英山粉加入量对烧结矿强度影响的试验研究

在不同的二元碱度下,应用微型烧结法试验,分别对英山粉配比为0％、3．0％、6．0％、9．0％、12．0％、15．0％时的铁矿石混合料进行烧结,研究英山粉加入量对烧结矿抗压强度的影响。研究结果表明：英山粉配比的增加对烧结试样的抗压强度不利,而碱度提高有利于增加烧结试样铁酸钙的生成数量,可以改善英山粉配比的增加对抗压强度的不利影响;英山粉配比不超过6．0％时,烧结试样要保持较高的抗压强度,烧结混合料的碱度应控制在1．9左右;英山粉配比超过6．0％以后,烧结试样要保持较高的抗压强度,烧结混合料的碱度应控制在2．3左右。     

基于模糊数学的低致敏营养餐包感官评价研究

以低致敏蛋白、微囊化油脂以及复合糖元为主要原料制备开发低致敏营养餐包。从粉体的颗粒特性、冲调特性和主客观感官特性等对餐包开展评价研究,利用模糊数学法对餐包冲调后的色泽、气味及滋味、组织状态进行感官评价;通过餐粉的均匀度、溶解稳定性、湿润性进行基本特性评定。结果表明：餐包粉体粒度分布与餐包冲调特性具有相关性,细粉颗粒（0~30 μm、0~50 μm、0~100 μm）与餐包冲调特性呈负相关性,与粗粉颗粒（200~500 μm）呈正相关性,即随细粉粉体颗粒体积不断增加,湿润时间不断增加,冲调特性逐渐变差;随粗粉粉体颗粒体积不断增加,湿润时间不断减少,则冲调特性不断加强。粉体粒径与餐包感官评分呈正向线性相关性,一定范围内,随粒径不断增大,感官评分不断加强,产品品质质量较好。该评价体系为完善低致敏营养包的加工工艺提供了理论依据。     

添加微细铬铁粉对烧结钢摩擦磨损性能的影响

研究了加入不同含量的微细铬铁粉对烧结钢干摩擦磨损性能的影响,并借助于扫描电镜观察分析其磨损形貌,探讨摩擦磨损机制。研究结果表明:添加微细铬铁粉可改善烧结钢的强度、硬度和摩擦磨损性能,铬的质量分数为1.5%时,耐磨性最佳。磨损造成一定厚度的塑性变形,硬度较高的材料塑性变形层较薄。磨损早期,磨粒磨损是主导机制,磨损后期,由于塑性变形导致亚表层产生裂纹,进而发生的剥层磨损是主导磨损机制。     

Strain hardening of porous iron under uniaxial compression

A series of experiments was carried out with powder iron of 1–40% porosity including deformation by compression to various degree of deformation, and strain hardening curves were calculated. It was established that change in the loading sign relative to uniaxial tension had practically no effect on the strain hardening laws of the solid phase, although it basically changed the porosity contribution to the loading curve formation. Translated from Poroshkovaya Metallurgiya, Nos. 1–2(411), pp. 106–112. January–February, 2000.     

添加物对Fe_2O_3超微粒的稳定作用

粒子的尺寸直接关系着气敏元件性能的好坏．为了防止Ｆｅ２Ｏ３超微粒在气敏元件烧结过程中长大，我们在纯Ｆｅ２Ｏ３中掺入５ｍｏｌ％碱土金属离子，利用ＸＲＤ和ＴＥＭ系统研究了掺杂物对Ｆｅ２Ｏ３超微粒子的稳定作用，并对由掺杂引起的Ｆｅ２Ｏ３电学性质的变化作了初步探讨．     

等离子喷焊铜基自熔性合金的研制

为了克服铜铁异种材料喷焊过程中易产生焊缝裂纹和基体裂纹的倾向,研制开发了一种Cu-Ni-Sn自熔性合金粉末材料.通过对Cu-Ni-Sn粉末材料的化学成分的设计,喷焊层的组织显微结构及抗腐蚀性能的综合分析,认为该材料等离子喷焊工艺性能良好,焊层耐腐蚀效果十分明显.在生产实际中应用等离子喷焊制备Cu-Ni-Sn焊层,能明显提高粉末材料的熔敷率和性能,并且改善劳动工作环境.该合金性能优于传统材料,值得推广.     

用熔盐电解法制备超细钨粉

在NaCl-KCl-Na2WO4-WO3熔体中,用熔盐电解法电解氧化钨制取细钨粉和超细钨粉。在电解温度为720℃,阴极电流密度为250mA/cm^2的条件下,得到平均等积圆直径为1．2μm、长宽比为1．6的超细钨粉。在低阴极电流密度时,阴极的电解反应为W^6 放电,在高阴极电流密度时,阴极的电解反应为Na^ 放电。研究了温度、阴极电流密度和Na2WO4的含量对电流效率的影响。     

钨铜化合物氢还原制备钨铜复合粉研究

通过对钨铜化合物氢还原过程进行热力学分析,找到了制备均匀细颗粒钨铜复合粉的热力学途径--彻底快速除去还原系统中的水分.设计了封闭还原系统,用此系统进行氢气热还原,不仅使氢气得到充分利用,而且容易判断反应终点.通过系统内的特殊装置除水,降低了还原温度,在600℃下还原得到了混合均匀的钨铜复合粉.系统能彻底快速除去反应生成的水分,使反应物的湿度大大降低,确保得到细颗粒的钨铜复合粉,其平均粒径小于80nm.     

The Effect of Formulation on Radioiodide Thyroid Uptake in the Hyperthyroid Cat

This investigation was designed to compare in vitro dissolution profiles from sodium iodide capsules with radioiodide thyroid uptake in hyperthyroid cats using sodium iodide capsules prepared with a formulation exhibiting a complete release of radioiodide (I-123) in vitro and a formulation with an incomplete release of radioiodide. In vitro dissolution profiles for I-123 sodium iodide capsules with two different formulations were determined using the USP XXIII dissolution test. The two formulations studied in vitro were sodium phosphate dibasic powder with 1% magnesium stearate and calcium phosphate dibasic powder with 3% magnesium stearate. By 20 min after initiation of the dissolution test, over 95% of the I-123 was released from capsules of sodium phosphate dibasic powder. The capsules of calcium phosphate dibasic powder reached 75% at 65 min, with no further release occurring thereafter. There was a statistically significant difference in the dissolution profiles of the two formulations. The thyroid uptake of I-123 from capsules exhibiting complete release and incomplete release of radioiodide was determined in hyperthyroid cats. At 4 hr, the mean percentage thyroid uptake value for sodium phosphate dibasic powder with 1% magnesium stearate (complete release formulation) was 12.0% compared to 9.4% for calcium phosphate dibasic powder with 3% magnesium stearate (incomplete release formulation); at 24 hr, the values were 34.4% compared to 23.7%. The data suggest that the incomplete dissolution profile observed in vitro may correlate with a reduction in the bioavailability of the radioiodide in vivo. However, using the Wilcoxon signed rank test, statistically significant differences did not occur between the complete release formulation and incomplete release formulation at either 4 hr or 24 hr (p >. 05). The results of the in vivo study with five hyperthyroid cats were not conclusive due to the variability in response between individual cats.