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The corrosion behavior of 2A02 Al alloy under simulated marine atmospheric environment has been studied using mass-gain, scanning electron microscope/energy dispersive spectroscopy (SEM/EDS), laser scanning confocal microscopy, X-ray diffraction spectroscopy and localized electrochemical methods. The results demonstrate that the relationship between the corrosion induced mass-gain and the corrosion time is in accordance with the power rule. The mass-gain increases gradually during the corrosion time, while the corrosion rate decreases. With ongoing of the corrosion, corrosion products film changed from a porous to a compact structure. The various spectroscopic data show that the corrosion products films composed mainly of Al(OH)3, Al2O3 and AlCl3. The electrochemical corrosion behavior of the 2A02 Al alloy was studied by electrochemical impedance spectroscopy (EIS). 相似文献
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视频信号的的采集和处理是一个复杂的过程,这需要程序设计者了解视频信号的构成,充分利用复合视频信号中的各种同步信息作为视频信号采集的控制信号,从而完成信号的采集。 相似文献
76.
This paper presents a novel signal processing technique for a square wave temperature modulated carbon black/polymer composite sensor. The technique consists of only two mathematical operations: summing the off- and on-transients of the conductance signals, and subtracting the steady-state conductance signal. The technique has been verified through its application to a carbon black/polyvinylpyrrolidone composite chemoresistor. Identification of water, methanol and ethanol vapours was successfully demonstrated using the peak time of the resultant curves. Furthermore, quantification of those vapours was found to be possible using the height of the peak heights, which was linearly proportional to concentration. The technique does not require zero-gas calibration and thus is superior to previously reported techniques. 相似文献
77.
Mariana Emilia Rasa Orlando Christopher M.A. 《Sensors and actuators. B, Chemical》2009,142(1):308-315
A new approach for building a bio-conductive interface for enzyme immobilisation is described. This strategy permits very simple preparation of the enzyme biosensor and also reveals direct electron transfer features. A graphite-epoxy resin composite (GrEC) electrode modified with functionalised multi-wall carbon nanotubes (MWCNTs) immobilised by 1-ethyl-3-(3-dimethylaminopropyl) carbodiimide together with N-hydroxysuccinimide (EDC–NHS) in a chitosan (Chit) matrix was prepared and characterised by cyclic voltammetry (CV) and electrochemical impedance spectroscopy (EIS) in the presence of hexaammineruthenium (III) chloride. It was then used as a base for glucose oxidase (GOx) immobilisation by the simple method of crosslinking with glutaraldehyde (GA) with bovine serum albumin (BSA) as carrier protein. The resulting mediator-free biosensor was applied to the determination of glucose in amperometric mode at different applied potentials and the mechanism of reaction was also investigated by cyclic voltammetry, with and without dissolved oxygen in solution. Analytical parameters, as well as reproducibility, repeatability and stability were determined. Interferences were assessed using different compounds usually present in natural samples, such as wines, juices or blood, in order to evaluate the selectivity of the developed biosensor. The novel combination of carbon nanotubes immobilised with chitosan crosslinked with EDC–NHS and glucose oxidase immobilised by crosslinking with glutaraldehyde offers an excellent, easy to make biosensor for glucose determination without interferences. 相似文献
78.
证明在离散余弦变换和小波变换中,图像经空域置乱前后在频域内不变的系数规律,根据构造的复合混沌迭代动力系统,提出2个利用不变频域变换系数规律的构造函数,生成复合混沌迭代动力系统需要的初始值,给出脆弱的图像自适应置乱算法以及相似度和抗攻击半径的置乱算法评价概念。实验表明,算法无需任何附加信息即可提取出原始图像,对各种攻击十分敏感,平均抗攻击半径高于一般算法,适用于法庭、医学等要求极其严格的场合。 相似文献
79.
聚乙烯/膨化石墨导电复合材料的研究 总被引:1,自引:0,他引:1
研究了不同的工艺条件对聚乙烯/膨化石墨导电性能和力学性能的影响。结果表明,溶液插层法具有较低的导电渗滤阈值,但其力学性能也较差。 相似文献
80.
以聚偏氟乙烯为基质,加入适量的P2O5,制备了P2O5填充的PVDF复合聚合物质子导电膜,采用交流阻抗谱的方法研究了P2O5的质量分数不同的复合膜的导电性能及相对湿度对电导率的影响.结果表明,该电解质的室温电导率达到10-2 S·cm-1,相对湿度在20%~90%范围内,对电解质的导电性影响不大. 相似文献