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51.
测量A0纯铝在去离子水中的极化曲线用来模拟反应堆池壳的点蚀.研究表明A0纯铝在去离子水中很容易钝化.实验中用美国EG&G普林斯顿应用研究公司生产的273型恒电位/恒电流仪测量模拟孔电位,极化曲线表明模拟腐蚀坑处于钝化状态,即便是氧化膜破裂,腐蚀坑也发展得很慢.用pH计测量孔中pH的变化,并得到其工作曲线,此曲线表明带有氧化膜的点蚀坑坑内存在明显的酸化现象.并对A0铝池壳的服务寿命进行了估计. 相似文献
52.
53.
Influence of expandable graphite on fire resistance and water resistance of flame-retardant coatings 总被引:1,自引:0,他引:1
Expandable graphite (EG) coating and ammonium polyphosphate-pentaerythritol-melamine (APP-PER-MEL) coating were prepared. Thermal degradation and char formation of the coatings were investigated by differential thermal analysis (DTA), thermogravimetry (TG), X-ray diffraction (XRD), scanning electron microscopy (SEM) and X-ray photoelectron spectroscopy (XPS). The results have shown that the anti-oxidation and fire-resistant properties of expandable graphite coating containing EG with size of 74 μm are better than those of APP-PER-MEL coating. The static immersion test was applied to study water resistance of the coatings, and the fire protection test and mechanical test were used to analyse heat insulation and mechanical properties of coatings before and after water immersion. The fire-resistant and mechanical properties of APP-PER-MEL coating were severely damaged by water immersion, whereas EG coating containing 8.5% EG with size of 74 μm could retain the good fire resistance even after 500 h water immersion. 相似文献
54.
Mario Gleria Roberta Bertani Roger De Jaeger 《Journal of Inorganic and Organometallic Polymers》2004,14(1):1-28
A general survey of fluorinated phosphazene polymers starting from their synthesis in 1965 to recent times is presented. Various types of fluorinated phosphazenes are described depending on the way fluorine atoms are connected to the polyphosphazene skeleton. The characterization, properties and practical utilization of these compounds in different domains are critically discussed. 相似文献
55.
The effect of SO2 on catalytic activity for NO reduction to N2 by methanol in excess oxygen over $\gamma$ -alumina has been investigated. SCR activity increased initially upon exposure of a fresh $\gamma$ -alumina catalyst to SO2 which is attributed to formation of Brønsted acid sites. Longer exposure to SO2 leads to a decline in catalytic activity to a lower steady-state NOx reduction activity which is independent of the SO2 content in the feed gas. 相似文献
56.
K. G. Shkadinskii N. I. Ozerkovskaya S. V. Kostin 《Combustion, Explosion, and Shock Waves》2004,40(3):285-294
The specific features of dynamics of the thermal explosion in systems porous reagent–active gas–solid product under conditions where the heattransfer and masstransfer regions are separated from the ambient medium are considered. In addition to the competition of heat release and heat removal, the process of initiation of exothermal chemical interaction in these systems under normal pressures depends significantly on conditions of filtration transport of the gaseous reagent. The induction and postinduction periods of the thermal explosion are studied. The theoretical analysis of thermalexplosion issues is supplemented by an experimental study of the process for the porous titanium–nitrogen–titanium nitride system. 相似文献
57.
根据实测γ~∞_1用单参数Wilson方程预测均三甲苯-DMP和偏三甲苯-DMP二元体系汽液平衡,并推算均三甲苯-偏三甲苯-DMP三元体系的汽液平衡,与实测数据比较,均获得良好结果。 相似文献
58.
In situ synchrotron X-ray studies on copper-nickel 5 V Mn oxide spinel cathodes for Li-ion batteries
Partial substitution of Mn in lithium manganese oxide spinel materials by Cu and Ni greatly affects the electrochemistry and the cycle life characteristics of the cathode. Substitution with either metal or a combination of both metals in the spinel lattice structure reduces the 3.9-4.2 V potential plateaus associated with the conversion of Mn3+ to Mn4+. Higher potential plateau associated with oxidation of the substituted transition elements is also observed. These substituents also significantly alter the onset of Jahn-Teller distortions in the 3 V potential plateau. Synchrotron based in situ X-ray absorption (XAS) was used to determine the exact nature of the oxidation state changes in order to explain the overall observed capacities at different potential plateaus. The studies on LiCu0.5Mn1.5O4 show single phase behavior in the 4-5 V potential region with a good cycle life. Lower cycle life characteristic observed in cycling LiNi0.5Mn1.5O4 and LiNi0.25Cu0.25Mn1.5O4 versus Li metal are ascribed to coexistence of several phases in this potential region. However, LiCu0.5Mn1.5O4 shows onset of Jahn-Teller distortions in the 3 V potential plateau, in contrast to LiNi0.5Mn1.5O4 and LiNi0.25Cu0.25Mn1.5O4 cathode materials. 相似文献
59.
A. A. Bukaemskii N. A. Sosedov L. S. Tarasova 《Combustion, Explosion, and Shock Waves》2005,41(1):97-105
A method is proposed to study the sequence of phase transitions in powdered materials under a shock-wave action. It is shown that the aluminum hydroxide-alumina system has the following sequence of phase transformations under a shock-wave action: bayerite boehmite -Al2O3 -Al2O3. It is found that there are no transitional high-temperature modifications of alumina. A method is developed for obtaining a submicron alumina powder, which allows obtaining materials with a controlled phase composition, including a thermodynamically stable -modification of Al2O3. The specific features of the morphological structure and the phase and structural characteristics of powders after a shock-wave action are considered.Translated from Fizika Goreniya i Vzryva, Vol. 41, No. 1, pp. 110–119, January–February, 2005. 相似文献
60.
《Expert systems with applications》2014,41(6):2957-2963
In this paper, we consider interactive fuzzy programming for multi-level 0–1 programming problems involving random variable coefficients both in objective functions and constraints. Following the probability maximization model together with the concept of chance constraints, the formulated stochastic multi-level 0–1 programming problems are transformed into deterministic ones. Taking into account vagueness of judgments of the decision makers, we present interactive fuzzy programming. In the proposed interactive method, after determining the fuzzy goals of the decision makers at all levels, a satisfactory solution is derived efficiently by updating satisfactory levels of the decision makers with considerations of overall satisfactory balance among all levels. For solving the transformed deterministic problems efficiently, we also introduce novel tabu search for general 0–1 programming problems. A numerical example for a three-level 0–1 programming problem is provided to illustrate the proposed method. 相似文献