用环境友好催化剂合成丙酸异丁酯的研究

报道了以固载杂多酸盐TiSiW12O40/TiO2为环境友好催化剂，对以丙酸和异丁醇为原料合成丙酸异丁酯的反应条件进行了研究。实验表明：TiSiW12O40/TiO2是合成丙酸异丁酯的良好催化剂，最佳反应条件为：n（醇）：n(酸）=1.2:1，催化剂用量为反应物料总质量的2.0%。反应时间1.0h，反应温度106-125℃，上述条件下，丙酸异丁酯的收率可达79.1%。     

JOINING MECHANISMS OF β''''-Al2O3 CERAMIC AND PYREX GLASS TO Al MATRIX COMPOSITE

The bonding of β'-Al2O3 and pyrex glass to Al matrix composites by anodic bonding process is achieved. The microstructure of the bonded interface and the joining mechanisms are analyzed with scanning electron microscope (SEM), energy dispersive X-ray fluorescence spectrometer (EDX). It is observed that the bonding region across the interface consists of the metal layer, oxide transitional layer and the ceramic layer, with the transitional layer composed of surface region and sub-surface region. The bonding process can mainly be categorized into anodic bonding process and solid state diffusing process. The pile-up of the ions and its drift in the interface area are the main reasons for anode oxidation and joining of the interface. The temperature, voltage and the drift ions in the ceramic or glass during the bonding process are the essential conditions to solid state diffusing and oxide bonding at the interface. The voltages, temperature, pressure as well as the surface state are the main factors that influence the anodic bonding.     

High Temperature Oxidation Behavior of La2O3-MosSi3/MoSi2 Composites

The oxidation behavior of 0. 8% La2O3- Mo5Si3/MoSi2 composites at 1200℃ in air was investigated. The results reveal that the oxidation resistance of the material with 0. 8% La2O3 and Mo5Si3 is impaired. The oxidation resistance is decreased with increasing Mo5Si3 content. The mass loss follows a linear law in the initial oxidation. With oxidation time prolonging, a continuous and dense oxidation scale prevents oxygen from diffusing increasing when and leads to mass change a Mo5Si3 content is less than 30%. However, the composite shows ＂PEST＂ with the addition of 40% Mo5Si3. With increasing Mo5Si3 content, the oxidation resistance of 0.8% La2O3- Mo5Si3/MoSi2 decreases. This attributes to the poor oxidation resistance of M05Si3 and the relative density decreasing of 0. 8% La2O3-Mo5Si3/MoSi2 composite.     

创意玩家

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Al/Fe2O3反应合成材料热力学

运用CALPHAD技术，基于多组元多相复杂平衡体系的吉布斯自由能最小化原理，用大型集成数据库F^*A^*C^*T系统，考察了铝和氧化铁经典反应体系的热力学规律。针对材料的反应合成技术，计算了化学计量铝和氧化铁体系以及各种产物中物种的相变情况；分析了原料初始温度、配料比和SiO2含量对绝热温度和平衡组成的影响。     

适合消费电子产品的电流转换逻辑技术

消费电子和通信产业正见证着I／O解决方案从并行到高速串行的转变：能够降低成本、简化设计，并具备可延展性，满足全新带宽的要求。这类接口I／O技术的市场潜力巨大，包括移动电话、DVD-RW和高清晰度LCD电视机，而低功耗、低电磁干扰(EMI)和高数据吞吐量在这些应用中极为重要。因此，业界一直致力于设计和开发这些串行I／O，以低功耗提供高速的数据速     

电磁成形技术

本文介绍了电磁成形技术原理及其在管坯胀形、管坯缩径、平板毛坯成形等方面的应用。     

一种RAID-10数据组织方式的并行文件系统及其I／O性能

Cluster已发展成为普遍用于高性能计算的一种体系结构，对于大规模并行计算，I／O仍是要解决的“瓶颈”问题。多种用于Cluster系统的并行文件系统将节点上的存储设备统一调度、管理，形成分布式磁盘阵列，以提供大容量、高性能存储系统，满足日益高涨的存储需求。