Crack growth in aluminium alloy sheet material under flight-simulation loading

Crack propagation tests were carried out on 2024-T3 sheet specimens to study the effects of omitting low-amplitude cycles from the gust-dominated TWIST load sequence (MiniTWIST) and the removal of small load ranges from the manoeuvre-dominated FALSTAFF load sequence (short FALSTAFF). In other tests high-amplitude loads of TWIST and MiniTWIST were truncated at different levels. The results are compared with data from similar test programmes, including crack initiation. Attention is paid to unstationary crack growth retardation and a transient retardation during initial crack growth started by an artificial crack.     

静态水热脱铝处理对HZSM-5分子筛的结构、酸性和催化性能的影响

开发了一种静态水热脱铝的方法。HZSM-5经此法处理后,正戊烷的裂解活性增加,脱氢和芳构化性能加强。可用改变处理温度的方法来控制脱铝的程度。用XRD和吡啶吸附红外技术进行了研究。HZSM-5分子筛催化剂性能的变化用非骨架铝产生的强L酸中心来解释。     

换热器防腐蚀方法介绍

文章对换热器的不同保护方法进行了介绍 ,重点讨论了渗铝、渗锌两种方法。在室温～ 80℃自来水和 3.5 %NaCl水溶液中 ,与碳钢基体相比 ,渗铝层的电位发生了反转 ,因而在针孔部位会形成大阴极小阳极的局面 ,易发生点蚀 ;而在相同条件下渗锌层不出现上述点蚀现象 ,更适宜在换热器的应用     

Failure of Al-Mg-Si alloys in bending

The bendability of two Al-Mg-Si heat-treatable alloys was studied and compared with the performance of a non-heat-treatable Al-Mg alloy. A semi-guided wrap-bend tester consistent with ASTM E290 was used to obtain minimum bend radii and produce consistent bend radii for analysis of fracture mechanisms. Bending failure in these alloys was based on a surface roughening, or orange peel, process where the outer surface grains separated and produced depressions on the surface of the material. These depressions acted as notches that increased local stresses and eventually caused failure. The fracture was intergranular in nature, with a jagged crack progressing through the thickness of the material. Several factors that affect the bendability of AA6xxx alloys are quantified in this study. Critical elements regarding natural aging, artificial aging, deformation, and composition are discussed. A parameter of specific interest is the inclusion of copper in these alloys. Copper was added in an effort to increase the artificial aging response of selected alloys. This is of particular importance in the automotive industry because artificial aging occurs during the painting process, but adequate time and temperature is not provided to fully strengthen the alloys. It is believed by some automotive manufacturers that the inclusion of copper can have a negative effect on formability and bendability.     

铝活塞余热淬火和自然时效的应用研究

图 1所示的活塞试件 ,在开型时间为 5 0s～ 5 5s时 ,其表面温度为 (4 90± 5 )℃ ,可满足淬火要求。自然时效时间为 2 4天时 ,其机械性能可达到国标技术要求。这种新工艺有明显的经济效益。     

液态中锰渣摇包生产高硅锰硅合金的探讨

论述了利用液态中锰渣摇包生产高硅锰硅的原理、工艺过程热平衡,并介绍了其操作过程、主要影响因素及所取得的经济、社会效益.     

尿素对以硝酸铝和葡萄糖为原料合成氮化铝粉末反应过程中相变及反应速率的影响

以硝酸铝(Al(NO3)3·9H2O)和葡萄糖(C6H12O6·H2O)为原料,利用碳热还原法制备氮化铝粉末,研究了尿素对前驱物的制备及前驱物氮化反应的影响,研究发现添加尿素合成的前驱物和未添加尿素合成的前驱物在氮化反应过程中相变和反应速率存在较大差异。在没有添加尿素合成的前驱物的氮化反应过程中,出现了γ-Al2O3、α-Al2O3、AlON和AIN相,该前驱物的反应速率慢,完全氮化需要在1600℃下才能完成。对于添加尿素合成的前驱物而言,在其氮化反应过程中仅出现了γ-Al2O3和AIN相,没有α-Al2O3和AlON的生成,AIN直接由γ-Al2O3氮化生成,该前驱物的氮化反应速率快,氮化反应温度低,在1400℃下即可实现完全氮化。分析讨论了两种前驱物的氮化反应速率不同的主要原因,并利用XRD、SEM等分析方法对粉末进行了表征。     

MCM用氮化铝共烧多层陶瓷基板的研究

通过实验优化AlN(氮化铝)瓷料配方及排胶工艺,对共烧W(钨)导体浆料性能及AlN多层基板的高温共烧工艺进行了研究,并对AlN多层基板的界面进行了扫描电镜分析。采用AlN流延生瓷片与W高温共烧的方法,成功地制备出了高热导率的AlN多层陶瓷基板,其热导率为190 W/(m·K),线膨胀系数为4.6106℃1(RT~400℃),布线层数9层,W导体方阻为9.8 m,翘曲度为0.01 mm/50 mm,完全满足高功率MCM的使用要求。     

添加CaF2-YF3的AlN陶瓷的热导率

用CaF2和YF3做添加剂，在1750℃制备了热导率高于170W/m.K的的AlN陶瓷，并用XRD和SEM研究了AlN陶瓷在烧结过程中的相组成，微结构以及晶格参数的变化，并讨论了其对热导率的影响，研究发现，当使用CaF2-YF3做添加剂时，微结构差异对AlN陶瓷热导率的影响很小，AlN陶瓷的热导率主要由AlN晶格氧缺陷浓度决定，由于CaF2-YF3能有效降低AlN颗粒表面的氧含量，从而有利于获得高的热导率。