连续式超临界流体萃取进卸料装置

概括了超临界流体萃取技术和包括连续式操作在内的超临界流体萃取装置的研究现状 ,提出了一种通过球形进、卸料器完成固相物料超临界流体萃取连续化进卸料的装置 ,介绍了该装置的结构和工作原理 ,给出装置中各主要部件的计算方法。     

混凝土浇筑质量对钢管混凝土性能的影响

着重阐述钢管与其核心砼粘结强度对钢管砼承载影响问题 ,并介绍三种常用浇筑方式和检测方法。     

Experimental Study of Concrete Subjected to Explosive Loading

The main subject of this paper is to demonstrate the response of structural concrete to different imposed strain rates. Attention is focused on the strain rate about 10^-2 s ^-1>, where some technical difficulties are experienced when an exact determination of mechanical properties for quasi-brittle materials is attempted. The design of a measurement system, which realizes computer acquisition, analysis, and graphic representation of data, is also presented.     

Strength of Metals at High Strain Rates

Results of metal testing in impact tension–compression and indentation are analyzed. As the analysis of these data demonstrates, the strength of metals increases greatly with strain rates and at moderate indentation rates. At high indentation rates, a decrease in the specific energy (per unit volume of a displaced material) necessary for the formation of a conical cavity was observed. The account of the effects of viscosity, temperature increase upon plastic deformation and its localization can be used to explain the above phenomena.     

Optimal size,hydraulic retention time and volatile solids loading rate of biogas unit using water hyacinth

With a view to evaluate the effects of hydraulic retention time and volatile solids loading rate on methane production using water hyacinth, experiments were conducted in a 160 dm³ capacity, well-mixed continuous digestion unit at ambient temperature. The optimal design of biogas plant using water hyacinth was elucidated, to provide a unit giving a maximum methane yield of 0.16 nm³ kg^?1 volatile solids added, which was 60% greater than the conventional plant using cowdung. The calculations of optimal design factors were based on reactor size, hydraulic retention time and volatile solids loading rate; considerations were made of capital cost, running costs and operational revenue.     

Biaxiale Ermüdung reibrührgeschweißter Strukturelemente

Biaxial fatigue of friction stir welded stiffened panels Within the framework of the European WelAir project, cruciform specimens made from stiffening FSW overlap joints were fatigued in the DLR biaxial test rig. To resemble the loading situation of pressurized fuselage structures, proportional loading without any phase shift, but with different load ratios λ between the loading components in both directions was applied.Natural crack initiation and subsequent crack growth were governed by the stiffness gradient caused by introducing the stringer. Cracks initiated and propagated at run‐in and run‐out locations in a direction perpendicular to the weld seam. The shortest fatigue life was observed for uniaxial loading in welding direction (λ = 0). An additional stress component perpendicular to the joint line (λ > 0) resulted in a higher number of cycles to failure. Similar to single stringer panels, increasing the load ratio also increased the number of cycles to failure for FSW clip‐stringer structural members, but additionally gives a different location of the fatal crack.     

Case Study of an Aerosol Explosion and a Method to Determine Explosion Temperatures

A failure analysis case study is presented for a two-piece aerosol containing tetrafluoroethane, commonly referred to as Refrigerant 134a. A gentleman was preparing to recharge the air conditioning system of an automobile when the bottom exploded off the aerosol container, propelling the body of the aerosol container like a rocket, which hit the man in the eye and blinded him in that eye. The aerosol was never connected to the air conditioner, therefore backpressure from the air conditioner (AC) compressor was ruled out as a cause for the explosion. The objective of the study was to determine why the aerosol exploded. Several recently developed test methods were used, including two types of heat-to-burst tests and a puncture chamber to measure the pressure-versus-temperature behavior of aerosols. More common test methods were also used, such as water bath pressure tests, hydro pressure burst tests, pneumatic pressure burst tests, hardness measurements, weight measurements, metallography, scanning electron microscopy (SEM), energy-dispersive spectroscopy (EDS), and an accident scenario recreation. A semi-empirical correlation between the hardness and weights of the container bottoms was used to determine the explosion temperature and/or pressure. This semi-empirical correlation agrees in principle with an analysis of the explosion pressures using finite-element analysis (FEA). The root cause for the explosion was determined to be a lack of strength of the bottom of the two-piece aerosol coupled with heating the aerosol to temperatures significantly above room temperature.     

基于加载算法的室内无线信道OFDM接收机的性能

本文研究了无线局域网中使信号频谱得到优化的一种简单OFDM子载波加载算法。此算法基于边缘自适应（Margin Adaptive）加载准则及其在室内无线信道上的性能。     

Two-stage fatigue loading of woven carbon fibre reinforced laminates

A brief review of the models used to predict the cumulative fatigue damage in FRP composites is presented. Two‐stage fatigue loading of a [0/90,± 45₂,0/90]_s quasi‐ isotropic woven carbon fibre/epoxy resin laminate was evaluated at stress ratio R = 0.05 and the failure mechanisms investigated using x‐radiography after each loading stage. The results are presented in terms of fatigue strength and damage growth and are compared with those in the literature. A low‐to‐high loading sequence is more damaging than a high‐to‐low one and the Palmgren‐Miner linear damage rule may no longer be valid for this kind of material, as previously reported.     

UV法测定聚甲基丙烯酸酯纳米粒中胰岛素的包封率

建立一种简便易行的测定聚甲基丙烯酸酯胰岛素纳米粒中游离胰岛素含量方法.用Nanosep OD100C33超滤膜分离纳米粒和游离药物,在276 nm处测定药物的吸光度,建立胰岛素含量测定方法,并对线性、回收率、精密度等指标进行考察,最后测定各种胰岛素和载体比例混合的纳米粒的包封率.结果发现,该超滤膜能较好地分离纳米粒和游离的药物,在0.11～1.10 u/mL范围内,药物在276 nm的吸光度和浓度存在良好的线性关系(r=0.999 8),线性方程为A=0.868 8C-0.001 6,高、中、低3种浓度的回收率和精密度良好.该方法操作简单、结果可靠,可用于胰岛素纳米粒中药物包封率的测定.