矿化剂对氧化铬绿色釉呈色性能的影响

针对氧化铬绿色釉存在色调暗不够鲜艳的缺点，研究了矿化剂对其呈色性能的影响，经分光光度分析的扫描电镜测试，表明矿化剂具有一定的助熔作用和还原性，从而提高了氧化铬绿色釉的鲜艳度和着色力，增强了装饰性，同时矿化剂还能降低烧成温度，节约能源，具有应用价值。     

单轴-平面W型复合锶铁氧体的制备及其吸波特性研究

用草酸盐共沉淀和微量掺杂法研制六角晶系W型Ni,Zn,Co,Al多元复合锶铁氧体，通过调节Ni2W同Co2W的摩尔比例，可使该种铁氧体易磁化方向从C单轴型向垂于C轴的平面型转化，控制置换锶铁氧体中部分Fe3 的微量掺杂Al3 ，可以调整4πMs值，提高磁晶各向异性场，测试分析了5种不同含Co量的W型复合锶铁氧体粉料涂层的吸波特性，发现其自然共振吸收峰随Co含量增加向低频方向偏移，最高吸收峰可达32．8dB，是适用于电子隐形技术的高品位的微波吸收剂。     

添加剂对尖晶石型锰酸锂性质表征的影响

以LiOH·H_20和MnO_2为原料,分别掺入H_2BO_3、Al_2O_3、SiO_2和P_2O_5等添加剂,用固相分段法制备尖晶石型锰酸锂。结果表明,SiO_2和P_2O_5可以有效地改善LiMn_2O_4的电化学性能,H_3BO_3对锰酸锂的电化学性能影响不大,而Al_2O_3破坏了LiMn_2O_4的电化学性能。面扫描结果显示,Si或P元素各自都均匀地分散于LiMn_2O_4的物相中。从元素电负性和原子半径的角度分析了B、Si、P和Al元素对尖晶石型LiMn_2O_4结构和性能的影响。     

Preparation and Properties of Sintering Additives Coated Si3N4 from Heterogeneous Nucleation Processing

The sintering additives such as Al2O3 and /or Y2O3 were coated on the surfaces of Si3N4 particles via heterogeneous nucleation processing using a buffered pH solution as the precipitation reagent .They nucleated and grew only on the surfaces of Si3N4 and did not form sol particles in solution by TEM observation .The isoelectric point(IEP) of coated Si3N4 was different from that of as-received Si3N4.The IEP of Al(OH)3-coated Si3N4 occurred at pH8.4, which is close to that of alumina .When Al(OH)3-coated Si3N4 particles were coated with Y(OH)3,the IEP of coated Si3N4 powder shifted from pH8.4 to pH9.2 ,similar to that of yttria.In addition ,the rheological data showed that Al2O3 and /or Y2O3 coated Si3N4 suspension is nearly Newtonian and that added Si3N4 suspension shows a shear rate thinning behavior.     

电磁胀形磁场力的有限元分析

研究电磁胀形过程中工件受到的磁压力沿长度方向和厚度方向的分布是工件变形分析的基础。采用有限元方法对电磁胀形过程中作用工件上的磁场力进行了数值模拟。在磁场特性理论分析的基础上确立了模型的边界条件，得到了磁场力沿工件长度和厚度方向的分布规律。模拟结果与测量值基本吻和。     

硫化胶交联结构及其性能

综合讨论了聚合物／聚合物之间的交联结构及聚合物／填料之间的偶联结构对硫化胶抗硫化返牟性，抗氧老化性及动态疲劳性能的影响。     

金属清净剂的性能研究

为了改进金属清净剂的抗氧性和极压抗磨性能，用一种含硫磷的羧酸衍生物部分中和清净剂中过碱性组分，得到两种改进的金属清净剂，并用四球机和热重分析仪评价其极压抗磨和抗氧化性能。结果表明功能化处理提高了金属清净剂抗氧化和极压性能，但未对分散和抗磨性能产生显著影响。     

线加权余量法及其在正交异性板弯曲分析中的应用

利用有限差分法对控制方程和边界条件进行半离散化,使其定义在一些离散线上,然后采用加权余量法求解。这就是本文提出的线加权余量法,也可称之为有限差分-加权余量分维耦合法。文中以正交各向异性薄板弯曲平衡问题为例推导了有关具体算式,给出了数值算例,说明了本文方法的有效性。     

Effects of a Nd—Fe—B magnetic filler on the crystallization of poly(phenylene sulfide)

The crystallization of poly(phenylene sulfide) (PPS) in a polymer–magnetic Nd—Fe—B powder suspension was studied. Isothermal crystallization behavior was analyzed by way of differential scanning calorimetry, and the kinetics were described via the Avrami equation. The Avrami parameters and the crystallization times were strongly affected by both the particle size and the presence of a coupling agent coated on the filler particles. The small Nd—Fe—B particles exhibited long induction and half‐times, whereas the large particles tended to have short crystallization times. Particles ranging from 38 to 150 μ appeared to have similar crystallization times and to have no significant change in the value of Avrami index with melt crystallization temperature. As a result of these analyses, the dynamic mechanical properties were determined to correlate the fundamental polymer crystallization characteristics and the physical properties of the PPS binder. The enhancement of the wetting of the filler to the binder was promoted through the coupling agent, as confirmed by dynamic mechanical testing performed on the samples. The storage modulus typically decreased because of the presence of the uncoated small particles. Conversely, the loss modulus was enhanced because of the presence of the coated small particles in the PPS binder. © 2002 Wiley Periodicals, Inc. J Appl Polym Sci 83: 1091–1102, 2002     

用于高压电容器的SrTiO3基陶瓷

报道ＳｒＴｉＯ３基陶瓷的制备方法和介电性质，给出了用此种陶瓷制成的高压电容器的试验结果，并对它位进行了讨论。