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161.
Influence of Mn and Cu addition on the hyperfine parameters of amorphous and nanocrystalline FeCoNbB alloys 总被引:1,自引:0,他引:1
The effects of Cu and Mn addition on the hyperfine field of FeCoNbB HITPERM alloys are discussed from Mössbauer spectrometry. Amorphous and nanocrystalline samples at different stages of the nanocrystallization were studied. The effect of Cu addition correlates with the observed refinement of the microstructure. Mn mainly partitions to the matrix, decreasing the average hyperfine field of the amorphous matrix, although some Mn remains in the nanocrystalline grains, presumably, in a concentration below the maximum solubility of Mn in -Fe. 相似文献
162.
Taxonomy for protective ability of rust layer using its composition formed on weathering steel bridge 总被引:2,自引:0,他引:2
For a quantitative evaluation of the protectiveness of a rust layer formed on a weathering steel bridge, the relationship between the corrosion rate of the bridge and the composition of the rust layers formed on the girders was first investigated. These corrosion rates were clearly classified by the protective ability index (PAI) of α/γ∗ and (β + s)/γ∗, where α, γ∗, β and s are the mass ratio of crystalline α-FeOOH, the total of γ-FeOOH, β-FeOOH and the spinel-type iron oxide (mainly Fe3O4), β-FeOOH and spinel-type iron oxide, analyzed by XRD, respectively. The inequality of the former index α/γ∗ > 1 expressed the protectiveness criterion of the rust layer, while that of the latter index, (β + s)/γ∗< 0.5 or > 0.5, classified the corrosion rate of the non-protective rust layer. The PAI is useful for a quantitative evaluation of the protectiveness of a rust layer formed on a weathering steel bridge and is an important item for the corrosion assessment of the bridge. 相似文献
163.
P. K. Siwach H. K. Singh N. Khare A. K. Singh O. N. Srivastava 《Journal of Alloys and Compounds》2003,350(1-2):56-61
A new manganite type CMR material, La0.7Hg0.3MnO3 has been successfully synthesized and has been found to exhibit magnetoresistance (≈9%) at low fields (≈1.5 kG). The synthesis has been carried out through a solid state reaction route consisting of the formation of La0.7MnO3 followed by diffusion of Hg leading to La0.7Hg0.3MnO3. The as grown samples are polycrystalline and correspond to an orthorhombic unit cell with the lattice parameters; a=5.5183 Å, b=5.6383 Å and c=7.5368 Å. The typical grain size as revealed by scanning electron microscopy is in the range of 0.5–2 μm. The ρ–T behaviour shows a peak at TIM=227 K. The ρ–T behaviour above this temperature corresponds to that of an insulator and below this to that of a metal. The ρ–T behaviour remains unaltered when a magnetic field (Hdc=1.5 kG) is applied. However, with this magnetic field a drop in the resistivity is observed up to 77 K. At room temperature the magnetoresistance ratio (MRR) is too small but it steadily increases as the temperature is decreased. Thus, MRRs at 227.13 and 77 K are 3.41 and 9.05%, respectively, in an applied field of Hdc=1.5 kG. At a given temperature the variation in MRR with field Hdc is rapid at lower field values (Hdc<1.2 kG) and scales linearly for higher field values (Hdc>1.2 kG). It may be mentioned that the present work on the synthesis and magnetoresistance behaviour of La0.7Hg0.3MnO3, is the first of its type. 相似文献
164.
D. Oleszak E. Jartych A. Antolak M. Pkaa M. Szymaska M. Budzyski 《Journal of Alloys and Compounds》2005,400(1-2):23-28
X-ray diffraction, Mössbauer spectroscopy and magnetization measurements were used to study the structure and some magnetic properties of Fe50Ge50 and Fe62Ge38 prepared by mechanical alloying from the elemental powders. In both cases in the early stages of milling the intermediate paramagnetic FeGe2 phase was formed. The mechanical alloying process of Fe50Ge50 resulted in the formation of the paramagnetic FeGe (B20) phase with an average crystallite size of about 15 nm. In the case of the Fe62Ge38, the ferromagnetic Fe5Ge3 (β) phase with a Curie temperature of about 430 K was obtained. The average crystallite size was about 9 nm. The average hyperfine magnetic field of about 16 T allowed it to determine that more than four germanium atoms exist in the nearest environment of the 57Fe isotopes in the Fe5Ge3 phase. 相似文献
165.
在X2001应力分析仪上采用悬臂梁加载法测试了可以用于铍的X射线应力测试的5个衍射晶面的应力常数。结果表明,铍的5个衍射晶面的应力常数差异较大,在进行X射线应力分析时.应采用相应衍射晶面的应力常数,才能获得准确的应力分析结果。由于X射线对铍有较大的穿透深度,必须考虑X射线穿透深度对应力常数标定的影响。 相似文献
166.
In the traditional scattering center extraction method based on the shooting and bouncing ray(SBR) technique,only the physical optics contribution of the target is considered.However,the physical optics method is unable to describe the contribution of the actual edge diffraction.By comprehensively considering the specular reflection and edge diffraction contribution of the target,an edge diffraction correction method for 3D scattering center modeling based on the SBR technique is proposed.Using the SBR technique and combining the image domain ray tube integration and equivalent edge currents method,the edge diffraction correcting formula for the 3D inverse synthetic aperture radar image is derived.Simulation results show that the proposed method is able to effectively improve the modeling accuracy of the 3D scattering center. 相似文献
167.
为了表征二维混凝土的传输过程,制备厚度为1 mm的混凝土薄片. 采用X射线透射成像(TXR)技术,联合扫描电镜、背散射和能谱分析技术(SEM/BSE/EDS)原位追踪水在2维混凝土薄片中的毛细自吸过程. 测试不同质量分数CsCl溶液对X射线透射图像的增强效果. 结果表明,CsCl能够提高吸水过程中混凝土薄片的TXR图像对比度,使得水在混凝土中的渗流路径更清晰、可辨. 水泥浆体在吸收CsCl后,扫描电子背散射图像的对比度显著增强. 不同位置铯原子的EDS能谱结果验证了TXR技术确定吸水前锋位置的准确性. 相似文献
168.
169.
We investigate the thermodynamics, kinetics, and capacity of the hydrogen storage reaction: Li2Mg(NH)2 + 2H2 Mg(NH2)2 + 2LiH. Starting with LiNH2 and MgH2, two distinct procedures have been previously proposed for activating samples to induce the reversible storage reaction. We clarify here the impact of these two activation procedures on the resulting capacity for the Li–Mg–N–H reaction. Additionally, we measure the temperature-dependent kinetic absorption data for this hydrogen storage system. Finally, our experiments confirm the previously reported formation enthalpy (ΔH), hydrogen capacity, and pressure–composition–isotherm (PCI) data, and suggest that this system represents a kinetically (but not thermodynamically) limited system for vehicular on-board storage applications. 相似文献
170.
Z.Y. Wu J. Zhang K. Ibrahim M.I. Abbas G. Li Y. Tao T.D. Hu F.Q. Liu H.J. Qian Y.N. Xie Q.H. Zhang L. Gao Z.Z. Chen 《金属学报(英文版)》2002,15(1):53-57
As a potential application of titanium-oxide nanoparticles, it is extremely important to investigate a detailed picture of the surface and interior structural properties of nanocrystalline materials, such as rutile and anatase with diameters 7.0 and 4.5nm, respectively. X-ray absorption spectroscopy has been used to identify the local Ti environment and related electronic structure. We combine the experimental results at the Ti edge in both bulk and nano-crystals to determine the lattice distortion in terms of differently characteristic preedge features and the variation in the multiple-scattering region of X-ray absorption near-edge structure (XANES) spectra. The relationship between the transition peaks and the surface-to volume ratio is also discussed. 相似文献