Contact interaction of double titanium and chromium diboride with Fe-Cr alloys

The kinetics of wetting double titanium and chromium diboride by iron-based alloys with different chromium content is studied. It is shown that contact angles are formed in such systems over the range 0–10°. The energy parameters of wetting are calculated. It is established that chromium as a surface-active element promotes Fe-Cr alloy spreading on the diboride surface. The microstructure of the interaction area is studied. It is shown that terminal solid solutions and eutectics are formed in the TiCrB₂-(Fe-Cr) system. The optimum compositions of the metallic binder are determined for TiCrB₂-based composite materials. __________ Translated from Poroshkovaya Metallurgiya, Vol. 46, No. 1–2(453), pp. 109–115, 2007     

20CrMo棒材带状组织的控制研究

通过Gleeble-1500热模拟机对20CrMo轧材精轧阶段轧制过程及冷却过程的模拟,研究了终轧温度、冷却速度对室温组织的影响,分析了形成带状组织的条件,最终得出了理想室温组织的终轧温度和冷却速度。     

钻井工程固井胶结界面研究现状

固井质量问题在石油勘探开发中备受关注，对特殊工艺井钻井、油水井开采寿命和勘探开发效益有直接的影响。对固井胶结界面的研究是从根本上提高固井质量的一项基础性研究工作。为了推动固井胶结界面研究工作的开展，分析了国内外近年来有关固井界面研究的文献，阐述了开展固井胶结界面基础研究工作的意义，着重分析了这一研究领域目前所采用的研究方法，以及提高固井界面胶结强度的主要途径。在分析文献的基础上，提出今后深入开展固井界面研究工作的重点是：1）继续完善研究方法；2）重视动态研究；3）从胶结界面的微观结构和钻井工程整体系统的角度开展研究工作；4）注重改善胶结界面水化产物的微观结构和钻井工作液之间的协调增强作用。     

Effect of Y2O3 Content on Microstructure of Gradient Bioceramic Composite Coating Produced by Wide-Band Laser Cladding

Hydroxyapatite (HA) ,a kind of bioactive materi-al , has wide application prospect in hard tissue re-placemen and repairment due to its si milar chemicalcomposition and crystallographic structure to that ofbone mineral[1 ,2]. Since HA has lowstrength (50 …     

稀土和磷复合变质对过共晶铝——硅合金硅晶体形貌与力学性能的影响

采用扫描电镜、Ｘ射线衍射、材料性能检测等实验手段对复合变质处理后的过共晶铝硅合金显微组织、形貌和力学性能进行了分析。结果表明：磷和稀土复合变质后，使粗大块状、条状的初晶硅的尺寸明显缩小且棱角钝化；较大针状的共晶硅变为颗粒状，使显微组织明显细化，从而导致过共晶铝硅合金的力学性能显著提高。     

添加高速钢粉对烧结钢组织与性能的影响

研究了添加高速钢粉对烧结钢组织与性能的影响。实验结果表明，含２０％高速钢的烧结钢综合力学性能最好；添加高速钢粉能导致烧结钢密度减小的冲击韧性降低，当高速钢含量增中时，硬度随之增加，烧结钢中残余奥氏体和马氏体的含量与高速钢的含量呈线性关系。烧结钢中的马氏体显微硬度很高，它主要原高速钢粒子和原铁粒子的连接区域形成。     

Comparison of interfaces in Ti composites reinforced with uncoated and TiB2/C-coated SiC fibres

Interfaces play an important role in determining the mechanical properties of composite materials. The interfaces established between a titanium-alloy matrix (Ti-6Al-4V) and uncoated and TiB₂/C-coated SiC fibres are analysed by scanning electron microscopy, transmission electron microscopy and X-ray techniques. Emphasis is placed upon the interfacial morphology and microstructure, identification of reaction products, and the stability of the coating layer. Complex multi-reaction layers are observed frequently in the interfacial zones. Previous, often contradictory, reports about the interlayers are reviewed. Experimental observation demonstrates that the type and distribution of interlayers vary in a given system, due to prolonged treatment of the samples at temperature. The formation and distribution of the interlayers are discussed further, with respect to these and previous findings. Methods of reducing interfacial reactivity are discussed.     

硫酸盐含量对全固废材料固化盐渍土抗压强度的影响

为探讨硫酸盐含量对全固废材料固化盐渍土抗压强度及微观结构的影响,采用击实试验和无侧限抗压强度试验,并结合扫描电镜、EDS、X射线衍射和热重分析等微观测试结果,从固化盐渍土的火山灰反应产物及其数量等角度分析含盐量对固化盐渍土抗压强度变化的影响。结果表明:硫酸盐含量低于2.7%时,固化盐渍土抗压强度随含盐量的增加呈先增大后减小,抗压强度峰值对应的含盐量为1.8%;固化盐渍土的火山灰反应产物主要为C-S-H和AFt,硫酸盐含量从0.3%增至1.8%时,反应产物明显增多,致使固化土抗压强度增大;但当硫酸盐含量从1.8%增至2.7%时,膨胀性AFt将试件内部孔隙完全填充并产生胀裂破坏,造成抗压强度降低。研究成果为全固废材料固化硫酸盐渍土的工程应用奠定了基础,对环境保护也有积极贡献。     

结构性黄土压缩特性的微观非连续变形分析

黄土的结构性与其形成过程密切相关,并对其物理力学性质产生重要影响。针对结构性黄土的大孔隙和胶结特性,对DDA算法进行了扩展,将结构性黄土中起主要胶结作用的黏粒胶结嵌入已有的DDA算法中;使用Monte Carlo法和DDA模拟黄土的沉积过程,该方法能够模拟颗粒下落过程中的相互碰撞及摩擦,分析结构性黄土在压缩过程中颗粒的平动和转动规律,由此构建与原状黄土孔隙比接近的微观结构模型;进一步使用扩展DDA对所生成的黄土结构模型进行不同压力下的一维压缩试验模拟,并与室内压缩试验进行对比。发现胶结试样颗粒位移比不含胶结试样颗粒位移小,但整体规律相似;每个颗粒位移的大小和方向不尽相同,但主要以竖向位移为主;在压缩过程中,不同区域的颗粒位移存在较大差异,上部颗粒位移大,越往下部颗粒的位移越小。该研究成果可为从微观认识黄土力学行为提供一条途径。     

Material flow and microstructure in the friction stir butt welds of the same and dissimilar aluminum alloys

The material flow and microstructural evolution in the friction stir welds of a 6061-Al alloy to itself and of a 6061-Al alloy to 2024-Al alloy plates of 12.7 mm in thickness were studied under different welding conditions. The results showed that plastic deformation, flow, and mechanical mixing of the material exhibit distinct asymmetry characteristics at both sides of the same and dissimilar welds. The microstructure in dissimilar 6061-Al/2024-Al welds is significantly different from that in the welds of a 6061-Al alloy to itself. Vortex-like structures featured by the concentric flow lines for a weld of 6061-Al alloy to itself, and alternative lamellae with different alloy constituents for a weld of 6061-Al to 2024-Al alloy, are attributed to the stirring action of the threaded tool, in situ extrusion, and traverse motion along the welding direction. The mutual mixing in the dissimilar metal welds is intimate and far from complete. However, the bonding between the two Al-alloys is clearly complete. Three different regions in the nugget zone of dissimilar 6061-Al/2024-Al welds are classified by the mechanically mixed region (MMR) characterized by the relatively dispersed particles of different alloy constituents, the stirring-induced plastic flow region (SPFR) consisting of alternative vortex-like lamellae of the two Al-alloys, and the unmixed region (UMR) consisting of fine equiaxed grains of the 6061-Al alloy. Within all of these three regions, the material is able to withstand a very high degree of plastic deformation due to the presence of dynamic recovery or recrystallization of the microstructure. The degree of material mixing, the thickness of the deformed Al-alloy lamellae, and the material flow patterns depend on the related positions in the nugget zone and the processing parameters. Distinct fluctuations of hardness are found to correspond to the microstructural changes throughout the nugget zone of dissimilar welds.