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41.
An oxide ceramic process was adopted to prepare high frequency manganese-zinc (MnZn) power ferrite. In combination with the microstructure analysis of material, the influences of sintering process on initial permeability (μi) and high frequency loss in unit volume (Pcv) of MnZn power ferrite were investigated. The results show that in order to obtain fine microstructure and high frequency properties, the preferable sintering temperature and atmosphere are 1230 ℃ and oxygen partial pressure ( PO2) of 4%, respectively. 相似文献
42.
Study on sintering process and characteristic of nanosized soft magnetic MnZn ferrite powders 总被引:1,自引:0,他引:1
The effect of sintering process (especially the sintering temperature) on the magnetic property and microstructure of sintered sample of nanosized soft magnetic MnZn ferrite powder was investigated. The sintered sample of MnZn ferrite was prepared by both traditional pressing and cool isostatic pressing on MnZn ferrite nanoparticals. The sintering process of which was segmented. Thedensity, microstructure and phase composition of sintered sample were analyzed by Archimedes'law, scanning electron microscopy (SEM) and X-ray diffraction (XRD). The grain growth and densification in sintering process of MnZn ferrite were investigated. The magnetic property was measured by vibrating sample magnetometer (VSM) and Nim2000 magnetic material testing system. The results show that the better sintering temperature is 850 ℃, at which the better magnetic property and microstructure of sintered compact were obtained. 相似文献
43.
The effects of NiO on microstructure and magnetic properties of Mn-Zn ferrite with a nominal composition of Zn0.32Mn0.60-xNixFe2.08O4 were investigated. The calcined powder of Mn-Zn ferrite was characterized by X-ray diffraction (XRD), the fracture surface of Mn-Zn ferrite was checked by scanning electronic microscope (SEM), and then the magnetic properties were measured. As a result, the substitution of Ni can cause the crystallattice constant of MnZn ferrite to decline, and the grain size to decrease, therefore improve the magnetic performance of MnZn ferrite whose density exceeds 5.0 g·cm-3. 相似文献
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Ferrous ion was transformed into feroxyhyte (δ-FeOOH) by oxidation. Then, manganese sulfate and zinc sulfate in some ratio were added to the feroxyhyte solution. The co-precipitation was boiling reflux conditions sometime under constant stirring. The nanosize MnZn ferrite powder was formed. The mechanism of preparation of the nanosize MnZn ferrite was discussed, and the formation of feroxyhyte which was playing a key role during the process was mentioned. The properties of powder was tested by means of X-ray diffraction, transmission electron microscopy and vibrating sample magnetometer. The results show that the samples of spherical particles about 20 nm, which have characteristics of ferrimagnetism, has larger saturation magnetization, but the remanent magnetization and coercivity are comparatively smaller. The spinel MnZn ferrite nanosize powder was successfully prepared from δ-FeOOH at low temperature, with low-carbon steel and peroxide as main material. 相似文献
46.
ZnFe2O4高温煤气脱硫剂的再生 总被引:1,自引:0,他引:1
在热天平上对自制的ZnFe2O4脱硫剂进行了再生工艺研究,考察了再生温度、O2浓度对ZnFe2O4脱硫剂再生性能的影响;进行了多次硫化、再生循环实验,并与加入玻璃粉的样品进行了比较。结果表明,700℃下氧含量2.0%(vol)时再生可以获得良好的再生率和二次硫化反应活性;玻璃粉的少量加入,会改善脱硫剂长期使用的稳定性,但反应活性有所下降。 相似文献
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Preparation of zinc ferrite in the presence of carbon material and its application to hot-gas cleaning 总被引:3,自引:0,他引:3
In order to develop an efficient absorbent of H2S in coal gasification, zinc ferrite (ZnFe2O4) was prepared in the presence of carbon materials such as activated carbon (AC), activated carbon fiber (ACF), and Yallourn coal (YL). The absorption behavior of absorbents for H2S was examined using a fixed-bed flow type reactor equipped with a quadrupole mass spectrometer.Carbon material-supported ZnFe2O4 exhibited larger desulfurization capacity for H2S than unsupported ferrites. They could efficiently remove H2S from 4000 ppm levels in a simulated coal gasification gas to less than 1 ppm at 500 °C. The absorption capacity of H2S with ZnFe2O4/AC, ZnFe2O4/ACF, and ZnFe2O4/YL exhibited nearly 100% of stoichiometric amount of loaded metal species. They could be regenerated by an air oxidation in O2-Ar (50 vol%) at 450 °C for 30 min. The regenerated ferrite can be used for repeated absorption of H2S with a very slight decrease in the absorption capacity. 相似文献
50.
通过加入添加剂,制备了晶相单一、结晶度完好、具有较好磁性能的锰锌铁氧体纳米晶,然后研究添加剂对铁氧体晶相、磁性能和居里温度的影响.研究结果表明:添加剂可以使晶体生长更完善,晶粒变大;同时可以改善样品的磁性能,降低居里温度. 相似文献