新型抗温抗盐降滤失剂FHJ-10的研制

以AM、ClCH2COOH及AMPS等为单体,并复合高温稳定剂D(主要成分为柠檬酸盐),制备了一种新型抗温抗盐降滤失剂FHJ-10,并对其性能进行了评价.实验结果表明,降滤失剂FHJ-10的抗温性能可以达到130 ℃,抗盐可达到25%,具有良好的应用前景.     

光热电站长轴多级熔盐泵模态抗震计算与分析

太阳能光热电站熔盐泵(文中简称熔盐泵)结构特殊、运行环境恶劣,对安全和性能要求很高,模态计算、抗震分析是熔盐泵安全评定的重要环节.使用ANSYS WORKBENCH平台,在充分考虑自重、熔盐泵附加质量、平台约束刚度矩阵等因素的条件下计算不同熔盐液位工况下熔盐泵的模态特性以及对核电安全停堆级地震(SSE)的响应情况,并采...     

盐业钻井大队职工培训初探

随着知识经济的到来,职工培训在组织发展中扮演着越来越重要的角色。本文针对盐业钻井大队职工培训的现状,进行了问题分析,提出了建立学习型组织、完善的培训体系和畅通的运行机制的建议,最后强调了制定培训计划应从加强培训需求性的调查研究、加强组织培训的协调性等五个方面把握。     

Synthesis of K6Ta10.8O30 nanowires by molten salt technique

The synthesis of single crystalline K₆Ta_10.8O₃₀ nanowires by molten salt method was reported for the first time. X-ray diffraction results indicated that the as-prepared products were pure phase K₆Ta_10.8O₃₀. Scanning electron microscopy and transmission electron microscopy results showed that the products consisted of wire-like nanostructures with 100-300 nm in diameter and several micrometers in length. High resolution electron microscopy and selected area electron diffraction results indicated that the K₆Ta_10.8O₃₀ nanowires were single crystalline with a growth direction of [0 0 1]. The ultraviolet-visible diffuse reflectance measurement showed that the band gap of the nanowires was about 4.1 eV. The effects of reaction temperature, time, and weight ratio of the precursor (mixture of K₂CO₃ and Ta₂O₅) to KCl salt on the morphology of the products were investigated.     

三聚氰酸为基的2,4,6-三氧-[1,3,5]三嗪烷-1-三氨基胍盐的合成、晶体结构和热性能（英）

以三聚氰酸钠(CANa)和三氨基胍盐酸盐(TAG-HCl)为原料,通过一步复分解反应制备了一种富氮含能化合物——2,4,6-三氧-[1,3,5]三嗪烷-1-三氨基胍盐(1),收率91%.采用X-射线单晶衍射、UV-Vis、FTIR、1H NMR以及元素分析等对产物进行了结构表征.计算了产物的生成焓和爆轰参数.通过差示扫描量热法(DSC,10 K·min-1)和热重-傅里叶变换红外光谱联用分析了其热稳定性、非等温热分解动力学和热分解过程.通过落锤法测试了产物的撞击感度.结果表明,化合物1的晶体为单斜晶系,P21/n空间群,计算密度为1.676 g·cm-3,生成焓为327.9 kJ·mol-1,爆速为7900 m·s-1,爆压为26.5 GPa.化合物具1有良好的热稳定性,分解峰值温度为538.9 K,提出了N2气氛下可能的热分解机理.且化合物1对撞击非常钝感,撞击感度大于60 J,优于TATB(50 J).     

单氟磷酸钠对天然碳化高炉矿渣砂浆的影响

研究了10%的单氟磷酸钠溶液作为表面处理剂对碳化高炉矿渣水泥砂浆耐久性的影响。砂浆养护10d后或暴露在自然环境中1a后,进行表面处理,这2种处理方式分别称为前处理与后处理。通常情况下,砂浆在碳化侵蚀后其微观结构被严重破坏。处理后的砂浆经碳化后的微观结构大为改观。试验结果表明:处理后的碳化高炉矿渣水泥砂浆的抗冻融循环能力得到了很大提高。     

Research on corrosion performance of 6061 aluminum alloy in salt spray environment

Salt spray corrosion test was carried out on 6061 aluminum alloy, and quasi-static tensile test at room temperature was carried out on the sample with universal testing machine. The effect of salt spray corrosion on the mechanical properties of 6061 aluminum alloy was studied by scanning electron microscope (SEM), energy dispersive spectrometer (EDS) and electrochemistry. The corrosion rate of 6061 aluminum alloy was quantitatively characterized by different corrosion parameters. It was found that local corrosion of 6061 aluminum alloy occurred in salt spray environment, mainly pitting corrosion and intergranular corrosion. With the increase of corrosion time, the polarization resistance of 6061 aluminum alloy decreases, and the corrosion rate significantly increases. The average corrosion rate and the maximum corrosion rate of 6061 aluminum alloy were characterized by corrosion weight loss and corrosion pit depth. And they can be transformed into each other. The mechanical properties of 6061 aluminum alloy were mainly affected by the depth of corrosion pit. With the increase of corrosion time, the tensile strength and fracture strain decreased, resulting in poor plasticity of the sample. At the same time, the change of elongation of 6061 aluminum alloy can be accurately predicted by the depth of corrosion pit.     

Influence of nitriding on corrosion resistance of martensitic X17CrNi16‐2 stainless steel

Nitriding increases surface hardness and improves wear resistance of stainless steels. However, nitriding can sometimes reduce their corrosion resistance. In this paper, the influence of nitriding on the corrosion resistance of martensitic stainless steel was investigated. Plasma nitriding at 440 °C and 525 °C and salt bath nitrocarburizing were carried out on X17CrNi16‐2 stainless steel. Microhardness profiles of the obtained nitrided layers were examined. Phase composition analysis and quantitative depth profile analysis of the nitrided layers were preformed by X‐ray diffraction (XRD) and glow‐discharge optical emission spectrometry (GD‐OES), respectively. Corrosion behaviour was evaluated by immersion test in 1% HCl, salt spray test in 5% NaCl and electrochemical corrosion tests in 3.5% NaCl aqueous solution. Results show that salt bath nitrocarburizing, as well as plasma nitriding at low temperature, increased microhardness without significantly reducing corrosion resistance. Plasma nitriding at a higher temperature increased the corrosion tendency of the X17CrNi16‐2 steel.     

基于窗口的自适应中值滤波算法

滤波窗口是影响椒盐噪声滤除效果的重要因素。针对自适应中值滤波算法(RAMF)的不足,提出了一种基于窗口的自适应中值滤波算法。该算法分为噪声的检测和滤除两部分。在噪声检测部分,主要通过混合窗口检测出准噪声点,将其用窗口中值代替,而其余信号点保持不变。重复此方法,直至所有的准噪声点处理完毕。然后,在噪声滤除部分,主要根据噪声密度选择合适的最大滤波窗口半径,进而实现噪声滤除。最后,为验证算法的有效性开展了仿真研究,仿真结果表明本算法对椒盐噪声的滤除具有很好的效果,增强了图像的清晰度。