疲劳裂纹扩展行为的研究现状及钛合金的疲劳裂纹扩展特征

疲劳裂纹扩展行为是现代材料研究中重要的内容之一。论述了组织结构、环境温度、腐蚀条件以及载荷应力比、频率变化对材料疲劳裂纹扩展行为的影响。总结出疲劳裂纹扩展研究的常用方法和理论模型,并讨论了"塑性钝化模型"和"裂纹闭合效应"与实际观察结果存在的矛盾。最后,对钛合金疲劳裂纹扩展研究的内容和研究结果进行了概述。     

Microstructure of Titanium after Hydrogenation

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Microstructural evolution and interfacial reactions between Ti and ZrO2/CaTiO3 composites

Various proportions of ZrO₂/CaTiO₃ powders were mixed and hot pressed at 1500°C/30 min for Ti casting. The hot-pressed ZrO₂/CaTiO₃ composites were reacted with pure Ti at 1700°C/10 min in Ar. The interfacial reaction between Ti and ZrO₂/CaTiO₃ composites was investigated through X-ray diffraction, scanning electron microscopy, transmission electron microscopy, and energy-dispersive X-ray spectroscopy. The ZrO₂/CaTiO₃ composites with less than 10 vol.%, CaTiO₃, and a minor amount of residual TiO₂ were found. When the content of ZrO₂ was increased to larger than 10 vol.%, two Ca₂Zr₅Ti₂O₁₆ and CaZrTi₂O₇ phases appeared in the composites. The amount of CaTiO₃ and CaZrTi₂O₇ in the composites gradually decreased as the amount of ZrO₂ increased. When Ti came in contact with ZrO₂/CaTiO₃ composites with less than 10 vol.% ZrO₂, the resulting eutectic reaction produced a liquid phase and induced melting. When ZrO₂ was increased to more than 30 vol.% in the composites, Ca₂Zr₅Ti₂O₁₆ and CaZrTi₂O₇ changed completely to CaZrO₃, Ti₂O, CaO, and ZrO₂. With more than 30 vol.% ZrO₂, no other reaction phases occurred in the Ti side after contact with the ZrO₂/CaTiO₃ composites, which is conducive for producing ceramic composites for Ti casting applications.     

Johnson-Cook dynamic constitutive relationship for TC 16 titanium alloy

The true stress--strain curves of TC16 alloy with a wide range of strain rates were investigated under uniaxial quasi-static tension and uniaxial dynamic compression with the lnstron 8032 test machine and the split Hopkinson bar respectively. The results indicate that the true stress increases with increasing strain rate, while decreases with increasing temperature. Under the 105 s^-1 high strain rate and temperature higher than 673 K, the true stress would even be less than that under quasi-static condition. A new method incorporating TCl6＇s stress strain curve developing item was proposed to determine the coefficients in J-C model easily and to avoid the estimation of the adiabatic temperature rising. The Johnson-Cook dynamic constitutive relationship for TC16 was obtained for the first time. Good agreement was obtained between the model prediction and the experimental stress--strain curves for TC16 under both quasi-static and dynamic loadings.     

The effect of α phase on the deformation mechanisms of β titanium alloys

The effects of α and β phase interactions on the tensile and creep deformation behavior of β titanium alloys was studied using Ti-6.0wt.% Mn and Ti-8.1wt.%V as the model two-phase alloys, and Ti-13.0wt.%Mn and Ti-14.8wt.%V as the single-phase β alloys. The β phase of α-βTi-8.1V deforms by stress-induced hexagonal martensite (α′), while slip and twinning occurs in the single-phase β alloy with the same chemistry as the β phase. No stress-induced martensite was observed in the β or α-βTi-Mn alloys. This behavior is modeled in terms of a number of factors, including elastic interaction stresses between the α and β phases, coherency between the α phase and hexagonal martensite, and β phase stability. This paper was presented at the Beta Titanium Alloys of the 00’s Symposium sponsored by the Titanium Committee of TMS, held during the 2005 TMS Annual Meeting & Exhibition, February 13–16, 2005 in San Francisco, CA.     

钛及钛合金抑菌技术的研究进展

钛作为食品接触材料不具备抑菌功能,使用过程中易滋生细菌对人体健康不利。文章主要介绍了钛及钛合金抑菌处理常用方法及最新的研究进展,包括合金化处理,离子注入、热喷涂、微弧氧化等表面处理方式。对抑菌钛合金的研究方向及其在日用餐具、炊具、水具等行业的应用前景作了展望。     

氢处理技术在钛合金中的应用

氢处理工艺是钛合金的一种特有的热处理方式，用于改善铸造、锻造钛合金件以及粉末冶金件的组织和性能。本文综述了氢处理在钛合金中的一些应用，主要介绍了国外的研究动向。     

纯铝等径角挤技术（I）——显微组织演化

研究了纯铝在 3种 (A、B和C)不同等径角挤工艺中的显微组织演化。结果表明 :纯铝经过等径角挤压变形后 ,其显微组织特征与加工路线有很大的关系。提出了立方元素扭转模型 ,分析了 3种不同加工路线的剪切面和剪切方向 ,较好地解释了采用 3种不同路线挤压后材料显微组织的演化规律。在路线C(各道次挤压间试样旋转 180°)中 ,每次挤压样品总是在相同的剪切面上发生剪切 ,每相邻道次之间的剪切方向相反 ,前一次变形产生的剪切应变被随后紧接着的下一次挤压所抵消 ,这导致了多余的剪切应变 ;在路线A(各道次挤压间试样不旋转 )中 ,有两个相交成 6 0°的剪切面 ,剪切交替地在两个剪切面上进行 ;在路线B(各道次挤压间试样旋转 90°)中 ,存在 4个不同的剪切面和剪切方向 ,挤压交替地在 4个剪切面上进行 ,X ,Y和Z平面上的晶粒都发生了剪切 ,这有利于等轴晶结构的形成     

热处理对Ti-Al-Sn-Zr-Mo-Si-X系合金性能的影响

研究了热处理对3种Ti-Al-Sn-zr-Mo-Si-X（X为ⅤB，ⅥB族一种或几种元素）系合金（A、B、C）室温拉伸性能的影响，对优化合金的热处理制度及优选热处理制度下3种合金的疲劳裂纹扩展行为也进行了探讨。结果表明，优选热处理制度下A、C合金的裂纹扩展速率差别不大，B合金560℃时效处理后，裂纹扩展速率比540℃时效处理的小。在相同热处理制度下，比较3种合金裂纹扩展速率的结果表明，IgΔK在1．2～1．5范围内B合金的抗疲劳裂纹扩展性能较优。     

纯铜动态再结晶的Monte Carlo法模拟

本文建立了一种基于能量判据的确定动态再结晶各个阶段临界应变的方法，并基于此种方法Monte Carlo(MC)法进行了纯铜动态再结晶的二维模拟，定量计算了变形引起的存储能与变形之间的关系，计算出了发生动态再结晶的临界应变。模拟结果表明，采用MC法可以揭示动态再结晶的形核生长过程与应变历史之间的关系。结合本文所建立的基于能量判据的确定动态再结晶各个阶段临界应变的方法，可以预测开始发生动态再结晶的临界变形条件。