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41.
机械合金化Fe-Ni粉末的相结构 总被引:1,自引:0,他引:1
使用XRD和Moessbauer等方法,研究了在Ar气氛下机械合金化Fe—Ni粉末相结构的变化.结果表明,在机械合金化Fe64-Ni36粉末过程中,fcc相的数量随着球磨时间的增加先增加然后减少,与加乙醇球磨Fe64-Ni36的情形相同.当Ni的含量(原子分数)大于50%时,有fcc相、顺磁相和FeNi3形成,当Ni的含量低于50%时,bcc相的数量随着Ni含量减少而增加.Moessbauer谱的结果表明,因球磨时间或Fe、Ni比例的不同,Fe—Ni球磨粉末固溶体具有不同结构的原子配比。 相似文献
42.
43.
O. A. Lambri J. I. Prez-Landazbal J. A. Cano V. Recarte 《Materials Science and Engineering: A》2004,370(1-2):459-463
Mechanical spectroscopy, neutron diffraction and differential scanning calorimetry (DSC) were performed on commercial Fe–6 wt.% Si alloy after quenching from high temperature. The damping spectrum shows a peak at around 800 K and an associated modulus defect. The modulus shows an increase during the second and subsequent heating runs. In addition, an anomaly in the modulus behavior has been found at around 400 K. Different thermal treatments allows to obtain two different recovery degrees of the quenched-in defects. The influence of the recovery degree on the 800 K internal friction peak and on the anelastic modulus has been evaluated and confirm the validity of the grain boundary mechanism associated to this peak. Experimental results are discussed on the basis of recovery and ordering processes. 相似文献
44.
M. Kaiarov E. Rudnayov J. Koval
ík J. Dusza M. Hnatko P. ajgalík A. Merstallinger 《Materialwissenschaft und Werkstofftechnik》2003,34(4):338-342
In the presented work some properties of a recently developed Si3N4/SiC micro/nanocomposite have been investigated. The material was tested using a pin on disc configuration. Under unlubricated sliding conditions using Si3N4 pin at 50 % humidity, the friction coefficient was in the range of 0,6 ‐ 0,7. The reduction of humidity resulted in a lower coefficient of friction, in vacuum the coefficient of friction had a value of about 0,6. The wear resistance in vacuum was significantly lower then that in air. The wear patterns on the Si3N4+SiC disc revealed that mechanical fracture was the wear controlling mechanism. Creep tests were realized in four point bending configuration in the temperature interval 1200‐1400 °C at stresses 50,100 and 150 MPa and the minimal creep deformation rate was established for each stress level. The activation energy, established from the minimal creep deformation had a value of about 360 kJ/mol and the stress exponent values were in the range of 0.8‐1.28. From the achieved stress exponents it can be assumed that under the studied load/temperature conditions the diffusion creep was the most probable creep controlling mechanism. 相似文献
45.
Finite element analysis of the hip implant is conducted in this paper for representative femoral cross-section geometries and development of stress in the presence of bone cement is elucidated. Differences in cement stresses generated by varying implant cross-sections were compared with conventional features derived from representative implants. The analysis was performed under idealized implant assemblies by constraining the implant movement in the assembly. The cross-sections and implant geometries used are generic and intended to be representative of available geometries. This paper is a part of student research projects, prepared from a series of activities in biomedical implant research currently underway at Ohio Northern and Arkansas Tech Universities. 相似文献
46.
Examination of the wreckage of a light aircraft revealed that approximately 20 cm was missing from one tip of the aluminum
alloy propeller. Fractographic and metallographic examination of the remaining portion of the propeller revealed extensive
grain-boundary separation in the vicinity of the fracture, and grain edges and corners rounded by corrosion on the fracture
surface. Energy dispersive X-ray analysis (EDXA) revealed fluorine on, and in the vicinity of, the fracture surface. In the
ensuing litigation, it was asserted that the crash occurred because the propeller fractured in flight as the result of intergranular
attack caused by the use of a fluorine-bearing cleaner. 相似文献
47.
48.
对铜在酸性CuCl_2溶液中蚀刻反应机理论述,利用氧化-还原电动势原理,详细论述了Ni80Cr20合金在酸性CuCl_2溶液中化学蚀刻反应机理,以及影响蚀刻速度的因素,并对溶液中金属离子的存在形式作了验证。 相似文献
49.
采用ZG31Mn2Si替代ZGMn13生产拖拉机和推土机履带板.改进铸造工艺,可以生产出合格的铸件;经淬火、低温退火处理,其基体组织为马氏体,属强韧性钢种,能够切削加工. 相似文献
50.
基于甲基异丁基甲酮于稀盐酸介质中定量地萃取Zn ̄(2+)与CNS ̄-形成的络阴离子。从而达到与共存的锰、镍、铝、铬的完全分离。在有氟化物、硫脲存在时Fe ̄(3+)、Cn ̄(2+)和Ag ̄+也不被萃取。有机相中的锌于PH5.5“六胺”缓冲介质中返萃取回水相,用EDTA滴定。在文中给定的条件下锌的一次被萃取率可达99%以上,成功地解决了锰铜基高阻尼合金中共存离子对锌量测定的干扰问题。 相似文献