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We investigated the impact of silica nanoparticles on the complex shear moduli and molecular dynamics of elastomeric nano-composites formed from ethylene propylene diene monomer (EPDM) and polypropylene (PP). The blended system was composed of immiscible amorphous/semi-crystalline polymers. The complex shear moduli of the EPDM/PP/SiO2 nano-composites and their corresponding neat filler blends were measured at different shear rates in the temperature window ? 95–50 °C. The impacts of filler on the stress–strain and thermal behaviors were also investigated. The nano-composites exhibited higher shear moduli than the corresponding neat polymer blends. This trend was linked to the hindered glass-relaxation dynamics of the EPDM polymer in the nano-composites. 相似文献
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插层法制备聚合物/粘土纳米复合材料的原理 总被引:8,自引:2,他引:8
介绍了聚合物/粘土纳米复合材料的插层方法、制备原理和工艺过程,探讨了纳米复合材料微观结构的影响因素,概述了聚合物/粘土纳米复合材料的形成机理。 相似文献
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《Ceramics International》2015,41(7):8748-8754
Y-type hexa-ferrite Sr1.8Sm0.2Co2Ni1.50Fe10.50O22 was synthesized via micro-emulsion route. Ferrite/PST composites were obtained by mixing the different ferrite ratio in the pure PST matrix. The microstructure was examined by scanning electron microscopy (SEM) and exhibited heterogonous distribution of grains. A keen observation of these SEM images revealed that the grain morphology changes noticeably with increasing ferrite filler contents. The electrical modulus, Cole–Cole plots and quality factor of ferrite polymer composites have been investigated in the frequency range (1 MHz to 3 GHz). The field dependent magnetic properties of the prepared samples were investigated at room temperature by using vibrating sample magnetometer (VSM). The shape of hysteresis loops and linearity of Ms, Mr, Hc values vs. ferrite contents unfold that the ferrite nanoparticles are evenly dispersed within the composite. The occurrence of resonance at high frequency suggests that the present investigated composite samples are best candidate for multilayer chip inductors. 相似文献
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Amanda S. Wu Anthony M. Coppola Matthew J. Sinnott Tsu-Wei Chou Erik T. Thostenson Joon-Hyung Byun Byung-Sun Kim 《Composites Science and Technology》2012
With the rise of composite materials as replacements for traditional monolithic materials comes an increase in demand for multifunctionality. Prior studies have demonstrated the ability of an embedded, electrically percolating carbon nanotube network to respond electrically to the onset and progression of damage in composite structures. We build upon this work by incorporating healing functionality into braided composites through the use of a hollow channel resin delivery system. This study demonstrates the ability of a carbon nanotube network to sense crack filling during resin injection, thus providing the scientific basis required for sensing healing in advanced composites. With practical application in mind, a two-part healant system is employed in this study. Two methods for qualitatively assessing healing are employed and compared; these include elastic modulus/strain energy recovery and FTIR spectroscopy. 相似文献
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Shaghayegh Pezeshkpour Babak Salamatinia Bahman Amini Horri 《Ceramics International》2018,44(3):3201-3210
In this study, nanocrystalline nickel oxide gadolinium-doped ceria (NiO-GDC) powder was synthesized in-situ using Na-Alginate as the template via ionic sol-gel technique. The effects of calcination time and temperature on the particle size and the physiochemical properties of nanocrystalline NiO-GDC are presented in this paper. Using this method, gel beads were formed by contacting sodium alginate solution as the gelling template and metal (gadolinium/cerium/Ni) nitrates as the precursor. The obtained nanocrystallites were characterized using Field Emission Scanning Electron Microscopy, powder X-ray diffraction, energy dispersive X-ray spectroscopy, thermo gravimetric analysis, nitrogen adsorption/desorption analysis, and Fourier transform infrared spectroscopy. It was observed that the increasing calcination temperature had affected both the particle size and the surface area of the NiO-GDC, whereas the increasing calcination time had only impacted the size of the particles. The smallest mesoporous nanocrystalline NiO-GDC powder (12.1225 ± 0.005 m2/g surface area), composed of cubic GDC (5.18 nm crystallite size) and cubic NiO (7.99 nm crystallite size) were synthesized at a calcination temperature of 500 °C for 2 h. This study hopes to inspire more researches on the ionic-gelation method for synthesizing other metal nanostructures as well as other reaction parameters. 相似文献
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We developed a new electrochromic device by using compact Prussian blue (PB)/antimony tin oxide (ATO) nano-composites as anodic electrode and viologen anchoring on titanium dioxide (TiO2) nano-particles as cathodic electrode. The anodic electrode was based on a transparent nanostructured ATO nano-particle film and was electro-deposited by Prussian blue to form compact Prussian blue/ATO nano-composites by means of galvanostatic electrodeposition process. Nanocrystalline TiO2 thin films on conducting glass were modified with a mono-layer of viologen with two anchoring groups, which were much strongly adsorbed onto the surface of TiO2 nano-particles. A polymer gel electrolyte sandwiched between the anodic and cathodic layers is used as the ionic transport layer. The 2.5 cm × 2.5 cm electrochromic device shows high contrast (64.8%, at 600 nm) very low transmittance at colored stage (0.1%, at 600 nm), fast switching time (600 and 720 ms for coloration and bleaching, respectively), high coloration efficiency of 912 cm2 C−1 at 600 nm and good stability. The enhanced performance of the electrochromic device can be attributed to the ATO nano-particles as inter-conductive materials. 相似文献
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