Evaluation of electrochemical properties of antibacterial ZnO layers deposited to 316LVM steel using atomic layer deposition

The presence of a biofilm can lead to the disappearance of the surrounding bone tissue and, as a result, disturb the osseointegration process. Unfortunately, both in the case of instability of the implant and long-term bacterial infections, there is often a need for reoperation as well as replacement of the implant, which in turn is associated with huge costs, but most of all discomfort for the patient associated with long-term hospitalization. In order to limit this unfavorable process, the physicochemical properties of the surface layer of implants are indicated. Therefore, the paper proposes applying a layer with antibacterial effect on the surface of 316LVM steel used in bone surgery. As part of the work, the ZnO layer was applied using the atomic layer deposition method with different parameters of the application process (different number of cycles at constant temperature). In the first stage, pitting corrosion resistance tests were carried out using the potentiodynamic method and studies using electrochemical impedance spectroscopy. The surface morphology tests using a scanning electron microscope were also complemented. Obtained results may form the basis for the development of more detailed criteria for the assessment of the final quality of medical devices used in the skeletal system.     

Evolution of microstructure and room temperature tensile properties in aluminum-bearing high strength steel processed by ultrafast cooling

An aluminum-bearing high strength steel with relatively high precipitation hardening was fabricated by lowering coiling temperature to 627 °C. The influence of coiling temperature on microstructure evolution and precipitation behavior was comprehensively investigated by means of scanning electron microscopy, electron back-scatter diffraction and transmission electron microscopy. Both yield strength and tensile strength can be increased by around 100 MPa through decreasing coiling temperature to 627 °C, whereas there is nearly no deterioration in ductility. In addition, The grain boundary precipitation of (Fe, Cr, Mn)_xC_y-type carbides can be effectively suppressed by lowering coiling temperature. Regardless of coiling temperature, both interphase precipitation consisting of curved and planar shape and random precipitation can be observed. Moreover, the sheet spacing can be refined from 29 nm–47 nm to 18 nm–27 nm by lowering coiling temperature from 721 °C to 627 °C. This small sheet spacing provides a greater precipitation hardening. Compared with a coiling temperature of 721 °C, the precipitation hardening can be increased by around 100 MPa for a coiling temperature of 627 °C.     

Modified laser beam welding of aluminum‐silicon coated 22MnB5

Press hardened 22MnB5 is an excellent structural material, but there are several issues when it comes to welding. Especially in the case of overlap joint laser welding, the most severe issue is precipitation of the aluminium silicon (AlSi) coating at the fusion line. If the coating remains on the sheets, an ultimate strength of 20 kN with a crack initiation at the fusion line is reached in tensile tests instead of 30 kN with a crack initiation in the heat affected zone (HAZ) when the coating is removed prior to welding. In the presented work, the influence of coating on the material properties as well as the structure of the precipitation at the fusion line are examined and discussed. It is stated that the precipitation does not consist of Al_xFe_y intermetallic phases, but of an iron, aluminium and silicon solid solution. The fractured surfaces of tensile tests show brittle behavior for the precipitation and ductile behavior for areas where the crack propagated through the steel. A modified beam oscillation in the shape of a recumbent “8” in welding direction is introduced. It was possible to increase the ultimate strength by 10 kN and nearly double the possible elongation.     

Fatigue crack propagation behavior in AISI 304 steel welded joints for cold‐stretched liquefied natural gas (LNG) storage tank at cryogenic temperatures

AISI304 steel welded joints are used in cold‐stretched liquefied natural gas (LNG) storage tanks used for storing and transporting of liquefied gases. Compared with a conventional liquefied natural gas storage tank, a cold‐stretched liquefied natural gas storage tank has many advantages such as reduced thickness, light weight, low cost and low energy consumption. However, liquefied natural gas storage tanks can be subjected to alternative loads at cryogenic temperatures; thus, it is important to investigate the fatigue crack propagation behavior in AISI 304 steel welded joints at cryogenic temperatures. Specimens were machined from a cold‐stretched liquefied natural gas storage tank with a welding structure. The crack length was determined using compliance method and confirmed by examination with traveling microscope. Fatigue crack propagation rates were evaluated at various stress ratios and temperatures. The fatigue crack growth rate of all specimens a little appears the effect of stress ratio, but it has a great influence at a cryogenic temperature. The fatigue crack growth rate of longitudinal welded joint is the fastest at room and cryogenic temperature. Fracture mechanism in the specimen is examined using a scanning electron microscope.     

Numerische Analyse geschweißter Verbindungen von Duplexstahl und Quarzglas

Numerical analysis of welded joints between duplex steel and quartz glass. Welded joints are a vital element in structural engineering. Originating from conventional carbon steel welding in construction, recent advancements in welding technology now allow the joint of modern high‐strength steel and glass materials. With today's methods, an analysis of the welded joints' structural behaviour can be conducted by experiment, as well as by numerical analysis. Particularly for the numeric analysis, capturing the non‐linear thermal and mechanical properties of the materials is important, in order to allow a realistic determination of temperature, microstructure and residual stresses for different types of joints. Simulations of multi‐layered weld joint on duplex steel show, that a targeted heat treatment during MAG‐welding by variation of the welding parameters achieves a beneficial ratio between ferrite and austenite which, for example, ensures a high resistance of the weld to corrosion. The material quartz glass can generally be welded as butt‐weld with a CO₂‐laser. The simulations of a welded joint of a plate and a pipe show, that an optimization of the welding technology of preheat laser beam and welding laser beam is necessary, in order to reduce the thermal impact during the welding process, as well as residual stress in the joint. At the Department of Steel Structures at the Bauhaus‐Universität Weimar, numerical simulations of welded joints between steel and glass materials are a current and topical research focus.