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61.
Angela Altomare Carmelo Giacovazzo Anna Grazia Giuseppina Moliterni Rosanna Rizzi 《Journal of research of the National Institute of Standards and Technology》2004,109(1):125-132
The ab-initio crystal structure solution by powder diffraction data requires great efforts because of the collapse of the experimental information onto the one dimensional 2θ axis of the pattern. Different strategies will be described aiming at improving the process of extraction of the integrated intensities from the experimental pattern in order to make more straightforward the structure solution process by direct methods. Particular attention will be devoted to the EXPO program. Some of its performance will be analysed and results will be shown. 相似文献
62.
共聚物水凝胶的合成及其溶胀性能研究 总被引:3,自引:1,他引:2
以过氧化二苯甲酰(BPO)为引发剂,合成了N-乙烯基吡咯烷酮(NVP)-甲基丙烯酸肛羟乙酯(HEMA)-甲基丙烯酸丁酯(BMA)共聚物水凝胶,可作为软性角膜接触镜材料。探讨了不同比例的NVP、HEMA、BMA对材料溶胀性能的影响。 相似文献
63.
This paper presents some results from a totally new and powerful fusion between automated, digital photoelastic techniques and mathematical analysis of a crack experiencing closure. In essence, real-time photoelastic stress field data is acquired and fitted to a Muskhelishvili complex potential model of a loaded crack experiencing closure. The fit entails optimisation of multiple variables via a memetic algorithm, which combines a genetic algorithm and a local search. From observations made in this work, it is proposed that the plastic enclave around a crack tip will shield the crack from the full influence of the applied stress field. Furthermore, the effects of this ‘back stress’ are overcome by the applied tensile load in a way that, often, cannot be readily correlated with crack contact length, wake contact force, or with compliance. 相似文献
64.
聚乙烯醇膜的阻醇及导电性能(Ⅱ)戊二醛交联聚乙烯醇膜 总被引:3,自引:0,他引:3
为提高直接甲醇燃料电池(DMFC)用膜的阻醇性能,采用在渗透蒸发领域广泛使用且具有良好分离效果的聚乙烯醇(PVA)为主要材料,制备了戊二醛(GA)交联PVA膜,考察了此类膜的阻醇及质子导电能力。PVA(GA)膜的阻醇效果较目前在DMFC中广泛使用的Nation膜有显著提高,但其自身不具有质子导电能力,需外加电解质溶液以提高其电导率。 相似文献
65.
Schottky diodes were built on different polycrystalline diamond films grown by Microwave Plasma and Hot Filament Chemical Vapor Deposition and their electrical properties were studied. The barrier height increased with the diamond film quality and the corresponding ideality factor decreased. Even though the lower-quality HFCVD film displayed poor rectifying properties, it was found to be much less sensitive to variations in the operating conditions (air vs. vacuum). The activation energies of the films depend on morphological parameters, as preferable grain size or orientation. The bulk conduction also depends on the quality of the deposited films, changing from ohmic to trap-free or shallow trap SCLC and SCLC with an exponential distribution of traps. The hypothesis of using the electrical measurements as an indicator for film quality has been discussed. 相似文献
66.
M. M. I. HAMMOUDA I. G. EL-BATANONY H. E. M. SALLAM 《Fatigue & Fracture of Engineering Materials & Structures》2003,26(7):627-639
An understanding into the macro kinetic and kinematic behaviour of fretted surfaces is provided. Making use of a modified version of a previously developed in‐house two‐dimensional elastic–plastic finite element analysis numerically simulates flat contact pad fretting fatigue tests. Basic macro mechanics concepts are adopted to idealise two bodies with rough contact surfaces and loaded at two different sites with arbitrary axial loading profiles. A time scale factor is devised to recognise the earliest candidate out of the events possibly accommodated at each loading increment. The present analysis utilises a relevant experimental set up developed in the Structural Integrity Research Institute of the University of Sheffield as an application. Computational results accurate to within 1.2% and corresponding to one contact pad span and six constant normal loads acting individually with four amplitudes of two sinusoidal axial load cycles are presented. The present computations include (1) the development of the global and local normal and tangential reactions and relative sliding displacement acting along the fretting surfaces and (2) contact pad deformation, generated stress fields and plasticity development within the neighbouring region of the fretted area. 相似文献
67.
用气相色谱测定液氧中乙炔及其他碳氢化合物的含量 总被引:1,自引:1,他引:0
利用气相色谱浓缩法和气相色谱直接法测定液氧中乙炔及其他碳氢化合物含量。通过比较。用气相色谱直接法测定,方法简便,快捷,准确。 相似文献
68.
The aim of this study was to bring to the surface the strategic use of imitative processes in the context of a 2-route model: (a) direct imitation, used in reproducing new, meaningless actions, and (b) imitation based on stored semantic knowledge of familiar meaningful actions. Three experiments were carried out with healthy participants who reproduced meaningful and meaningless actions within an established time limit. The study investigated 3 factors that could potentially affect the selection of processes used for imitation: (a) the composition of the experimental list (blocked or mixed presentation), (b) the presence-absence of instructions (Experiments 1 and 2), and (c) the relative proportions of the stimuli (Experiment 3). Overall, the results suggest that each of these factors influences the selection of imitative strategies in healthy individuals with temporarily reduced capacities, as happens in the case of brain-damaged patients. (PsycINFO Database Record (c) 2010 APA, all rights reserved) 相似文献
69.
浅谈绿色生态住宅小区的给排水设计 总被引:5,自引:0,他引:5
介绍了设计绿色生态住宅小区的水环境系统各个子系统时应满足的水质、水量和应遵循的设计规范。提出了对节水设施、器具和绿色管材的选用原则 相似文献
70.
The effects of boiling Aqua Regia (AQ), N2/Cl2 plasma followed by AQ and O2 plasma followed by AQ surface treatments prior to Ni/Au (20 nm/20 nm) metallization to p-GaN:Mg (∼ 3 × 1017 cm− 3) have been investigated. N2/Cl2 plasma was employed in a bid to lower the Ga/N and O/Ga ratios of the GaN surface to improve the contact properties to p-GaN, while O2 plasma was employed as an alternative to incorporate O into the Ni/Au system. Results show that a low Ga/N ratio does not necessarily correspond to a better contact. The positive effect of O2 over N2 anneal is observed only for the AQ-treated sample, although the mechanisms responsible for its positive effect: NiO formation and Ni/Au layer-reversal were observed for all O2-annealed contacts. We conclude that the effect of O2 anneal on the Ni/Au contact is dependant on the p-GaN surface prior to metallization. 相似文献