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排序方式: 共有10000条查询结果,搜索用时 468 毫秒
41.
ABSTRACT: Physical aging of amorphous anhydrous fructose at temperature 5 °C and at 22 °C was studied using differential scanning calorimetry (DSC). The dynamic glass transition temperature, Tg0 for unaged samples was 16 °C and 13.3 °C for heating rate of 10 °C/min and 1 °C/min, respectively. The fictive temperature, Tf0 for unaged samples calculated by Richardson and Savill method was 12 °C, which is close to the dynamic value obtained from the lower DSC heating rate. The fictive temperature Tf of the aged fructose glasses at temperatures both below and above the transition region was fitted well by a non-exponential decay function (Williams-Watts form). Aging above the transition region (22 °C) for 18 d increased both the dynamic glass transition temperature Tg and the fictive temperature Tf . However, aging below the transition region (5 °C) for 1 d increased the dynamic glass transition temperature Tg but decreased the fictive temperature Tf . 相似文献
42.
The bonding of β'-Al2O3 and pyrex glass to Al matrix composites by anodic bonding process is achieved. The microstructure of the bonded interface and the joining mechanisms are analyzed with scanning electron microscope (SEM), energy dispersive X-ray fluorescence spectrometer (EDX). It is observed that the bonding region across the interface consists of the metal layer, oxide transitional layer and the ceramic layer, with the transitional layer composed of surface region and sub-surface region. The bonding process can mainly be categorized into anodic bonding process and solid state diffusing process. The pile-up of the ions and its drift in the interface area are the main reasons for anode oxidation and joining of the interface. The temperature, voltage and the drift ions in the ceramic or glass during the bonding process are the essential conditions to solid state diffusing and oxide bonding at the interface. The voltages, temperature, pressure as well as the surface state are the main factors that influence the anodic bonding. 相似文献
43.
Jonathan P. Belnoue Giang D. Nguyen Alexander M. Korsunsky 《International Journal of Fracture》2007,144(1):53-60
This paper presents a new 1-D non-local damage-plasticity deformation model for ductile materials. It uses the thermodynamic
framework described in Houlsby and Puzrin (2000) and holds, nevertheless, some similarities with Lemaitre’s (1971) approach.
A 1D finite element (FE) model of a bar fixed at one end and loaded in tension at the other end is introduced. This simple
model demonstrates how the approach can be implemented within the finite element framework, and that it is capable of capturing
both the pre-peak hardening and post-peak softening (generally responsible for models instability) due to damage-induced stiffness
and strength reduction characteristic of ductile materials. It is also shown that the approach has further advantages of achieving
some degree of mesh independence, and of being able to capture deformation size effects. Finally, it is illustrated how the
model permits the calculation of essential work of rupture (EWR), i.e. the specific energy per unit cross-sectional area that
is needed to cause tensile failure of a specimen. 相似文献
44.
45.
《稀有金属材料与工程》2006,23(4):12-16
透过性能对用于过滤分离、流体混合、布气分流等方面的多孔材料是一项十分关键的质量指标。主要介绍了多孔材料透过性能的表征方式,包括流体流动的基本概念、层流条件下流体的透过性能表征、多孔材料透过性能的综合表征、气体透过多孔材料时渗透系数的具体表征等方面。 相似文献
46.
防腐蚀施工工艺掌握的好坏,直接影响到工程投入生产后的使用寿命,为保证工程质量,以太钢不锈冷轧改造工程冷线防腐为例,对其常发生的质量通病进行认真分析,总结出一套行之有效的施工技术。 相似文献
47.
48.
P. WEBSTER 《Journal of microscopy》1993,169(1):85-88
A novel method of using the LKB 7800 series Knifemaker to produce glass knives using a balanced break is described. The method produces knives of sufficient quality to section aldehyde-fixed, sucrose-cryoprotected, frozen biological material in a cooled cryochamber of an ultramicrotome. The modifications to the Knifemaker are minimal and, if required, the machine can be returned easily to its normal state after use. 相似文献
49.
Shiro Matsuoka 《Journal of research of the National Institute of Standards and Technology》1997,102(2):213-228
The high frequency end of the relaxation spectrum for polymer molecules involves the rotation of the segmental bonds. This fast relaxation process, however, cannot take place easily in the condensed state crowded by the densely packed conformers, necessitating the slower cooperatively synchronous relaxation. As the temperature is lowered, the domain of cooperativity grows towards the infinite size at the Kauzmann zero entropy temperature, though actually the system deviates from the equilibrium as the glass transition intervenes typically at 50 K above that temperature. The excess enthalpy and entropy drop faster than predicted by the rotational isomeric states which would reach zero only at 0 K. The real ΔCP is greater than that of the RIS value. The actual volume in excess of the crystalline lattice volume, however, points towards zero at 0 K. Thus, a polymer with higher Tg typically exhibits a lower density and modulus in the glassy state. Since the configurational entropy associated with the free volume is proportional to the logarithm of the latter, the Kauzmann temperature can be scaled by ln M, where M is the algebraic average of the conformer molecular weight. The temperature dependence of the most dominant, i.e., the largest equilibrium domain size will result in the Adam-Gibbs and Vogel equations for the characteristic relaxation time. The cooperative domain distribution leads to the relaxation spectrum that follows a power law. The relationship between the characteristic relaxation time and the rate of physical aging is derived. 相似文献
50.
彩色PDP用玻璃基板 总被引:4,自引:0,他引:4
本文讨论了彩色PDP现用钠钙玻璃的热稳定性,指出由于这种玻璃在热处理过程中易变形和收缩,因而不适合作大面积彩色PDP基板材料,介绍了彩色PDP基板玻璃的制造方法和特点。最后介绍了日本旭硝子公司和美国康宁公司各自为彩色PDP新开发的玻璃基板材料PD200和CS25。 相似文献