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11.
Nuclear magnetic resonance (n.m.r.) studies of 19F nuclei in a random copolymer of vinylidene fluoride and trifluoroethylene were performed at 9.14 MHz and 20.0 MHz. The free induction decays (FIDs) were analysed in terms of two T2 components attributed to the amorphous and crystalline portions of the polymer. The changes in crystallinity as well as the effects of the ferroelectric transition were observed during cycles of heating and cooling between 20°C and 140°C. The crystalline component of the FID lengthens by a factor of 2 at 100°C on heating and decreases by this factor at 60°C on cooling, thus exhibiting the thermal hysteresis of this ferroelectric transition. The spin-lattice relaxation was also investigated. From measurements at 9.14 MHz the observed longitudinal relaxation time T1 appears to be dominated by the dynamics of the amorphous phase and exhibits no anomaly through the phase transition. However, from measurements at 20 MHz, well defined minima of T1 were observed, which are associated with the ferroelectric transition (especially after repeated annealing of the samples). Results are discussed in terms of the crystalline phase structure, which appears dynamically disordered above the ferroelectric phase transition. An analogy is considered with the plastic phase transitions encountered in molecular crystals. 相似文献
12.
脉冲激光沉积SrBi2Ta2O9铁电薄膜电容特性研究 总被引:2,自引:0,他引:2
用PLD方法成功地制备了SBT铁电薄膜,并制作成Pt/SBT/Pt薄膜电容器。SBT薄膜的晶面取向以(008)和(115)为主。在5V电压下,极化反转,并且得到较饱和的电滞回线,剩余极化强度和矫顽电场分别为84μC/cm2和57kv/cm。IV特性测试显示两个对称的双稳峰,并得到零电压下,面积为314×104μm2,厚度为035μm的电容器,电容约为560pF,介电常数约为600。疲劳测试表明Pt/SBT/Pt具有优良的抗疲劳特性。 相似文献
13.
铁电致冷材料及其应用 总被引:4,自引:1,他引:3
利用铁电材料的电热效应(即逆热释电效应)可以制作新型致冷器。近年的研究进展表明,铁电致冷有可能发展成为一种新型的室温致冷技术。本文扼要介绍了铁电致冷的基本原理、可行性,以及铁电致冷材料和相关技术的发展,并展望了铁电致冷材料的发展前景。 相似文献
14.
The electroclinic effect in the smectic A phase of ferroelectric liquid crystals is a sensitive probe for measuring the soft
mode response near the A-C* transition point. It is possible to evaluate several coefficients of the Landau theory describing
the A-C* transition by simultaneously measuring the frequency dependence of both the optical signal and the current through
the sample. We have made such measurements on a couple of homologous series [2S,3S]-4′-(2-chloro-3-methyl pentanoyloxy) phenyl-trans-4″-n alkoxy cinnamates synthesized in our labortory. The results show that the Landau meanfield theory is adequate to describe
the A-C* phase transition in these compounds.
Presented at the 15th International Liquid Crystal Conference, Budapest, 3–8 July 1994. 相似文献
15.
16.
驻极体声传感器及其储电材料的现状 总被引:1,自引:0,他引:1
综述了驻极体声传感器及其储电材料近年来的迅猛发展。传统的FEP(tetrafluoroethylene—hexa—fluoropropylene copolymer)极体电容式声传感器及以铁电聚合物PVDF(poly vinylidene fluoride)家族为芯片的声传感器和超声抉能器仍焕发着青春活力。Si基微型驻极体声传感器的理论和实验研究已经日趋成熟,而用空间电荷型多孔聚合物驻极体压电薄膜为芯片可望研制出新一代声电和电声传感器、压力传感器和驱动器。 相似文献
17.
Storage effects on nutritional quality of commonly consumed cereal grains are studied. Freshly harvested wheat, maize and rice grains were stored at 10, 25 and 45 °C for six months. A significant decrease in pH and an increase in titratable acidity was observed during storage of these three cereal grains at 25 and 45 °C. A gradual decline in moisture, total available lysine and thiamine contents was observed during storage. Total available lysine contents decreased by 6.50% and 18.5% in wheat, 14.3% and 20.7% in maize and 23.7% and 34.2% in rice during six months of storage at 25 and 45 °C, respectively. Six month’s storage of rice, maize and wheat grains at 25 and 45 °C resulted in reduction of thiamine contents by 16.7% and 29.2%, 17.2% and 24.1% and 21.4% and 29.5%, respectively. About 36.4–44.4% decrease in total soluble sugars at 45 °C and 9.30–31.8% increase in total soluble sugars were observed at 10 and 25 °C during six months storage of these cereal grains. Protein and starch digestibilities of cereal grains also deceased during six months of storage at 25 and 45 °C. No significant change in nutritional quality was observed during storage of cereal grains at 10 °C. 相似文献
18.
Precusors to the YBa2 Cu3 O7-δ material were prepared by both the oxalate precipitation method and conventional ceramic processing. Second-phase grains were observed to develop on the exposed fracture surface during annealing at 500° to 600°C in an ambient atmosphere. The second-phase grains were identified to be BaCO3 using EDX and XRD. The liquid phase, which was formed because of local chemical inhomogeneity in the Y-Ba-Cu-O system, contributed to the formation of second-phase grains as a source of Ba. 相似文献
19.
不锈钢上激光熔敷涂层结构特征与质量研究 总被引:1,自引:0,他引:1
采用5kW连续CO2激光器对经等离子喷涂的NiCoCrAlY结合层和ZrO2陶瓷层进行二次重熔处理,并利用金相显微镜、扫描电镜、电子探针和显微硬度计对激光熔敷涂层进行了显微结构、元素分布以及显微硬度观察与测试,结果表明:多道搭接工艺能降低熔敷涂层气孔率,ZrO2陶瓷层稀释度低,与基体结合完好,并观察到NiCoCrAlY合金层中存在明显的对流图案,加入了TiO2-Al-Ti添加剂的ZrO2陶瓷层激光重熔后得到了无裂纹的定向生长柱状晶,并且呈现一次枝晶平均间距为2.3μm的表层和平均间距为3.8μm的次表层结构。 相似文献
20.
本文研究了用金属有机物热发解法制备PLT8薄膜的工艺过程和基片对薄膜结构的影响,并且给出了铁电性能的测量结果。 相似文献