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71.
由于存储空间异常引起的系统故障,系统开发或维护人员很难从失效特征直接判断到根原因。另外,存储空间异常通常会引起整个系统崩溃,对于安全关键系统,如航空电子系统,系统的失效往往会引起坠机或人员伤亡,因此,对安全关键系统的空间分析显得尤为重要。由于系统栈空间的分析涉及系统动态运行状态,在程序的任意点都有可能被中断服务程序或实时操作系统的其它任务中断。此外系统的栈分析需要基于目标码等特性,再次增加了对于系统栈空间分析的难度。本文从栈空间分析的必要性出发,提出一种综合中断抢占图的栈分析理论和方法,并就安全关键系统如何保证栈空间使用的确定性进行论述。最后,就安全关键软件系统FCOS的栈空间分析过程进行详细的阐述。 相似文献
72.
磺酸型Gemini表面活性剂的合成及表面活性 总被引:2,自引:0,他引:2
以壬基酚、1,4-二溴丁烷和氯磺酸为主要原料,通过三步反应合成了新型的磺酸型Gemini表面活性剂9BA-4-9BA,讨论了合成反应时间、温度以及催化剂对产物纯度和产率等因素的影响,优化了反应过程。利用核磁共振谱和红外光谱表征了产物结构,并通过DCTA21表面/界面张力仪测试其水溶液中的表面张力。和传统表面活性剂相比,合成的Gemini表面活性剂9BA-4-9BA具有更高的表面活性,其临界胶束浓度和C20分别为6.2×10-4mol/L和1.1×10-5mol/L。 相似文献
73.
74.
K. N. Mehrotra M. Chauhan R. K. Shukla 《Journal of the American Oil Chemists' Society》1996,73(7):897-902
The ultrasonic velocity and density measurements of europium soaps in a mixture of benzene and methanol (3:2, vol/vol) were
used to evaluate various acoustic parameters and molar volume and to determine the critical micelle concentration. The results
showed that the ultrasonic velocity, specific acoustic impedance, molar sound velocity, and molar compressibility increase,
and intermolecular free length, adiabatic Compressibility, and relative association decrease with increasing concentration
and chainlength of the soap. The results were interpreted in terms of soap-solvent interaction. 相似文献
75.
76.
The preparation of dibasic acid-containing soy phospholipid was made by transesterification reaction with alkyl ester of diabasic acid with both lipase and alkoxide as a catalyst. The extent of incorporation of a dibasic acid varied with the molecular size of the dibasic acid. The extent of incorporation in soy phospholipids was 4–13% in the case of adipic acid and 9–20% in the case of sebacic acid. The surface-active properties of these modified soy phospholipids were examined and were found to be different from those of the original (unmodified) soy phospholipid. The interfacial properties such as critical micelle concentration (CMC), γCMC, surface excess concentration Γmax, and minimum area per molecule (Å), and thermodynamic parameters such as standard free energy of micellization, were found to depend on the hydrophobic part of the dibasic acids. 相似文献
77.
78.
Man-Hee HanJung-Whan Kim Jinwon KimJung Yoon Ko Jules J. MagdaIn Suk Han 《Polymer》2003,44(16):4541-4546
The acrylic comonomers hydroxypropyl methacrylate (HPMA) and N,N-dimethylaminoethyl methacrylate (DMA) have been used in several earlier studies to produce pH-responsive hydrogels. However, these same monomers can also be used to prepare hydrogels that are highly responsive to temperature. One manifestation of this temperature sensitivity is a sharp decrease in hydrogel optical transparency that occurs when the temperature exceeds a critical transition value. For example, a hydrogel that exhibits a swelling transition at the physiological pH value of 7.4 has a transition temperature of about 45 °C when the environmental salt concentration is 0.15 M. The value of the transparency transition temperature is shown to depend on hydrogel synthesis parameters such as comonomer mole ratio, crosslinker mole ratio, and even initiator concentration. By reducing the mole ratio of the crosslinker tetraethylene glycol dimethacrylate (TEGDMA), the transition temperature can be lowered by as much as 15 °C. Environmental salt concentration and solvent polarity are also shown to influence the transition temperature. 相似文献
79.
Nabel?A.?NegmEmail author Salwa?M.?I.?Morsy 《Journal of surfactants and detergents》2005,8(3):283-287
A weight loss technique was used to determine the corrosion inhibition efficiency of synthesized alkyl mono-and dibenzoate
triethanolammonium bromide derivatives (TEAMB, TEADB) in an acidic medium (2 N HCl) at different doses (50, 100, and 200 ppm).
The results showed that monoderivatives had a higher corrosion inhibition efficiency than diderivatives. The results were
correlated with several factors, including the alkyl chain length of the hydrophobic chains, interfacial tension (IT), critical
micelle concentration (CMC), and adsorption free energy of these inhibitors. Increasing the geometric length of the alkyl
chains in the synthesized inhibitors had an increasing effect on their corrosion inhibition efficiency, whereas decreasing
the CMC and IT had an increasing effect on their tendency toward corrosion inhibition. The number of hydrophobic chains attached
to the inhibitor molecules had a vital influence on their efficiency as corrosion inhibitors. 相似文献
80.
The effects of loading rate, fiber sizing, test temperature and global strain level on the adhesion strength between carbon fibers and a thermosetting epoxy (Epon 815) are studied using the single fiber fragmentation test procedure. Analytical methodology describing the viscoelastic behavior observed is also presented. The possibility of rate-temperature-interphase thickness superposition for the interfacial strength function is illustrated based on the analytical models discussed. Experimental data are discussed using Weibull statistics and also presented in the form of percent relative frequency histograms for the fiber fragments in a collective fashion. The use of histograms allows for interpretation of the skewness in the data population. 相似文献