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91.
K38G合金及其溅射微晶层的高温氧化 总被引:3,自引:0,他引:3
研究了K38G铸造镍基高温合金及其用平面磁控离广溅射工艺制备的微晶涂层在800-1000℃500小时内的抗高温氧化性。结果表明,微晶化极大改善合金的抗氧化能力,并改变合金表面生成的氧化物类型,由Cr_2O_3变为α-Al_2O_3。还讨论了铸态K38G合金及溅射微晶层的氧化机理。 相似文献
92.
The oxidation behavior of a single-crystal (SC) Ni-base superalloy was studied over the temperature range from 1000–1150°C and analysed by TGA, XRD, EDAX, and SEM. The results indicated that the SC Ni-base superalloy exhibited parabolic oxidation kinetics, which were controlled by the growth of the inner -Al2O3 layer. A mixed scale formed on the SC Ni-base superalloy after prolonged oxidation. The scale consisted of an outer layer of spinel, a sublayer of mainly -Al2O3 with small amount of spinel adjoined by a very thin and even discontinuous layer of CrTaO4-rich oxide, and an inner -Al2O3 layer. The inner -Al2O3 layer provided good protection. No internal oxides or nitrides were observed below the inner -Al2O3 layer after 1000 hr at 1000°C, and after 200 hr at 1100 and 1150°C. 相似文献
93.
预压缩单晶镍基合金的组织结构及在拉伸蠕变期间的粗化特征 总被引:1,自引:1,他引:1
对[001]取向单晶镍基合金进行压应力处理,获P-型筏状结构后,对其进行拉伸蠕变性能测试及SEM形貌观察,研究了P-型筏状结构的粗化特征及影响因素。结果表明:由于应力场的差别,样品不同位置筏状γ'相粗化程度及特征不同,近断口处筏状γ'相扭曲且粗化程度加剧,随离断口距离增加,γ'相粗化程度减弱。有限元分析认为:外加载荷改变了水平和垂直γ基体通道中的错配应力分布,并使立方γ'相不同界面晶格发生挤压或扩张应变,这可以促进元素的互扩散和γ'相的定向生长,是形成P-型筏状组织的主要原因。在高温及拉应力作用下,P-型γ'相端部沿垂直于应力轴方向优先生长和相互横向连接,并进一步形成折叠的层状组织。 相似文献
94.
The oxidation behavior in air at 1473 K, and sulfidation behavior in a H2S–H2 gas mixture with a sulfur partial pressure of 10–2 Pa at 973 K of Al–Re coated CMSX-4 were studied. Investigation on the sulfidation behavior of the Re-coated CMSX-4 was carried out in a H2S–H2 gas mixture with a sulfur partial pressure of 10–2 Pa at 973 K. The experimental results show that a Re-rich alloy layer was formed between an -Al2O3 layer and the inner concentration zone of Ta and Ti for the CMSX-4 single crystal alloy with an Al–Re coating after oxidation. The Re-rich alloy layer containing Cr, W, Ni, Co, and Mo effectively inhibited the outward diffusion of alloying elements and the inward diffusion of Al. The Al/Re-coated CMSX-4 single crystal alloy had excellent sulfidation resistance; the Re-rich alloy layer, containing W, Ti, Ta, and Mo, which formed during the sulfidation process and located between the alumina scale and the CMSX-4 base alloy, plays a role in inhibiting the outward diffusion of alloying elements. The sulfidation resistance of CMSX-4 single-crystal alloy is greatly improved by a Re coating on the CMSX-4 alloy surface; this is attributed to a Re–Cr–W alloy layer that retarded the outward diffusion of cations and the oxide layer containing Ta, Ti, and Al, which inhibited the inward penetration of sulfur. 相似文献
95.
The superplastic formability of SP- lnconel 718 superalloy was evaluated using the argon blowing method. Relationships among
superplastic forming parameters (forming temperature, argon pressure, and forming time) and specific dome height (dome height/workpiece
diameter) were investigated, as were changes in material properties after superplastic forming. Experimental results showed
the optimum forming temperature range for SP- lnconel 718 to be between 975 and 995 °C. During the superplastic forming process,
5- phase precipitates formed at grain boundaries and limited the grain growth, which is considered beneficial for superplastic
deformation. On the other hand, increasing the forming deformation also increased the formation of cavities, which can be
attributed to the existence of niobium- rich inclusions. This degraded the superplasticity of the superalloy. Electrochemical
tests showed that the corrosion resistance of SP- lnconel 718 after superplastic forming worsened because of the existence
of both S- phase precipitates and niobium- rich inclusions. 相似文献
96.
97.
H. Mughrabi H. Biermann T. Ungar 《Journal of Materials Engineering and Performance》1993,2(4):557-564
The γ-γ lattice mismatch of specimens of the monocrystalline nickel-base superalloy SRR 99 has been measured by a high-resolution
X-ray diffraction technique for the undeformed state and after high-tem-perature creep deformation. During creep deformation
beyond the minimum creep rate (total strain =0.5%), the lattice mismatches, measured in and perpendicular to the [001] stress
axis, respectively, un-dergo changes in opposite directions. This reflects the buildup of a complex deformation-induced triaxial
state of internal stress in the phases y and γ. The overall resolved shear stresses that act in γ and y due to the combined
action of the external and internal stresses are estimated, and the conditions under which cutting of the γ phase by dislocations
should occur are discussed. 相似文献
98.
Jung-Chel Chang Cheol Choi Jae-Chul Kim Young-Hoon Yun 《Journal of Materials Engineering and Performance》2003,12(4):420-425
Effects of the hot-isostatic pressing (HIP) process on microstructures and mechanical properties of Ni-base single crystal
superalloy CMSX-4 were investigated. In the overall heat treatment process, the HIP treatment remarkably induced the healing
behavior of micropores and decreased the pore size and porosity of superalloy CMSX-4 compared with normally treated specimens.
The microstructure of γ′ phase after the HIP process showed rather a coarsening tendency and could be developed by the partially solution and aging
treatment. Consequently, the elimination of cast micropores using the HIP step resulted in the inhibition of crack initiation
in microstructure and improved the stress-rupture lives of Ni-base single crystal superalloy by 185%. 相似文献
99.
根据已知镍基合金成分和γ′相成分,运用分层宽容多目标优化法,分别计算了γ相成分及γ′相含量.优化测算过程的实现是通过建立使杠杆定律等式两端数值差最小和两相共格错配度最小的目标函数,并通过设置γ′相含量和基体相成分取值范围的约束条件而实现的.验证了该方法的可行性和准确性. 相似文献
100.
IntroductionSLlperalloyandheat-resistingsteelarenowwidelyusedasstructurematerialsinaerospace,a\-lationalldshipbuildingindustries.Nickel-basesuperalloywasfirstlyrevealedasanengineeringmaterialduringtheearly1960swhenitwasrecognizedasbeingsuitableforllledium-temperaturegasturbinel'l.Now.nickel-basesuperalloyhasbeenpracticallyusedinhigheffectiveturbinestosatisfytheincreasingdemandsforhighertemperatureenvironmentsIZI.Insomeaerospaceengines,theimpellersshouldserveattemperatureof1000C~1100C,andala… 相似文献