Yttrium sol–gel coating effects on the cyclic oxidation behaviour of 304 stainless steel

The present results reveal the interest of sol–gel coating technique to improve 304 steel high temperature oxidation resistance. An yttrium sol–gel coating appears to enhance the oxidation resistance during isothermal oxidation test, to decrease widely the oxide weight gain and to reduce the initial transient oxidation stage generally observed in the case of blank steels. Moreover, the experimental results confirm that yttrium sol–gel coating also plays a significant role on the cyclic oxidation behaviour of the 304 steel. In fact, the yttrium addition promotes remarkably the prolongation of the period during which the oxide scale still remains adherent to the substrate.     

溶胶–凝胶法制备ATO-SiO_2抗静电复合薄膜的特性研究

采用两步溶胶–凝胶法制备出 ATO(掺锑氧化锡)-SiO_2复合抗静电薄膜。通过 DTA-TG、XRD、SEM 对 薄膜的结构和形貌进行了表征,结果表明:抗静电复合薄膜表面均匀致密。薄膜中 SiO_2为无定形结构,ATO 的衍射峰 与 SnO_2一致。研究了 SnO_2的含量对薄膜导电性能、结合强度和透过率的影响,发现随 SnO_2含量增加 ?(SnO_2/ SiO_2)从 5 至 12.5,薄膜的表面电阻降低(从 1010ù/□降低到 108ù/□),薄膜的结合强度下降,薄膜的透过率降低(从 89.0%降至 84.2%),结合三方面性能,得出最佳 SnO_2的配比为:?(SnO_2/ SiO_2)=10。     

C60高性能预拌混凝土的生产及应用

介绍了C60高性能预拌混凝土的研制及生产应用的过程与方法 ,对材料的性能、搅拌工艺进行了深入分析 ,为生产高强高性能混凝土提供了详细的思路     

Production of silver‐doped analcime by isomorphous substitution technique

BACKGROUND: Metal‐exchanged zeolites have been reported to have significant limitations on cayalytic activity, such as counterbalancing the negative framework charges and limitation of active space. Alternative methods of incorporating silver ions into the framework of zeolites are therefore necessary. This paper reports on a technique for producing silver doped analcime by isomorphous substitution of silver ion into the framework of analcime. The amount of aluminium in the gel composition was reduced by a factor of 5%, 10% and 20% and an equivalent amount of silver was added to the gel and treated in a conventional manner for zeolite crystallisation. Some of the aluminium in the reaction gel was replaced with the silver. The silver‐doped analcime samples where characterised by X‐ray diffraction (XRD), scanning electron microscopy (SEM), energy dispersive X‐rays (EDX), Fourier transform infrared (FTIR) spectroscopy and inductively coupled plasma‐atomic emission spectroscopy (ICP‐AES) analysis. RESULTS: The amount of silver ions loaded for each reduction of aluminium as determined by EDX were found to be (w/w) 0.29%, 1.41% and 2.10%, respectively. XRD pattern SEM images of the silver‐doped analcime showed the presence of zeolite P in addition to analcime. CONCLUSION: Silver‐doped analcime was successfully produced with different silver loadings and may exhibit higher anti‐microbial activities than silver‐exchanged counterparts. Copyright © 2008 Society of Chemical Industry     

轻质高效保温材料掺杂硅气凝胶

利用正硅酸甲脂（ＴＭＯＳ）为原料的溶胶－凝胶过程，摸索了不同反应条件下形成凝胶的规律，并选用ＴｉＯ２粉末及玻璃纤维作为掺杂剂，采用超临界干燥处理制备出掺ＴｉＯ２的硅气凝胶，通过对红外光谱以及不同温度和气压条件下热导率的测量，讨论了不同成份配比以及相应的热传输过程对材料热导率的影响。结果表明，密度为２６０ｋｇ／ｍ＾３的掺杂硅气凝胶在８００Ｋ时的热导率为０．０３８ｗ／ｍ．ｋ，是一种新型的轻质高效保温材     

热分解法制备钛酸铅镧薄膜及其电性能研究

本文研究了用金属有机物热发解法制备ＰＬＴ８薄膜的工艺过程和基片对薄膜结构的影响，并且给出了铁电性能的测量结果。     

带有光放大的波分复用技术在光纤通信中的应用

本文论述了波分复用技术的优点及其应用；介绍了波分复用技术与光纤放大器相结合后的发展概况２；评述了波分复用技术发展中的主要问题及其在当前实用系统中的解决方案和今后的发展方向。     

Holmium-doped Porous Silicon Prepared by a New Electrochemical Approach and Its Photoluminescence

Ｐｏｒｏｕｓｓｉｌｉｃｏｎ（ＰＳ）ｗａｓｆｏｕｎｄｔｏｅｍｉｔｖｉｓｉｂｌｅｌｕｍｉｎｅｓｃｅｎｃｅａｔｒｏｏｍｔｅｍｐｅｒａｔｕｒｅｂｙＣａｎｈａｍｉｎ１９９０［１］．Ｔｈｉｓｐｈｅｎｏｍｅｎｏｎｉｍｐｌｉｅｄａｐｏｔｅｎｔｉａｌａｐｐｌｉｃａｔｉ...     

微量Si在W—7Ni—3Fe重合金中的行为

研究了掺到原料Ｗ粉中微量Ｓｉ（４００ｐｐｍ）在Ｗ－７Ｎｉ－３Ｆｅ重合金中的分布及在液相烧结过程中的行为。结果表明，Ｓｉ主要以固溶形式分布在Ｗ晶粒中。Ｘ射线光电子能谱（ＸＰＳ）分析发现，在掺杂Ｓｉ的Ｗ－Ｗ及Ｗ－基体相界面富集ＳｉＯ２和Ｎａ２ＳｉＯ３在未掺杂试样的断口表面发现了较弱的ＷＯ２的ＸＰＳ谱，而在掺杂合金中未发现ＷＯ２。