Continuous formation of slurry ice by cooling water–oil emulsion in a tube

Water-silicone oil emulsion with an additive, (C₂H₅O)₃SiC₃H₆NH₂, was examined as a heat storage material. A spiral tube used as a heat exchanger was immersed in a low temperature bath and the emulsion was circulated in the tube to make ice continuously. Ice was separated from the ice–liquid suspension in an outlet tank. The amount of formed ice, the temperatures of the inlet and the outlet of the heat exchanger, and the temperatures in the tube wall were measured and the overall heat transfer coefficient and the heat flux through the tube were calculated. Experiments were carried out, varying the flow rate, the temperature of cooling brine, and the thickness of tube wall. The condition under which slurry ice was formed continuously without adhesion of ice to the cooling wall was clarified. Though decrease in the thermal resistance of the tube increased the rate of ice formation or raised the brine temperature, it narrowed the range of the flow rate and of the brine temperature in which slurry ice was formed continuously.     

取样光栅周期中等效啁啾的实验研究

在Moire取样Bragg光纤光栅（SBG）的理论基础上，首次通过用相位模板旋转和2次曝光的方法，得出了带有取样啁啾的SBG的各个Fourier级数的等效啁啾率。实验数据和理论值的误差小于9%。     

Residue curve maps for reactive distillation systems with liquid-phase splitting

A model has been developed to study the effects of chemical kinetics on the residue curve maps (RCM) for reactive distillation systems with liquid phase splitting. In the model, chemical reaction can occur in both or only one of the two liquid phases. The heating policy V/V₀=H/H₀ is applied so that the kinetic effect can be described by a single parameter, the Damköhler number Da. The effects of reaction kinetics on pseudohomogeneous and heterogeneous mixtures have been compared. The properties of their RCMs are the same outside, but are fully different inside the liquid-liquid (L-L) region if they have different chemical equilibrium curves. Inside the L-L region, the chemical equilibrium curve coincides to a unique reactive liquid-liquid tie line in case that the pseudohomogeneous chemical equilibrium curve intersects with the L-L envelope. When the reaction occurs in only one of the two liquid phases, the residue curves inside the L-L region are strongly affected by the L-L envelope, especially at high Da. In the present paper, first an illustrative arbitrary reaction system, and then the reaction of cyclohexene with water to cyclohexanol are analysed with respect to their RCMs.     

Dissolution of phase-separated domains after a jump to a temperature in the single-phase region

Phase-separated domains prepared in the two-phase region were dissolved at a temperature in the single-phase region, and their dissolution dynamics was studied by using the time-resolved light scattering (TRLS) technique and a scanning electron microscope (SEM). The time t_ps of preparation of domains was chosen to be long enough for phase separation to proceed into the late stage. The scattered light intensity at small wavenumbers increased before it attenuated. As t_ps increased, the increase at smaller wavenumbers became more significant and the peak intensity decreased only slightly with dissolution time. The characteristic wavenumber q_m evaluated from TRLS and SEM followed the power-law relation q_mt^−0.3.     

自适应相位制中波同步广播及现场试验

在本试验中，采用智能同步广播激励器和ＣＣＴＶ传输的１ＭＨｚ标频，实现了中波同步广播同频保护率趋于０ｄＢ．并提出了自适应相位跟踪同步的概念。     

一种混沌信号去噪方法的研究

以Takens嵌入定理和影子定理为理论依据，提出一种能对混沌信号去噪的局部投影方法。该方法不需潜在动力学系统的先验知识，符合工程实用的要求。通过实验结果表明这种方法对混沌信号去噪很有效。     

精密扇形扫描稳速控制

在扇形扫描中，马达稳速的控制是通过相位补偿实现的。本文提出一种新的稳速控制方法、相位补偿控制，并介绍了相位补偿电路的设计。     

受干扰波相位测量的一种新方法

为了测量受噪声和谐波干扰的两个信号间的相位差，基于自适应带通滤波器（ABF）和测量信道交换技术，提出了一种新的测量方法。ABF采用可编程开关电容滤波器（PSCF）和锁相环，明显地抑制了噪声和谐波干扰，频率跟踪范围超过四个倍频程（0．5Hz-6kHz）。用微处理器控制4个开关来交换测量信道，可以基本上消除测量通道引入的附加相位移。两种方法结合提高了相位差的测量精度。实验说明了该测量方法的有效性，该方法也适合于被测信号为慢时变情况。     

中频数字化及数字式正交解调

本文介绍用数字式下变频法实现中频正交解调的基本原理及主要性能。     

Impurity Distribution Behavior in Caprolactam Extraction with Environmentally Benign Mixed Solvents

In a previous study a solvent mixture of heptane containing 40 mass % heptanol was selected as an alternative in the industrial extraction of caprolactam to replace benzene, toluene, or chlorinated hydrocarbons. This work reports the equilibrium distribution ratio of caprolactam and four model impurities of organic nature, namely, cyclohexanone, aniline, n‐methylcaprolactam, and cyclohexane‐carboxamide, comparing the mixed solvents with toluene as a reference. The resulting phase equilibria were interpreted using the equilibrium stage model. Based on these calculations it was found that, compared to toluene, the co‐extracted fraction of cyclohexanone and aniline was higher, that of n‐methylcaprolactam was comparable, and that of cyclohexane‐carboxamide was lower using the mixed solvent. Overall, the mixed solvent reduced the fraction of co‐extracted impurities by almost 10 %.