Combustion of bulk density powder mixtures in a coflow of nitrogen gas: 3. The Ti-(Ti + 0.5C) layered system

Explored is the filtration combustion in Ti-(Ti + 0.5C) layered powder systems in a coflow of nitrogen gas. The presence/absence of nitrogen coflow through the layered system was found to drastically affect the character of wave propagation and structure/properties of product. The obtained data can be regarded as a basis for fabrication of new layered and composite materials in the mode of dynamic filtration combustion.      

劈刀和肋环夹持工况对超声键合换能系统电学特性的影响

通过实验分析了肋环夹持松紧度和劈刀存在两个因素对超声键合换能系统电学导纳特性的影响规律。对换能系统在悬挂有无劈刀和夹持8个松紧度等各个情况下进行谐振频率附近的导纳圆测量,确定换能系统等效电路各特征参数的变化情况。由实验结果的分析可知,劈刀的附加质量以及肋环松紧程度对换能系统谐振频率的影响不大,但劈刀的存在改变了换能系统的能量分布和耗散,是影响换能系统各特征参量的主要因素之一。这些结论有助于超声键合换能系统的优化。     

Measurement accuracy enhancements for wideband modulated signals

Time‐domain waveform measurements of wideband modulated signals, although attractive for communication systems modeling applications, have until now lacked the required accuracy for quantitative analysis. New developments described here enhance the accuracy of these measurements, enabling their application to communication system characterization and modeling. © 2003 Wiley Periodicals, Inc. Int J RF and Microwave CAE 13: 32–39, 2003.     

低渗透油藏回注污水的深度处理中试研究

为达到将油田采出水回注低渗透油藏的水质要求，在辽河油田进行含油污水处理试验：先在油田来水进入沉降罐前加入除油剂，使水中油的含量从20g／L降至约0．15g／L．悬浮物含量从10g／L降至3g／L左右；再采用气液多相泵气浮技术净水，使水中油的含量降至约0．005g／L。悬浮物含量降至约0．03g／L；进行初级过滤后，采用硅藻土动态膜超滤工艺精密过滤，最终使水中油和悬浮物含量均小于0．002g／L，悬浮物粒径控制在1μm左右。硅藻土动态膜超滤工艺集中了填充床过滤技术易再生和超滤膜过滤技术高水质的优点，运行费用低，应用前景很好。图6参11     

地层测试对油层改造选井选层的重要性及改造措施有效性评价

经对胜利油田近三年来典型井例测试资料分析评价及其增产措施效果分析认为，有三类地层压裂增油效果很好：地层物性相对较好的常压系统且存在严重堵塞的储层；物性较好的常压地层；高压低渗透储层。有两类地层酸化效果很好：灰岩、白云岩裂缝、低产低渗透储层；物性较好且存在严重污染堵塞的储层。其它地层压裂、酸化一般是无效的。     

低渗透储集层中油水层的地球化学综合判识——以济阳坳陷基山砂岩体为例

为了提高低渗透油藏油、水层识别的准确性，以济阳坳陷惠民凹陷基山砂岩体低渗透油藏为研究对象，探索以地球化学方法综合判识储集层流体性质的方法。以试油数据为参考，首先以热解定量方法初步评价，油层与油水同层、油水同层与水层的ST界限分别定为4．00mg／g及2．00mg／g；再以热解色谱定性方法将水层（或干层）与油层及油水同层明确区分；仍不能有效区分的油层及油水同层，则辅以热解参数表征的储集层变异系数进一步评价，变异系数高于0．3的为油水同层，低于0．3的为油层。具单一油源的多口井，可借助菲与二苯并噻吩（P／DBT）将油层及油水同层准确识别，P／DBT值大于12．5则为油层、小于等于12．5则为油水同层。对于相变较快，泥质薄层较多的低渗透油藏，利用热解参数S1／S2可评价储集层的真假隔层及油柱的纵向连通性。图4参17     

超低渗广谱油层保护技术在板深51区块的应用

板深51区块存在压力敏感地层，在非目的层井段存在大段高渗低压砂岩，而目的层又属于高压低渗地层，属于难采油气田。室内进行的砂床滤失量、砂床封堵带承压能力、岩心封堵带的承压能力及油气层保护效果实验表明，在超低渗钻井液中增加固相含量，能够提高超低渗透膜结构强度，提高地层承压能力，降低砂床侵入深度，增强保护油气层效果，而且有选择性地增加有用固相效果更佳。基于这一理论，研究成功了超低渗广谱屏蔽暂堵油层保护技术，并在板深51区块长22—15井和长23—17K井进行了试验应用。该技术的关键是依据地层特性确定复配暂堵剂。长22-15井和长23-17K井射孔后未经过压裂、酸化、排液处理，获自喷高产，尤其是长22-15井形成自喷油流，创油田单井试采产量最高记录。应用结果表明，超低渗广谱保护油气层钻井液技术封堵隔层的承压能力强，很大程度地提高了漏失层的承压能力和破裂压力，较好地解决了含多套压力层系长裸眼段钻井过程中发生的漏失、井喷、卡钻、油气层保护等技术难题。     

NMR characterization of penetrants in high permeability polymers

Spectra of xenon-129 sorbed into two high permeability polymers are reported. The polymers are the copolymer of tetrafluoroethylene and 2,2-bis(trifluoromethyl)-4,5-difluoro-1,3-dioxole as well as poly(1-trimethylsilyl-1-propyne). At room temperature, the xenon-129 shifts are smaller than in conventional glassy polymers. The smaller xenon-129 shift indicates the presence of larger sorption sites in high permeability polymers relative to conventional polymers. The temperature dependence of solubility in these polymers is drastically different from the behavior in conventional polymers. There is a rapid exponential increase in solubility in high permeability polymers as temperature decreases corresponding to a large negative enthalpy change on sorption and it is this increase in solubility which leads to a large increase in shift with decreasing temperature. Pulse field gradient (PFG) determinations of the self-diffusion constant are made for xenon, propane, pentane and a decafluoropentane in the copolymer. Rapid diffusion is observed as well as a dependence of the apparent diffusion constant on the time scale of the PFG experiment. The translational mobility of smaller simpler moieties depends less on the time scale or equivalently, the length scale of observation in the PFG NMR experiment. For larger, more complex species, the interconnectedness of high free volume domains plays a role in reducing the apparent diffusion constant as the time of measurement increases.     

低渗透挥发性油藏注烃类气驱室内实验研究

通过注烃类气驱实验研究，了解文留油田低渗透挥发性油藏注气开发的一般机理和开发特点。采用PVT分析方法分析地层流体的物理性质、注入溶剂的组份；通过细管实验研究地层流体同注入溶剂在130℃时的最小混相压力；长岩心驱替实验分析气驱、水驱、水气交替注气的采收率、压力的变化规律。细管实验研究表明，最小混相压力为47．1MPa，长岩心注天然气驱替实验表现出近混相的特征。天然气驱注气压力低，采收率高，适合于文南油田低渗透挥发性油藏。     

透水性沥青面层材料设计新法及应用

本文提出了一种根据主骨料空隙率设计透水性面层沥青混合料级配的新方法，根据这一方法设计的透水性沥青面层具有良好的路面使用功能，应用前景广阔。