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61.
Anionic copolymerizations of styrene (M1) with excess 1-(4-dimethyl-aminophenyl)-1-phenylethylene (M2) were conducted in benzene at 25°C for 24h, using sec-butyllithium as initiator. Narrow molecular weight distribution copolymers with M?;n = 16.1 × 103 g/mol (M?w/M?n = 1.04) and 38.2 × 103g/mol (M?w/M?n = 1.05), and 24 and 38 moles of M2 per macromolecule, respectively, were characterized by size exclusion chromatography, 1H NMR spectroscopy and DSC. The monomer reactivity ratio, r1 = 5.6, was obtained from the copolymer composition at complete consumption of M1, assuming that the rate constant k22 =0,i.e. r2 =0. The polymers exhibited Tg values of 128 and 119°C, respectively, which correspond to an estimated Tg = 217°C for the hypothetical homopolymer of M2. 相似文献
62.
63.
地应力对工程岩体的稳定性影响很大,工程实践中常需定量地确定工程范围内的地应力。本文简要地介绍了地应力的概念、应用及常用的测量方法。 相似文献
64.
首先对OFDM的发展以及应用做了简要的介绍,然后讨论了当前OFDM研究过程中的两个关键技术问题,最后展望了OFDM的未来发展。 相似文献
65.
Thomas J. R. Hughes Arif Masud Isaac Harari 《International journal for numerical methods in engineering》1995,38(19):3193-3210
Finite element methods for dynamic analysis employing elements with drilling degrees of freedom are presented. The formulation is based on a variational principle in which displacements and rotations are interpolated independently. The issue of zero masses corresponding to rotational degrees of freedom is addressed and techniques for defining consistent and lumped rotational mass matrices are presented. 相似文献
66.
67.
Rates of ammonia (NH3) loss from a ryegrass sward measured using a system of small wind tunnels were compared with concurrent measurements made using a micrometeorological mass balance method. Measurements were made during two experiments within a circular plot (radius 10m) treated with urea at a rate of 200kgNha?1. In the first experiment, air speed through the tunnels was adjusted as necessary to maintain a value of approximately 1ms?1. This value differed on most occasions from the mean ambient wind speed which was measured at a height of 250mm and which ranged from 0.61 to 2.95ms?1. Rates of loss measured using the wind tunnels differed by a factor of between two and five from those measured using the mass balance method; there was no consistent pattern in the differences between the rates of loss. The total losses of NH3 measured during 15 days were equivalent to 49.1 and 30.2kg Nha?1 for the mass balance and wind tunnel methods, respectively. In the second experiment, air speed through the tunnels was adjusted as necessary to maintain a value as close as possible to the mean ambient wind speed measured at a height of 250mm. Rates of NH3 loss measured using the two methods did not differ significantly; total losses of NH3 during 17 days were equivalent to 96.9 and 101kg Nha?1 for the mass balance and wind tunnel methods, respectively. The difference between the findings of the two experiments could be attributed to the direct effect of air speed through the tunnels rather than to differences between ambient temperatures and those inside the tunnels. During and following periods of rain the rates of loss measured using the tunnels were up to six times greater than those observed with the mass balance method. Rates of loss measured by the two methods became similar again when the tunnels were moved following rain. The study demonstrates that enclosures can be designed and operated to provide reliable measurements of the rate of NH3 loss from grassland. Potential applications of the two methods are discussed. 相似文献
68.
济钢350m^3高炉高富氧生产技术 总被引:1,自引:1,他引:0
分析了济钢350m^3高炉高富氧对产量,理论燃烧温度,炉况顺行状况,焦比和生产效益的影响,高富氧可提高产量,但升高焦比和高炉理论燃烧温度,一定程度上影响高炉顺行,存在富氧效益最大化的适宜富氧率.高炉生产应低富氧高喷煤,根据钢目前的情况,富氧率经2%-3%为宜. 相似文献
69.
In this paper we design a dynamic dictionary for
the priced information model initiated by Charikar et al. Assume that a set S consisting of n elements is given such that
each element has an associated price, a positive real number. The cost of performing an operation on elements of S is a function
of their prices. The cost of an algorithm is the sum of the costs of
all operations it performs. The objective is to design algorithms
which incur low cost. In this model we propose a dynamic dictionary, supporting
search, insert and delete, for keys drawn from a linearly ordered set.
As an application we show that the dictionary can be used in
computing the trapezoidal map of a set of line segments, a fundamental problem in
computational geometry. 相似文献
70.
A methodology for evaluating the reactivity of titanium with mould materials during casting has been developed. Microhardness
profiles and analysis of oxygen contamination have provided an index for evaluation of the reactivity of titanium. Microhardness
profile delineates two distinct regions, one of which is characterised by a low value of hardness which is invariant with
distance. The reaction products are uniformly distributed in the metal in this region. The second is characterised by a sharp
decrease in microhardness with distance from the metal-mould interface. It represents a diffusion zone for solutes that dissolve
into titanium from the mould. The qualitative profiles for contaminants determined by scanning electron probe microanalyser
and secondary ion mass spectroscopy in the as-cast titanium were found to be similar to that of microhardness, implying that
microhardness can be considered as an index of the contamination resulting from metal-mould reaction. 相似文献