在役加氢反应器试验板脆化和氢损伤的测定与研究

充分利用了带主焊缝的役后试板，在国内首次开展回火脆化、氢介质下断裂韧性与疲劳扩展的研究，结果表明，加氢反应器焊缝有明显的脆化表现。同时，核查了反应器开停车升温速度和降温速度规定，以及确定了裂纹允许尺寸的参考数据，为今后安全运行提供了充分的依据。     

Pyrolysis of tertiarybutylphosphine at low pressure

The pyrolysis of tertiarybutylphosphine (TBP) has been studied in the low pressure conditions used for chemical beam epitaxy (CBE). The pyrolysis studies were carried out in low pressure reactors of two different configurations, one of which is a cracker cell designed for use in a CBE system. The reaction products were studied using a quadrupole mass spectrometer. The products observed are accounted for by a reaction mechanism involving homolysis of the parent TBP molecule to produce PH₂ and C₄H₉ radicals. These undergo subsequent reactions to form the stable products C₄H₈, PH₃ and H₂, with smaller amounts of P and P₂ being produced. The production of the sub-hydride PH₂ using this cracker cell design indicates that the use of partially cracked TBP may be a promising technique for reducing the amount of carbon incorporated into the growing epitaxial layer.     

TiB2和SiCW对Al2O3陶瓷材料高温摩擦磨损特性的影响

研究了Ａｌ２Ｏ３、Ａｌ２ｏ３／ＴｉＢ２和Ａｌ２Ｏ３／ＴｉＢ２／ＳｉＣＷ三处陶瓷材料在不同条件下的擦靡损特性。结果表明：三种陶瓷材料与硬质合金摩擦副的摩擦系数随温度温度的增加有不同的变化规律，摩擦表面的Ｘ射线衍射分析表明，摩擦系数的变化与陶瓷物膜的和结构有关，在高温下Ａｌ２Ｏ３／ＴｉＢ２陶瓷材料摩擦表面形成了具有优良的高温润性的ＴｉＯ２氧化膜，因而ＴｉＢ２的加入明显改善了Ａｌ２Ｏ３陶瓷材料 摩擦磨损     

1μm宽硅深槽刻蚀技术

介绍了硅深槽刻蚀的基本原理和影响刻蚀效果的几个主要工艺因素。提出了一种实现１μｍ宽的硅深槽刻蚀工艺途径；并给出了１μｍ宽、８μｍ深、侧壁及底部光洁的硅深槽刻蚀工艺条件。     

Volatile organo-halogen trace analysis in beverages by thin-layer headspace enrichment and electron-capture gas-chromatography

Applicability of thin-layer headspace (TLHS) procedure giving an aqueous concentrate and also classical purge and trap (PT) in off-line mode to isolate and enrich volatile organohalogen compounds in common beverages was tested. Both enrichment tech-niques were used in combination with gas chromatography – electron capture detection (GC-ECD). TLHS, combined with direct aqueous injection (DAI)-GC-ECD, proved applicable in the determination of volatile organohalogen compounds in all studied beverages, while the PT in a version with no preliminary sample pre-treatment was of limited applicability. Detection limits of the TLHS-based procedure were in the order of 1 ppt. Content of volatile organohalogen compounds in a number of beverages available on the Polish market including mineral waters, beers, juices, carbonated and non-carbonated soft drinks, etc. was determined by means of TLHS-DAI-GC-ECD.     

国际乳业的热点论题：蛋白质标准化

介绍了蛋白质的标准化这一国际乳品界正热的研究和讨论题目，综述了蛋白质标准化的必要性和世界上目前采用的方法，展望了膜技术在蛋白质标准化上的应用前景。     

流延法制作AlN陶瓷基片工艺

研究出一种用流延法制作ＡＩＮ陶瓷基片的工艺。制备出性能优良的ＡＩＮ基片。经１６５０℃，保温２ｈ无压烧结制得的基片，其热导率达１３０Ｗ／（ｍ·Ｋ）、密度为３．３４ｇ／ｃｍ￣３，表面光滑平整，瓷体结构均匀，性能达到用干压法制备的同类基片的性能。     

努力攀登科技高峰 为把石化工业建成支柱产业多做贡献

概述中国石化总公司成立以来所取得的重大科技成果。     

节理岩体的边界元模型及其应用

边界元法广泛应用于岩石力学问题的最大障碍是岩体的非均质及其包含的大量节理断层，本文采用多子域思想结合节理断层的非线性模型较好地解决了这一难题。该法在老厂锡矿的应用较好地解释了该矿采场顶板的冒落机理。     

加脂的化学柔软作用机理

加脂是软革制造过程中最重要的工序。本文建立了一个加脂过程和加脂机理的模型。在该模型中，传统的完全依赖ＰＨ值的观察被扩展，结合了加脂剂与浴液间的相互作用的性能和传送提供润滑作用的中性油组分的乳化剂的作用，并扩展了乳化剂的角色。以这种方式引入的化学柔软作用对革的强度有积极的效果，而相比效应力柔软作用会降低革的强度。