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61.
Microwave plasma synthesis of TiN and ZrN nanopowders 总被引:2,自引:0,他引:2
This work demonstrates that TiN and ZrN nanopowders can be prepared by microwave plasma synthesis method. The effects of flow rate of plasma forming gas, flow rate of carrier gas and feeding rate of precursor raw material to the average particle size were studied. The TiN and ZrN nanopowders were characterized by means of transmission electron microscopy (TEM) and X-ray diffraction (XRD). 相似文献
62.
Two-phase (B2+L12) nickel aluminide intermetallic compounds were synthesized by the pressure-assisted volume combustion synthesis (CS). The production and characterization of the samples containing NiAl+Ni3Al were investigated. Aluminum (99% pure, 15 μm) and carbonyl nickel (99.8 pure, 4-7 μm) powders were used. The production of intermetallic compound was carried out at 1050 °C under 150 MPa uniaxial pressure in open air atmosphere in an electrical resistance furnace for 60 min. The formation temperature of intermetallic compound was determined by differential scanning calorimeter (DSC) analysis, and exothermic temperature of powder mixture was determined as 653 °C. The characterization of samples was confirmed by optical microscope, SEM and XRD analysis. It was observed that the structure of compound has very low porosity and the formation of NiAl was completed successfully. The relative density of test materials measured according to Archimedes’ principle was 98.04%. The microhardness of test materials was about 351 HVN1. 相似文献
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Despite its energetic interest, the use of microwaves for the thawing or temperage of food products presents a major drawback called thermal runaway. This is mainly due to the important gap between the dielectric properties of water in solid and liquid phases. A monitoring approach of the temperatures inside a foodstuff during microwave defrosting is therefore proposed to, in a first step, detect the critical phenomena of thermal runaway, and, in further work, to control it. An observer allowing to estimate the internal temperatures from the temperature of the surface has been developed. An Extended Kalman Filter, because of its simplicity of design, has been chosen, but this choice is not exclusive. The heat transfer with phase change and microwave effects is represented by a nonlinear distributed parameters system, and the observer is based on a standard finite volume scheme. The approach is experimentally carried out and validated during the defrosting of a block of tylose. 相似文献
66.
En-Hai Sun Yong-Ho Choa Tohru Sekino Tomohiko Adachi Koichi Niihara 《Materials Research Innovations》2002,6(3):105-111
Cordierite/ZrO2 composites with 5 to 25 wt% ZrO2 were fabricated by conventional powder mixing and pressureless sintering method. Their densification behavior, microstructure,
mechanical and thermal properties were studied. By dispersing 25 wt% (9.57 vol%) ZrO2, densified cordierite/ZrO2 composite with a relative density of 98.5% was obtained at an optimum sintering condition of 1440 °C and 2 h. ZrO2 particles were homogenously dispersed within matrix grains and at the grain boundaries. The intragranular particles were
finer than 100 nm and the intergranular particles were coarser. Both fracture strength and toughness could be enhanced more
than two times higher, compare to those of monolithic cordierite, by dispersing 25 wt% ZrO2 into the cordierite matrix. The toughening mechanism in the present composites was mainly attributed to martensitic transformation
due to ZrO2 dispersion.
Electronic Publication 相似文献
67.
GaN材料系列的研究进展 总被引:3,自引:0,他引:3
GaN及其合金作为第三代半导体材料具有一系列优异的物理和化学性质,在光电子器件,高温大功率电子器件及高频微波器件应用方面具有广阔的前景,已成为当前高科技领域的研究重点,论述了这种材料的研究历史与发展现状,物理与化学性质,薄膜的生长方法及在光学电子和微电子器件应用于方面的研究进展。 相似文献
68.
微波介质谐振器介电参数的测量 总被引:6,自引:0,他引:6
本文讨论了微波介质谐振器介电参数测试技术。用研制的测试装置对多个介质样品进行了实测,结果表明,本文的分析与实际值是吻合的。该测试技术可对微波介质谐振器的复介电常数进行迅速、准确、可靠、宽频带、无损伤、自动化和批量检测,具有较强的实用性。 相似文献
69.
王福臣 《固体电子学研究与进展》1992,(4)
对WC76型S频段大功率振荡用砷化镓场效应晶体管的微波性能作了介绍。文中给出了测试振荡器的设计。测试结果表明,WC76型振荡管在s频段的微波性能良好,振荡频率在3GHz左右时,输出功率可达3.5w,直流—射频转换效率可达44%,而且在2~4GHz的整个S频段均能满意地工作。 相似文献
70.