phase transition and a / alumina phase ratio between 0.5 and 10. Results from temperature programmed desorption (TPD) studies revealed that a maximum in weakly chemisorbed hydrogen as well as in total amount of desorbed hydrogen was found for the same catalysts. By hydrogen chemisorption studies the total hydrogen uptake was found to correlate with the observed hydrogenation maximum. It is suggested that both the chemical and physical properties of the alumina influence the activity. An optimal metal-support interaction and structural defects on the alumina due to the phase transition can explain the observed maximum in the number of active sites and in hydrogen uptake. 相似文献
69.
In this paper,we use elliptic nets to implement the optimized Ate pairings and optimal pairings on the Barreto-Naehrig curves with embedding degree 12.In order to do the arithmetic of elliptic curves over finite fields with elliptic nets,we first give some basic properties of elliptic nets associated to elliptic curves over finite fields and the expression of Miller function in terms of elliptic nets.Then we give formulae to compute some optimized pairings with elliptic nets,which is a new method to implement pairings.This method with elliptic nets has time complexity comparable to Miller’s algorithm and it can be optimized. 相似文献
70.
Seong Ik Yoo Tae Yeon Lee Jin‐San Yoon Ik‐Mo Lee Mal‐Nam Kim Han Sup Lee 《应用聚合物科学杂志》2002,83(4):767-776
The interfacial reaction of the polyethylene (PE)/starch blend system containing the reactive compatibilizer maleated polyethylene (m‐PE) was directly characterized by Fourier transform infrared (FTIR) spectroscopy. A significant amount of anhydride groups on m‐PE existed as hydrolyzed forms, resulting in a large amount of carboxyl groups. Using a vacuum‐heating‐cell designed in the laboratory, the carboxyl groups were successfully transformed into the dehydrolyzed state (i.e., anhydride group). This result enabled the direct spectroscopic observation of chemical reaction occurring at the interface. For the PE/starch blend system containing m‐PE, the chemical reaction at the interface was verified by the evolution of ester and carboxyl groups in the FTIR spectra. The effect of the reactive compatibilizer on the interfacial morphology was also examined by scanning electron micrography (SEM). Enhanced interfacial adhesion was clearly observed for the blend system containing reactive compatibilizer. Tensile strengths of blend systems containing m‐PE also increased noticeably compared with the corresponding system without compatibilizer. A similar observation was made for the breaking elongation data. © 2002 Wiley Periodicals, Inc. J Appl Polym Sci 83: 767–776, 2002 相似文献