溶胶玻璃原位合成碳纳米管的研究

目前，碳纳米管的各种制备方法如电弧法、激光消融法、催化热解法及化学气相沉积法等，都是在500～3500℃温度范围内经由气固相接触表面合成的，从而使反应的深度和广度都受到了限制．利用固相热解法尝试在溶胶玻璃中原位合成碳纳米管，该方法可以使反应在整个固相范围内同时发生，而不只是在气固相的表面合成．在制备样品的过程中采用了溶胶-凝胶法，成功地将碳源(乙酰丙酮)和催化剂(硝酸钴)均匀地分散在SiO，溶胶玻璃中，制备了纳米级的复合材料．另外，选择了乙酰丙酮作碳源，将碳纳米管的合成温度降到了400℃，实现了在低温固相条件下原位合成碳纳米管．最后通过TEM对生成的纳米碳管进行表征．     

Q345C低合金高强度结构钢板的试制

介绍采用氧气顶吹转炉→吹氩喂丝→板坯连铸→控制轧制生产Q345C低合金高强度结构钢板的生产工艺。通过对化学成分的合理设计及制订适合该厂冶炼、连铸、轧制的工艺，采取微合金化和控轧控冷相结合的有效技术措施，提高钢板的综合性能，特别是低温冲击韧性。生产的Q345C钢板，其产品质量完全符合GB／T1591—94标准要求。     

Low-temperature X-ray microanalysis of the differentiating vascular tissue in root tips of Lemna minor L

The fracture faces of bulk-frozen tissue offer a number of advantages for the analysis of diffusible elements. They are easy to prepare, remain uncontaminated, and, unlike most frozen-hydrated sections, can be shown to exist in a fully hydrated state throughout examination and analysis. Root tips of Lemna minor briefly treated with a polymeric cryoprotectant are quench frozen in melting nitrogen. Fractures are prepared using the AMRAY Biochamber, lightly etched if necessary to reveal surface detail and carbon coated while maintaining the specimen at 110 K. The frozen-hydrated fracture faces are analysed at 110 K using the P/B ratio method which is less sensitive to changes in surface geometry and variations in beam current. The method has been used to investigate the distribution of seven elements (Na+, Mg⁺⁺, P, S, Cl^?, K+ and Ca⁺⁺) in the developing vascular tissue of the root tip. The microprobe can measure relative elemental ratios at the cellular level and the results from this present study reveal important variations in different parts of the root. The younger, more actively dividing cells, appear to have a slightly higher concentration of diffusible ions in comparison to the somewhat older tissues which have begun to differentiate into what are presumed to be functional vascular elements.     

小流量灰浆泵组合密封设计

用于输送含有细小颗粒流体的小流量（0．5～5t／h）氢氧化钙浆液泵的机械密封，极易被溶液中含有的固体颗粒磨损而丧失密封性能。针对这一问题，提出了一种背叶片加上橡胶波纹管机械密封组合的密封结构，并辅之以溢流结构来保护电机，从而解决了灰浆泵的密封问题，延长了泵的使用寿命，使泵装置的体积大大缩小，且易于维修。本文阐述了这种组合密封结构的原理及尺寸设计。     

考虑动作误差的低励限制与失磁保护定值配合方法研究

关于低励限制与失磁保护定值匹配的研究多聚焦于将其转换到同一功率平面或阻抗平面进行校核的方法,鲜有文献考虑实际装置动作特性对定值匹配结果的影响。该文从理论上详细分析各参数变化对失磁保护和低励限制的影响,提出基于装置动作误差的低励限制与失磁保护定值匹配校核原则,并论述定值失配时的定值调整方法,为当前各发电厂开展低励限制与失磁保护定值校核及整定提供了有效指导原则。     

Shut-cut nitrification characteristics of aerobic granule in a sequencing batch airlift reactor at low temperature

To investigate the shut-cut nitrification characteristics of aerobic granule,an aerobic granular sequencing batch airlift reactor(AG-SBAR) was carried out with mixed carbon sources of sodium acetate and glucose at 10±1 ℃.Results indicated that ammonia oxidizing bacteria was accumulated inside the aerobic granules and the reactor performed stably with shut-cut nitrification for a long term at low temperature.During the stable operation period,the effluent ammonia nitrogen concentration was maintained at 13.6 mg/L without nitrate and nitrite when the COD/N ratio was 20:1.However,the effluent concentration of ammonia nitrogen was below 0.5 mg/L with effluent nitrosation ratio of 96.7% on average when the COD/N ratio was reduced to 15:1 and 10:1.And the effluent phosphorus concentration was less than 0.4 mg/L during the stable period with the sludge retention time of 30 d.The phosphorus removal efficiency was not strongly influenced by the adjustment of COD/N ratio in this experiment.The removal efficiencies for COD,NH4+-N and PO43--P were 91.3%-94.6%,97.9%-99.7% and 97.1%-99.5%,respectively.     

关于低热值材料燃烧热值结果的影响因素探讨

对于一些低热值并意向达到A级燃烧性能的建筑材料,燃烧热值是评估的必检项。由于该类材料热值低,测试时不易点燃,无法获得准确测试结果,因此需通过人工干预手段使其完全燃烧。本文针对测试标准中的坩埚试验方法,探究测试过程中的影响因素,如样品形状、添加助燃剂苯甲酸的形状、上述两者在测试时相对摆放位置及其质量比例等对测试结果的影响,从而确定有助于样品完全燃烧的试验方式。     

纳米隔热材料在水泥厂中的设计应用

纳米隔热材料具有良好的隔热性能和热稳定性,在水泥厂高温部分使用可有效降低系统表面散热。本文通过建立设计模型量化散热量,对纳米隔热材料使用规格、部位作进一步优化。     

湖北省农网配网低压台区综合配电箱现状调研

统计分析了湖北省各地区农网配网低压台区综合配电箱的运行现状,提出了其中存在的主要问题,为正在进行的低压综合配电箱的典型设计工作提供了参考和建议。     

基于压电驱动的微振动主动减振控制系统研究

本文以压电陶瓷促动器构建并联六自由度减振平台,采用NI Compact-RIO实时控制系统和Fx-LMS自适应控制算法进行振动主动控制,对次级通道辨识方法和主动控制算法进行了模拟仿真,并搭建主动减振控制系统进行实验验证。仿真与实验结果表明,设计的主动减振控制系统对于7~50 Hz范围内的低频微振动有很好的控制效果。