On the thermal stability of xanthan gum

The thermal stability of xanthan gum in dilute aqueous solutions at 90°C is considered. The relative viscosity as a function of ageing time is discussed, and it has been found to depend on the polymer concentration and conformation as well as on the salt content. The effectiveness of a quencher demonstrates the existence of a free-radical process in the degradation. During ageing, the molecular weight first decreases by rapid random hydrolysis of the main chain and loss of the pyruvate and acetate substituents. Later, oligomers are formed corresponding to a breakdown of both the side chain and the main chain. The identification of cellodextrins in the oligomer pool demonstrates the second effect.     

电子陶瓷和器件的低温共烧技术

较系统地介绍了电子器件用低温共烧陶瓷(low temperature cofired ceramics,LTCCs)材料,探讨了其工艺中的若干问题。电子器件用低温共烧陶瓷材料包括:玻璃/陶瓷复合材料、结晶化玻璃、晶化玻璃/陶瓷复合材料以及液相烧结陶瓷,其中典型的和最为常用的LTCCs为玻璃/陶瓷(特别是氧化铝)复合材料。正在研究的一些陶瓷介质材料中,Bi基介质材料引起了人们的关注。玻璃/陶瓷复合材料的制备工艺中,应当着重关注和加深了解玻璃的流动性和结晶性、玻璃的起泡、玻璃和陶瓷颗粒间的反应、共烧材料的匹配等问题,从优选材料配方和优化工艺着手,从而获得优质可靠的材质和器件。     

高负荷下聚酯工艺参数的优化

介绍原 2 0万t/a装置增容到 2 4万t/a时的工艺参数优化。PTA平均粒径 95～ 110 μm ,n(EG) /n(PTA) =2 .6～ 2 .7,酯化液位 63 %～ 64 % ,温度 2 92～ 2 96℃ ;乙二醇锑催化剂 ,稳定EG、DEG量 ,选择TiO2 消光剂 ,滤除凝聚粒子 ;预缩聚温度 2 87～ 2 89℃ ,压力 2 .4～ 2 .8kPa,液位 42～ 48cm ;终缩聚温度 2 90～ 2 91℃ ,压力 2 .5～ 3 .0hPa,液位 60～ 62cm ,搅拌速度 2 .7r/min。     

乙烯二聚制高纯丁烯－1技术经济评价

本文对生产高纯度丁烯－１的Ａｌｐｈａｂｎｔｏｌ工艺进行了技术经济评价，认为该工艺条件简单、反应条件温和，而且投资少，所以很适合事在发展中国家应用。     

A novel shaft-less double suction mini pump

A novel double suction shaft-less mini pump was developed for heat control of small energy systems in this study.The mini pump impeller with an exit diameter of 40 mm was combined with the motor rotor supported by the hybrid dynamic bearing.The specific speed of the pump was 125 min-1 m3 min-1 m.The hydraulic performance of the pump was investigated experimen-tally under four rotational speeds.From the test results,it was recognized that the pump could provide a flow discharge of 5 L/min and head of 1.5 m,w...     

可监控EXE进程的Windows服务程序设计

EXE进程一旦意外停止,将给应用带来严重后果。该文基于微软的基础平台开发库设计了一个Windows服务程序,该服务程序在机器启动时自动运行指定EXE进程,在服务程序工作线程组中监控EXE进程运行状态,自动重启已停止进程,此服务程序可实现一个或多个EXE进程不间断运行。     

动态挖掘进程内在机制研究

针对动态挖掘进程内在运行机理,通过对动态挖掘进程中不同挖掘任务的优化分析以及动态挖掘进程和生物免疫过程之间的对比分析,提出了动态挖掘进程的eDMP机制;定义健壮型协调器,融合进化计算和免疫算法,设计了eDMP机制的实现方案;在理论分析和方案设计的基础上,给出了eDMP机制的一般流程。实验结果表明,eDMP机制及其实现方案在解决动态挖掘问题上有效、适用。     

Study of the physico–chemical characteristics and rheological behaviour of boehmite dispersions for dip-coating applications

Dispersions of a totally dispersible AlOOH powder have been studied. The effect of the initial composition has been studied to outline the reactions that determine the final rheological behaviour of the dispersions. The final viscosity and viscoelastic properties of the dispersions are determined by the sol–gel phenomena occurring during the ageing treatment. Gel formation is favoured by low water and high acid contents, while it is disfavoured by prolonged stirring. Gelling time from 48 h to 4 months has been observed depending on the initial composition.     

MC(Mid-Century)催化氧化过程的研究进展

介绍了MC催化氧化过程规律；从催化荆体系的改进、新型溶剂体系的开发、反应器构型和配套设施的改进、富氧氧化技术的开发等方面综述了近年来MC技术的发展；探讨了MC液相催化氧化技术应用范围的拓展以及MC液相催化氧化过程的发展方向。