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91.
Tsutomu Takeichi Yuki Saito Tarek Agag Hiroyuki Muto Takehiro Kawauchi 《Polymer》2008,49(5):1173-1179
Two series of high-performance polymer alloys were prepared by mixing typical benzoxine monomers, 3-phenyl-3,4-dihydro-2H-1,3-benzoxazine (P-a) or 6,6-(1-methylethyliden)-bis-(3,4-dihydro-3-phenyl-2H-1,3-benzoxazine) (B-a), with a typical bismaleimide, 4,4-bismaleimidodiphenyl methane by various ratios followed by thermal treatment up to 240 °C. DSC and IR of the alloys were examined to follow the curing reaction. These analyses showed that the obtained polymer alloys are AB co-cross-linked polymer networks through the formation of ether linkage between the hydroxyl group of polybenoxazine and the double bond of bismaleimide. Viscoelastic analysis and softening temperature measurement revealed that the polymer alloys have much higher glass transition temperatures than those of each homopolymer. The thermal stability also increased with the increase of bismaleimide content as evidenced by TGA. 相似文献
92.
本文将介绍三种不同成分的低合金钢粉。在混入2 0%铜和不同石墨含量的条件下,对该三种粉进行了试验评定。试件的密度为6 9g/cm3,在氮氢混合气氛中于1120℃下烧结25min,在炉内冷却带650~400℃温区的冷却速度为0 4或1 5℃/s条件下,对烧结态和回火后试件的力学性能进行了测试。回火条件为200℃下保温60min。在一定的冷却速率和碳含量条件下,各种钢粉烧结后的硬度可高达40HRC。回火后,硬度仍可以保持在30HRC以上。 相似文献
93.
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95.
Some batches of detonator housings made up of Chromium plated Zn–Al alloy were found in an extensively cracked condition after few months of storage at room temperature. An analysis of the failure showed that the cracks were due to intergranular corrosion facilitated by segregation of lead at the grain boundaries. Improper chromium plating further aggravated the corrosion problem. This failure case emphasises the need for strict control of chemical composition for components made from Zn–Al alloy and the process of Cr plating of the components. 相似文献
96.
对不同温度及不同搅拌工艺下得到的材料的显微组织的比较,确定了合理的半固态温度和搅拌工艺,即半固态温度为590℃,震荡电流为500A。随后对单个线圈电磁搅拌过程进行建模及电磁场和流速场的耦合模拟得到了电磁场和流速场分布,此结果与电磁搅拌的原理及实验结果相一致。计算出在该温度和工艺下熔体内部的平均流动速度为3.2cm/s,将该结果作为能否得到半固态浆料的判据。 相似文献
97.
Synthesis and characterization of acidic properties of Al-SBA-15 materials with varying Si/Al ratios
G. Muthu Kumaran Shelu Garg Kapil Soni Manoj Kumar J.K. Gupta L.D. Sharma K.S. Rama Rao G. Murali Dhar 《Microporous and mesoporous materials》2008,114(1-3):103-109
Al-SBA-15 of varying Si/Al ratios in the range 11.4–78.4 was synthesized using tri-block copolymer P123. The calcined materials were examined by XRD, pore size distribution, surface area, 27Al NMR spectroscopy. The acidity and acid strength distribution were studied using microcalorimetric adsorption of NH3. The acidic properties were also examined by cumene cracking reaction as a function of Si/Al ratios. Systematic variation of acidity and activity was observed as a function of Si/Al ratio. The initial heats of NH3 adsorption correlated well with activity indicate that acid sites with ΔH > 100 kJ/mole is responsible for cumene cracking activity. Linear correlations were obtained with total acidity and cumene cracking activities. The tetrahedral aluminum was found to be responsible for the observed acidities and catalytic activities. 相似文献
98.
Mesoporous GaSBA-15 molecular sieves with different nSi/nGa ratios have been directly synthesized using Pluronic 123 triblock polymer as a structure-directing agent by pH-adjusting method. The mesoporous materials have been characterized using ICP-AES, XRD, N2 adsorption, 71Ga-MAS NMR, SEM and TEM. ICP-AES studies show a high amount of gallium incorporation on the silica pore walls. The structural and textural properties of calcined GaSBA-15 are characterized by XRD and N2 adsorption. 71Ga MAS NMR results demonstrate that a high amount of tetrahedral-gallium could be substituted for Si in the framework of SBA-15. TEM and FE-SEM images show the uniform pore diameter and rope-like hexagonal mesoporous structure of GaSBA-15. These GaSBA-15 materials have been used as catalysts for vapour-phase t-butylation of 1,2-dihydroxybenzene (DHB) for selective synthesis of 4-t-butylcatechol (4-TBC) under different reaction conditions. GaSBA-15(10) gave the highest 93.2% conversion of DHB and 95.7% selectivity of 4-TBC as compared with other GaSBA-15 catalysts. 相似文献
99.
总结了电渣 2 0Mn1A钢从电炉冶炼到电渣重熔钢中铝、钛及主要成分的变化情况 ,为该钢的生产提供了控制成分的依据 相似文献
100.