低温吸附法脱除一氧化碳中甲烷的实验研究

在液氮温度下,采用吸附剂CNA X进行低温脱甲烷动态吸附实验,结果表明CNA X在液氮温度下可以将一氧化碳中0 1%左右的甲烷脱除到10×10-6。     

压力计探测液面法探讨

针对油田地质特征复杂，易结蜡，测试中易出现假液面等情况，为准确快速测得液面资料，提出压力计测试液面法。该方法可作为回声仪测液面方法的有效补充。     

液晶电控效应的实验研究

详细阐述了液晶的电光效应,介绍了利用分光光度计测量液晶透射比的方法。通过改变加在液晶盒上的电压大小及其频率高低,详细测量了液晶的透射比。通过做图分析了液晶的电控双折射效应,得出液晶的透射比随所加电压的大小和频率的高低而变化,以及液晶的阈值电压随频率的增高而减小的规律,这对液晶器件的设计与研究均具有一定的参考价值。     

掺杂铁电纳米粉的液晶的电光特性

铁电纳米粒子悬浮在向列相液晶母体中，增强介电各向异性，而且对施加的电场信号敏感。本文也展示了纳米粒子对所述复合材料可实现的总的相变的作用。这种方法也许可应用于设计新型显示材料。     

Al-Cu双金属复合结构的扩散连接试验研究

应用扩散连方法进行了Al-Cu双金属复合结构的试验研究，比较了不同的焊接工艺，材料组合以及母材状态情况Al合金与Cu的连接性，观察了接头区域的微观组织结构，研究表明，固相扩散连接是一种适用于异种材料连接的有效方法，通过在连接区域形成Al-Cu金属间化合物，达到Al和Cu的有效连接，材料组合，母材原始状态以及连接工艺参数对Al合金与Cu的扩散连接存在着明显的影响。表面镀Ni工艺不但能够有效阻止Al和Cu之间形成脆性相，而且Al和Ni之间形成了良好的扩散连接，改善了接头性能。     

电控平行排列液晶光栅的光衍射特性研究

对电控平行液晶光栅的理论进行了分析,并配以结构原理图。通过对平行排列及90°扭曲排列液晶指向矢的计算,得出液晶盒中相应的折射率、相位差与电压之间的关系图,两者经比较证明平行排列更具适用性,并在实验中观测到了平行排列液晶光栅衍射特性与电压的关系。     

棒状液晶分子相变问题的机械旋转模型研究

综述一种关于棒状液晶材料的分子结构与液晶相的相关关系的研究成果。介绍了有关液晶分子的机械旋转模型。该模型将液晶分子视作一种高速旋转的转子,通过分子参数计算,对液晶材料的相变温度和分子结构之间的关系给出了一种全新的解释。最新研究表明,含氟三苯液晶材料的分子结构中存在slim和fat现象,能够对液晶材料的相变进行合理解释。该模型能够通过简单的模型方法对新型液晶材料的分子设计与合成提供有用的信息。     

Plastic deformation of bcc metal thin foils without dislocation

Heavy plastic deformation of fcc metal thin foils to fracture has been found recently to proceed without involving dislocations, and it results in the formation of high density of vacancy clusters. Thin foil specimens of bcc metals such as V and Mo were plastically deformed to fracture in in situ elongation experiments under an electron microscope. Morphology of thinning and fracture was found to be similar to fcc metals, and no dislocation was observed during heavy deformation. Electron diffraction analysis at the tip of a crack during deformation confirmed a large elastic deformation of up to 5%. Unlike in fcc metal thin foil specimens, point defect clusters were not observed near fractured tips. This difference is attributed to the difference in vacancy reaction, though the deformation in bcc metals without dislocation most likely does produce vacancies.     

Rheology in Processing of in Situ Composites of Polypropylene and Low Melting Poing Metals

The low melting point metallic tin powder or alloy of tin and lead was blended with polypropy-lene. A kind of in situ composite has been prepared. The variations of torque were studied when the composites were mixed in Haake torque rheogeniometer. By way of capillary extrusion, effects upon rheology of the in situ com-posites of the low melting point metals (LMPM) and coupling agent for their different variety and content, were investigated. From flow curves, the results indicate that in situ composites mixed with the LMPM are a kind of pseudoplastic fluid. If the LMPM were melted, the higher the content of the LMPM , the lower apparent viscosity of composites. Meanwhile, when the coupling agent is added into composites, the viscosity of composite will go up first and drop then. This shows that the LMPM have a promoter flow action on the polypropylene.     

Transport of chromium(VI) through a Cyanex 921‐supported liquid membrane from HCl solutions

The transport of chromium(VI) through a flat‐sheet supported liquid membrane containing Cyanex 921 as a carrier has been investigated. The permeation of the metal is investigated as a function of various experimental variables: hydrodynamic conditions, concentration of chromium(VI) and HCl in the feed phase, carrier concentration and diluent in the membrane and strippant concentration in the stripping phase. The mass transfer coefficient and the thickness of the aqueous boundary layer were calculated from the experimental data. Furthermore, the selectivity of Cyanex 921‐based flat‐sheet supported liquid membrane towards different metal ions and the behaviour of the system against other carriers are presented. Copyright © 2003 Society of Chemical Industry