Predicting the shape of organic crystals grown from polar solvents

A method for predicting the shape of organic crystals grown from polar solvents is presented. The model is an improvement of the recent method developed by Winn and Doherty (A.I.Ch.E. Journal 44 (1998) 2501) for predicting the shape of organic crystals grown from solvents in which the energy of adhesion at the interfaces is dominated by dispersive forces (e.g., non-polar solvents). The principal characteristic of the new method is that it can account for the role of hydrogen donor and hydrogen acceptor atoms in forming strong bonds at the interface. This technique is a first step towards predicting the shapes of organic crystals grown from polar solvents, and has been applied successfully to predict the shape of adipic acid grown from water, and succinic acid grown from water and from propanol.     

Contributions of source and inhibitory mechanisms to age-related retroactive interference in verbal working memory.

Determining contributions of source-monitoring and inhibitory function to age-related forgetting has been an elusive goal for cognitive theorists. Five studies used a verbal working memory paradigm to examine mechanisms accounting for disproportionate retroactive interference (RI) experienced with adult aging. Participants distinguished studied target-word pairs from interfering pairs that were read aloud. Source-monitoring and inhibitory task components varied through manipulations of response requirements. RI effects were primarily due to source-monitoring failures rather than to inhibitory failures. Removing both source and inhibitory components eliminated age differences in RI. When source monitoring was emphasized, RI continued to be observed in all age groups but disproportionately for older adults. Process dissociation analyses of memory found recollection decreases and familiarity increases consistent with source failures. (PsycINFO Database Record (c) 2010 APA, all rights reserved)     

Suitable test structures for submicron ion beam analysis

For the precise determination of the sizes of submicron beam spots test structures with an excellent edge definition are required. For this purpose a semiconductor heterostructure consisting of an 1.62 μm GaInP epi-layer grown on (0 0 1) GaAs has been made, which provides atomically sharp edges for beam spot size measurements. Since the sample has been thinned down by standard transmission electron microscope (TEM) preparation techniques, it can be used for both PIXE and STIM. The sample has been investigated with a TEM and the ion nanoprobe LIPSION. A one-dimensional beam profile in the low current mode was determined by a STIM measurement using 2 MeV protons and yielded a FWHM of (41±4) nm, which is the smallest value reported so far for high energy nuclear micro- and nanoprobes. Furthermore we present nickel nanowhiskers produced at the GSI Darmstadt by electrochemical preparation of etched ion track membranes that have been used to obtain two-dimensional images of the shapes of submicron beam spots. For these measurements a scan over a single nickel nanowhisker having a diameter of 220 nm and a height of about 6 μm was performed.     

Quantity,controls and functions of large woody debris in Midwestern USA streams

Large woody debris (LWD) can increase stream habitat heterogeneity by providing structure, altering flow patterns, enhancing sediment deposition, forming pools and retaining organic matter. In North America, the role of LWD has been studied extensively in streams of mature forests (e.g. Pacific Northwest), but few studies have assessed LWD in streams of younger forests (e.g. Midwestern USA). Our objectives were to: (1) quantify the volume and abundance of LWD in a set of Midwestern streams; (2) evaluate possible factors influencing LWD quantity; (3) identify the functional roles of LWD; and (4) compare LWD levels in the upper Midwest to those elsewhere in North America. In 2002 and 2003, we measured LWD and geomorphological variables in 15 low‐gradient streams draining previously logged watersheds in the Upper Peninsula of Michigan. Mean (±SE) LWD volume (0.77 ± 0.12 m³ 100 m⁻²) and abundance (33 ± 3 pieces 100 m⁻¹) were 71% and 10% lesser, respectively, than in streams of similar gradient elsewhere in North America. Channel shape (width:depth ratio) explained 30% of the variation in LWD volume (multiple stepwise regression, P = 0.015) while LWD length and length:channel width combined, explained 72% of the variation in LWD density (multiple stepwise regression, P < 0.0001). About 50% of the LWD either stored sediment or stabilized banks and 14% of the LWD formed pools, although pool density was not significantly related to LWD volume or density. LWD levels, overall, were low in upper Midwestern streams, but the relative importance of that LWD to ecosystem function may be magnified in these wood‐poor systems. Copyright © 2006 John Wiley & Sons, Ltd.     

异形柱框架结构设计方法分析与参数控制

近年来,异形柱框架结构(框轻结构体系),因其能较好地满足建筑使用上和结构性能上的要求,而逐步得到了推广应用,并被列为建设部首批住宅建设新技术推荐目录。但异形柱框架结构设计目前还没有可依据使用的国家标准和行业标准。本文根据对江苏省地方标准《钢筋混凝土异形柱框架结构技术规程》(DB32/512-2002)的理解,结合笔者设计实践经验,提出个人看法,供同行参考。     

工程结构优化设计发展综述

 着重评述了工程结构优化设计研究领域从最初的尺寸优化发展到形状优化、拓扑优化的基本历程及其相关特点，并对优化设计选用的优化算法进行了归类，提出了这一领域今后仍然有待于发展的主要方面．     

On the improvement of detection characteristics of trans-stilbene crystals by improving crystal perfection

Organic molecular scintillating crystals are noted for their good timing and particle discrimination process. Trans-stilbene is one such candidate noted for its good particle detection characteristics for the past five decades. Progressive strengthening of detection characteristics of trans-stilbene has been attempted by improving crystal perfection. A series of timing resolution studies have been carried out for the Bridgman grown trans-stilbene crystals under different experimental conditions. The results were compared with the previously reported values. Pulse shape discrimination process has been carried out for ²⁴¹Am and ²⁵²Cf sources and good discrimination has been obtained for gamma-alpha and gamma-neutron sources from the grown organic phosphor crystal. Electronic Publication     

精密陶瓷部件近净成型技术的发展

重点介绍了近十年发展起来的陶瓷部件的近净成型技术 ,主要包括直接凝固注模成型、凝胶注模成型、陶瓷注射成型、陶瓷无模成型和微注入成型。对这些新的成型方法的原理、工艺过程及应用特点进行了较全面的分析与比较。     

浓缩大豆磷脂制取工艺及设备的研究

对水化油脚采用新工艺和新设备制取浓缩大豆磷脂，并对制取浓缩大豆磷脂的影响因素进行分析和优化，得到了制取浓缩大豆磷脂新工艺和最佳工艺参数。