核电材料在模拟反应堆环境中应力腐蚀破裂测试技术与性能评价

简要介绍了采用慢应变速率试验，Ｕ型弯曲和Ｃ形环试验等技术，分别对８００合金，３０４和３１６及３１６Ｔｉ不锈钢Ａ５３３Ｂ压力容器用多在模拟核反应堆环境中的应力腐蚀破裂敏感性性进行的试验研究的一些主要结果；并结合电化学测试和表面膜俄歇电子能谱分析结果进行了讨论。     

Chemical leaching and magnetic properties of non-equilibrium Al(Co–Cu) powders produced by rod milling

We report upon the chemical leaching and magnetic properties of nanoscale crystalline Al_0.6(Co₂₅Cu₇₅)_0.4 alloy powders produced by rod milling. X-Ray diffractometry (XRD), transmission electron microscopy, differential scanning calorimetry, vibrating sample magnetometry, and superconducting quantum interference device magnetometry were used to characterize the as-milled and leached specimens. After 400 h of milling, only the b.c.c. phase of the intermetallic compound γ-Al_3.892Cu_6.10808 was detected by XRD. After annealing the leached specimen at 600 °C for 1 h, the nanoscale crystalline phase was transformed into the f.c.c. Cu phase, and this was accompanied by a change in the magnetic properties. The peaks of the magnetization shifted towards lower temperature with increasing external field. The temperature behavior at T_f (45 K) for direct current (d.c.) magnetic susceptibility measurements was quite different for field cooling and zero-field cooling. After cooling the leached specimen from 800 °C, magnetization increased gradually.     

由光率体求导折射率及振动方向的新方法

从光率体出发，利用坐标轴旋转，导出了光在晶体中传播时折射率及振动方向的公式。     

Distribution of properties from sampling inhomogeneous materials by line transects

A theory related to the statistics of the structure and properties of inhomogeneous materials has been proposed, dealing with the distribution of properties from sampling of inhomogeneous structures by line transects. It is demonstrated that the empirical cumulative distribution functions of the intercepts from the microstructural constituents and their variances are important fingerprints of the inhomogeneous structures.Simulated sampling of the images of the microstructure by line transects has been proposed as a powerful method for characterization the distribution of properties of inhomogeneous structures. One of the advantages of the method based on the expected values of the order statistics of the intercepts is that the probability bounds of the property are determined without prior knowledge of the functional relationship between the property and the intercepts from the structural constituents.The concept intercept variance has an important application in determining the minimum transect length that stabilizes the variation of the intercept at a low value. Additionally, the concept ‘intercept variance’ can be used for topological optimization of the microstructure regarding the risk of intercepting a large amount of the weaker constituent. Equations regarding the variance of the intercepted fraction characterizing transect lengths with a specified distribution have also been derived.     

新型高k栅介质材料研究进展

随着半导体技术的不断发展，MOSFET（metal-oxide-semiconductor field effect transistor）的特征尺寸不断缩小，栅介质等效氧化物厚度已小至nm数量级。这时电子的直接隧穿效应将非常显著，将严重影响器件的稳定性和可靠性。因此需要寻找新型高k介质材料，能够在保持和增大栅极电容的同时，使介质层仍保持足够的物理厚度来限制隧穿效应的影响。本文综述了研究高k栅介质材料的意义；MOS栅介质的要求；主要新型高k栅介质材料的最新研究动态；展望了高k介质材料今后发展的主要趋势和需要解决的问题。     

国外农用非织造布覆盖材料的应用

非织造布在现代农业生产中占有重要地位 ,非织造布作为农用覆盖材料在柑橘、草莓、茶叶、花卉、水稻和玉米育苗以及人参栽培等多方面应用较为广泛 ,本文对国外农用非织造布覆盖材料的特点、性能以及应用情况作了介绍     

The effect of doubly tapered strut morphology on the plastic yield surface of cellular materials

Although the literature on the mechanics of cellular materials is vast, there is no theoretical model to account for the effects of axial yielding of struts aligned to the applied loading direction on the plastic yield surface under multiaxial loading conditions. An anisotropic hexagonal model having tapered strut morphology is developed to show these effects on the plastic yield surface under multiaxial tensile loading condition. This model covers several types of cellular structure such as two-dimensional (2D) hexagonal and square cellular materials, and three-dimensional (3D) hexagonal and rhombic cellular materials of rod-like columnar structure. A tetrahedral element with tapered strut morphology is also used for a foam model to illustrate these effects on the yield surface under axisymmetric loading condition. Plastic collapse due to bending moment in the inclined struts is a dominant mode. However, under multiaxial tensile loading, the collapse due to axial yielding of struts parallel to the loading direction is found to be an important mode. The shape of plastic yield surface was found to depend not only on relative density but also on the strut morphology.     

碳素材料超声检测的信号处理方法

针对碳素材料超声无损检测存在信噪比较低的问题,从自相关性出发分析了典型超声检测信号的组成成分,提出了在自相关分析的基础上的小波去噪思想,探讨了自相关分析和小波分析相结合的信号处理方法。利用此方法进行实际超声信号分析效果良好。     

Facile modifications of polyimide via chloromethylation: II. Synthesis and characterization of thermocurable transparent polyimide having methylene acrylate side groups

From chloromethylated polyimide, a useful starting material for modification of aromatic polyimides, a thermocurable transparent polyimide having acrylate side groups was prepared. In the presence of 1,8‐diazabicyclo[5,4,0]undec‐7‐ene, chloromethylated polyimide was esterified with acrylic acid to synthesize poly(imide methylene acrylate). The polymer was soluble in organic solvent, which makes it possible to prepare a planar film by spin coating. The polymer film became insoluble after thermal treatment at 230 °C for 30 min. Optical transparency of the film at 400 nm (for 1 µm thickness) was higher than 98 % and not affected by further heating at 230 °C for 250 min. Adhesion properties measured by the ASTM D3359‐B method ranged from 4B to 5B. Preliminary results of planarization testing showed a high degree of planarization (DOP) value (>0.53). These properties demonstrate that poly(imide methylene acrylate) could be utilized as a thermocurable transparent material in fabricating display devices such as TFT‐LCD. Copyright © 2004 Society of Chemical Industry     

Motion and structure interpretation of an optical switch

This paper focuses on tracking, reconstruction and motion estimation of a well-defined MEMS optical switch from a microscopic view. For out-of-view reconstruction, a homography capable of transforming feature points and feature lines between a microscopic image and a CAD model of the switch is implemented. The homography between two sequential microscopic images is decomposed and factorized for motion estimation. Optical flow has also been explored to provide rough estimations of rotation centre and angle. The paper also illustrates motion parameter optimization principles to deal with uncertainty inherent in micro world. After non-linear optimization, estimation accuracy for rotation angle and rotation centre can reach 0.06° and pixel level, respectively.