On the magnetic ordering of R6Fe13X compounds

Neutron diffraction performed on Pr₆Fe₁₃Ag and Pr₆Fe₁₃Au powder samples reveals a collinear antiferromagnetic ordering of the four Fe and the two Pr sublattices associated with the wave vector q=(001) (I_P magnetic lattice with anticentering translation). The moments of all sublattices located at (xy0) layers, sandwiched between successive X layers perpendicular to z at z=−0.25, 0.25, are confined to the same direction within the (xy0) plane. They change their direction collectively when going to the next Ag(Au) layers at z=0.25, 0.75. The Pr moments at 1.5 K are 2.5(2)μ_B and 2.6(1)μ_B/Pr atom, while the average Fe ordered value is 2.2μ_B/Fe atom, in agreement with Mössbauer results. Detailed results are presented for Pr₆Fe₁₃Ag.     

不锈钢精密薄壁件外表面磁力研磨工艺研究

磁性研磨是一种利用磁场中的磁性磨料,对具有相对运动的工件表面进行光整加工的新技术。选择铝、镍、钴磁粉作为磁性磨料时,对奥氏体不锈钢精密薄壁件外表面具有良好的研磨作用。     

Effect of hard-disk drive spindle motor vibration on dynamic microwaviness and flying-height modulation

In order to achieve higher recording densities up to 1 Terabit per square inch using conventional magnetic recording technologies, the recording slider will need to be physically spaced very close to the rotating disk, possibly via the use of an air-bearing surface. However, as the recording slider is flying at such ultra-low spacing of few nanometers over a high-speed rotating disk, it is experiencing disturbances from various different sources and of a wide frequency range. These disturbances may cause the recording slider to vibrate significantly, a condition known as flying-height modulation (FHM), which may result in data loss and possibly head–disk interface failure. A significant source of slider excitation is due to low frequency surface topographical features of the rotating disk, termed dynamic microwaviness. Dynamic microwaviness is a dynamic property of the disk and differs from regular topographical microwaviness, which is a static property. Most research works on dynamic microwaviness and FHM have been focused at the component level, using somewhat idealized conditions, such as high performance air-spindle motors that exhibit very low vibration amplitudes. In this paper, actual hard-disk drive spindle motors are used to investigate the effect of spindle motor vibration on dynamic microwaviness and FHM. It is found that there is a clear connection between spindle motor vibration and dynamic microwaviness that affects FHM.     

Ti(CN)基金属陶瓷微观组织的研究

用X－射线，电子探针及磁性测量等手段对Ti（CN）基金属陶瓷切削刀具的显微组织进行了系统分析，以瑞典山特维克同类刀具与国产刀具进行对比，发现国产刀具中Co-Ni粘结相中出现了无磁性的Ni3TiC相，从而降低了材料的磁饱和、矫顽磁力及抗弯强度。Ni3TiC的出现与烧结气氛有关，是烧结时材料脱碳的结果。文章对材料中的硬质相、粘结相等进行了微区成份定量分析，确认了各元素的分配状况。对于轻元素氮的分市则采用了X－射线波谱仪对刀具断面进行扫描，发现与国外名牌产品相比，国产刀具中氮的分布欠均匀。     

Quaternized magnetic microspheres for the efficient removal of reactive dyes

In this paper, a novel quaternized magnetic resin, NDMP, was prepared and characterized. Two reactive dyes (RDs), Orange G (OG) and red RWO, were used as a small-molecular RD and large-molecular RD, respectively, to investigate their adsorption on NDMP. A common quaternized magnetic resin, MIEX, was selected for comparison. The adsorption kinetics of OG onto both resins and the adsorption kinetics of RWO onto NDMP followed pseudo-second-order kinetics, whereas the adsorption of RWO onto MIEX was better fitted by pseudo-first-order kinetics. The experimental data illustrated that the equilibrium adsorption amount of both RDs onto NDMP (1.9 mmol OG/g, 0.70 mmol RWO/g) was twice as large as that on MIEX (1.0 mmol OG/g, 0.35 mmol RWO/g). The Langmuir equation and the Freundlich model fit the isotherm data for OG and RWO adsorption, respectively. The adsorption of OG on the NDMP and MIEX resins declined in the presence of NaCl or Na₂SO₄. The effects of the salts on the adsorption of RWO were different. The recyclability of NDMP and MIEX were also evaluated. This work provides a reusable efficient adsorbent for the removal of RDs.     

Bench-scale testing of a magnetic ion exchange resin for removal of disinfection by-product precursors

The objective of this research was to compare enhanced coagulation with anion exchange for removal of disinfection by-product (DBP) precursors (i.e. natural organic matter (NOM) and bromide). Treatment with a magnetic ion exchange resin (MIEX((R))) was the primary focus of this study. Raw waters from four utilities in California were evaluated. The waters had low turbidity, low to moderate organic carbon concentrations, a wide range of alkalinities, and moderate to high bromide ion concentrations. The treated waters were compared based on removal of ultraviolet (UV) absorbance, dissolved organic carbon (DOC), trihalomethane formation potential (THMFP), and haloacetic acid formation potential (HAAFP). The results indicated that treatment with MIEX is more effective than coagulation at removing UV-absorbing substances and DOC. Treatment with MIEX and treatment with MIEX followed by coagulation yielded similar results, suggesting that coagulation of MIEX-treated water does not provide additional removal of organic carbon. MIEX treatment reduced the THMFP and HAAFP in all waters, and did so to a greater extent than coagulation. Treatment with MIEX was most effective in raw waters having a high specific UV absorbance and a low anionic strength. Following MIEX treatment, subsequent chlorination resulted in a shift to the more brominated THM and HAA species as compared to chlorination of the raw water. MIEX also removed bromide to varying degrees, depending on the raw water alkalinity and initial bromide ion concentration.     

Magnetic field detection for current evaluation by magnetic force microscopy

A current measurement method through magnetic field detection by magnetic force microscopy was proposed and demonstrated. We observed the magnetic field induced by an AC below 2.2 μA around a GaAs/AlGaAs mesa stripe. To achieve high sensitivity in magnetic field detection, we tuned the AC bias frequency to the torsional resonant frequency of the cantilever. As a result, the sensitivity of the magnetic field detection was much improved and specific features of the magnetic field around the mesa stripe were clearly observed at a current in sub-μA range.     

油管缺陷在线检测仪的研究

文中研究了油管局部缺陷和壁厚减薄缺陷的漏磁场检测原理。研制了一种新型的井口式油管缺陷检测仪,缺陷检测传感器的组合式探头具有自动张合、浮动和随动功能,能够满足油管在线检测对检测传感器的要求。仪器可用在井口对油管进行在线连续定量检测,检测结果不受管表面的油泥或其它非导磁性材料的影响。测试表明,该仪器具有精度和分辨率高,结构简单,安装方便,性能可靠等优点。     

电化学磁粒光整加工实验

从电化学磁粒光整加工对材料去除量和表面粗糙度影响规律的实验结果表明,由于磁粒加工过程中不断地去除钝化膜,使表面露出的新基体,从而进一步加速了电化学过程,实现表面整平,磁粒光整加工和电化学过程的复合,使光整加工效率和表面质量得到提高。     

Investigations of nano- and macro-wear of magnetic tape head materials

The nano- and macro-wear characteristics of calcium titanate, single crystal ferrite and polycrystalline ferrite were investigated using nano-scratch testing and wear bar testing. Nano- and micro-indentations were made to determine nano- and micro-hardness, and nano-scratch testing was used to evaluate relative wear rates on the nano-scale. The macro-wear characteristics of the various head materials against metal particle tapes was investigated as a function of tape speed using wear bars mounted in a DLT tape drive. The micro-indentation method was used to investigate wear of the head/tape interface in a linear tape drive. The results from nano- and macro-wear tests were analysed and correlated with the microstructure of the materials.