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101.
Characterization of polyhydroxyalkanoates synthesized in activated sludge using three carbon sources
张艳萍 《北京理工大学学报(英文版)》2016,25(3):429-434
Polyhydroxyalkanoates(PHAs) were synthesized in activated sludge using three types of carbon sources (sodium acetate,sodium propionate and sodium butyrate), and their characterization were studied. It was shown that the content of PHA synthesized by microorganisms in activated sludge were different. The biggest synthetic amount up to 36.7% of VSS was obtained when sodium acetate was used as carbon source. The polymer yield was lower when using sodium propionate as the carbon source than when using others, with 25.1% of VSS, while resulted in an increase of hydroxyvalerate(HV) units produced. The structure and thermal properties of extracted biopolymers were analyzed by scanning electron microscope (SEM), Fourier transform infrared spectroscopy (FTIR) and themo-gravimetry (TG). 相似文献
102.
103.
本文介绍了山东电网一起红外测温发现的500kV复合绝缘子外护套损坏案例,分析了损坏的原因,阐述了红外测温带电测试技术诊断复合绝缘子内部缺陷的机理和判别方法,测温结果及实验室试验表明红外成像法能够有效地检测出缺陷复合绝缘子,并给出了提高复合绝缘子安全运行水平的措施和建议。 相似文献
104.
文章针对一起由红外热成像仪发现的氧化锌避雷器故障,利用在线监测、红外图谱分析、带电测试等多种检测手段对其进行诊断分析,通过不同检测结果的对比,最终确定避雷器故障发生的原因。不同检测手段的灵敏度差异,对电力设备维护有一定的指导意义。 相似文献
105.
为研究家用冰箱储藏室中挥发性有机化合物(VOCs)的释放量及主要来源,采用气相色谱–质谱法对工作状态下冰箱储藏室的VOCs含量进行检测;利用傅里叶变换红外光谱仪对冷藏室的物料进行成分分析,同时用密封舱法探究冷藏室不同物料对VOCs含量贡献。结果表明,冰箱冷藏室物料中发泡聚苯乙烯风道泡沫释放的总挥发性有机化合物(TVOC)、正戊烷及异戊烷最多,是造成异味的关键性物料,而正戊烷、异戊烷是冰箱异味的主要成分。聚氯乙烯门封条对异味的贡献也较大,通用聚苯乙烯抽屉体贡献的VOCs种类最多;在工作状态下,随着密闭时间的增加,冰箱储藏室的VOCs的种类及含量增加,但苯、甲苯、二甲苯、TVOC及戊烷类的含量均未超过国家标准。储藏室异戊烷含量较高,是冰箱的异味的主要来源。 相似文献
106.
107.
J. D. Haman A. A. Boulware L. C. Lucas D. E. Crawmer 《Journal of Thermal Spray Technology》1995,4(2):179-184
Plasma spraying is used to produce most commercially available bioceramic coatings for dental implants; however, these coatings
still contain some inadequacies. Two types of coatings produced by the high- velocity oxyfuel (HVOF) combustion spray process
using commercially available hydroxyapatite (HA) and fluorapatite (FA) powders sprayed onto titanium were characterized to
determine whether this relatively new coating process can be applied to bioceramic coatings. Diffuse reflectance Fourier transform
infrared (FTIR) spectroscopy, x- ray diffraction (XRD), and scanning electron microscopy (SEM) were used to characterize the
composition, microstructure, and morphology of the coatings. The XRD and FTIR techniques revealed an apatitic structure for
both HA and FA coatings. However, XRD patterns indicated some loss in crystallinity of the coatings due to the spraying process.
Results from FTIR showed a loss in the intensity of the OH∼ and F∼ groups due to HVOF spraying; the phosphate groups, however, were still present. Analysis by SEM showed a coating morphology
similar to that obtained with plasma spraying, with complete coverage of the titanium substrate. Interfacial SEM studies revealed
an excellent coating-to-substrate apposition. These results indicate that with further optimization the HVOF thermal spray
process may offer another method for producing bioceramic coatings. 相似文献
108.
J. H. Li P. Deshpande R. Y. Lin 《Journal of Materials Engineering and Performance》2004,13(4):445-450
The objective of this study is to investigate an innovative infrared (IR) technique to enhance adhesion of electroplated copper
(Cu) on Ti-6Al-4V without dichromate dipping. The ultimate goal is to develop a Cu coating process on Ti-6Al-4V without hazardous
hexavalent chromium (Cr) solution treatments. Cu coatings of around 50 μm were electroplated on Ti-6Al-4V specimens at a current
density of 0.03 A/cm2 in an acidic Cu solution. To improve adhesion of coatings, IR heat treatments were performed on the Cu-coated samples at
different temperatures and durations: 860 °C for 600 s and 875 °C for 20–120 s. This process was accomplished in an attempt
to replace the use of dichromate dipping before electroplating. For samples heat treated at 860 °C, no bonding existed, even
after 600 s. It is believed that solid-state diffusion prevailed at 860 °C and that 600 s was not enough for sufficient diffusion
to occur. Adhesion was poor when samples were heat treated at 875 °C for 20 s. Excellent adhesion was observed when the heat
treatment holding time was increased to 40 s. For 90 s, the surface appearance of coatings partially changed from Cu-colored
to a grayish color. There was no Cu left on the surface after a 120 s heat treatment. From optical microscopic observations
on sample cross sections, an interlayer between the Cu and Ti-6Al-4V formed when heat treated at 875 °C for 40 s and longer.
The interlayer thickness increased as the holding time increased, until depletion of Cu. The sheet resistivity of coated specimens
was on the order of pure Cu for samples heat treated at 875 °C and less than 90 s. During the 875 °C heat treatment, the following
occurred: solid-state diffusion of Cu in Ti-6Al-4V, formation of eutectic solutions, dissolution of Cu and Ti-6Al-4V into
the liquid phase, and the formation of intermetallic compounds. The lowest eutectic temperature of 875 °C played a key role
in this innovative process of Cu coating on Ti-6Al-4V.
This paper was presented at the 2nd International Surface Engineering Congress sponsored by ASM International, on September
15–17, 2003, in Indianapolis, Indiana and appears on pp. 403–10 of the Proceedings. 相似文献
109.
基于不同氧化物与碳的结合能不同,与碳的还原反应在不同的分析条件下具有先后次序,用脉冲红外氧化物夹杂分析仪,对4μm的烧结Nd Fe B永磁材料粉末的氧化行为进行了方法研究。实验结果表明,通过合理设置参数,选用跟踪升温模式,可以快速分离Nd Fe B永磁材料粉末中的不同氧化物,并可以通过加权方法进行定性验证。 相似文献
110.
HUANG Yi LIN Xuerong XU Jun Institute of Metal Research Academia Sinica Shenyang China HUANG Yi Associate Professor Institute of Metal Research Academia Sinica Shenyang China 《金属学报(英文版)》1990,3(10):277-283
The infrared emission of a high pressure vessel steel and two thin wall pressure vessel modelshave been investigated by use of vibro-thermography.The experimental infrared cracklengths were found to be agreed closely with the optical values during fatigue process.A possi-ble nondestructive testing method used to evaluate the pressure vessel has been given. 相似文献