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941.
研究了自蔓延燃烧合成Si3N4粉的氧化处理(在空气气氛中分别于400、600、800℃保温3 h)以及添加的分散剂种类(分别为聚丙烯酸钠、六偏磷酸钠、三聚磷酸钠、木质素磺酸钙)对制备的Si3N4浆料的抗沉降性、ζ电位和黏度的影响。结果表明:1)在空气气氛中于800℃保温3 h氧化处理后,粉体中Si2N2O含量增多;用其制备的浆料的稳定性最好,ζ电位绝对值较大,黏度最小。2)以六偏磷酸钠作为分散剂制备的Si3N4浆料的稳定性较好,ζ电位绝对值最大,黏度最小。3)添加0.021%(w)六偏磷酸钠制备的Si3N4浆料的ζ电位绝对值最大,黏度较小。 相似文献
942.
Adam Bratten Ruoyu Chen Joshua Rittenhouse Ming Leu Haiming Wen 《International Journal of Applied Ceramic Technology》2022,19(5):2480-2488
High solids loading silicon carbide (SiC)-based aqueous slurries containing only .5 wt. % organic additives were utilized to create specimens of various geometries via an extrusion-based additive manufacturing (AM) technique. Pressureless electric field-assisted sintering was performed to densify each specimen without deformation. The combination of these techniques produced parts with >98% relative density despite containing only 5 wt.% oxide sintering additives. After sintering, specimens contained only the α-SiC and yttrium aluminum perovskite phases. This suggests the evolution of a nonequilibrium yttrium aluminate phase, as well as transformation from β-SiC to α-SiC. The fabrication method presented in this work has advantages over other AM techniques commonly used with SiC, because it does not require significant organic additives nor additional postprocessing steps such as chemical vapor infiltration or polymer impregnation and pyrolysis. 相似文献
943.
研究了高硅铝硅合金(45wt% Si)熔体电磁分离过程中,Sb添加量、下拉速率、温度等对分离效果的影响,对Sb在高硅铝硅合金电磁分离过程中的变质机理进行了分析。结果表明,在1500℃、下拉速率为10 μm/s时,过共晶铝硅合金熔体中加入Sb进行定向凝固后,合金部分硅铝比从11.53%降至11.21%,初晶硅富集区的硅含量从86wt%增至90wt%;当1500℃、下拉速率为40 μm/s时,合金部分硅铝比从12.56%降至12.13%,初晶硅富集区的硅含量从81wt%增至86.5wt%;加入变质剂后合金部分共晶硅相在α-Al基体中分布均匀且连续,形貌有所细化。 相似文献
944.
Shishuai Li Huanbei Chen Weide Wang Dongxu Yao Yongfeng Xia Yu-Ping Zeng 《International Journal of Applied Ceramic Technology》2022,19(5):2873-2882
In this work, the effects of Y2O3/MgO ratio on the densification behavior, phase transformation, microstructure evolution, mechanical properties, and thermal conductivity of Si3N4 ceramics were investigated. Densified samples with bimodal microstructure could be obtained by adjusting the ratio of Y2O3/MgO. It was found that a low Y2O3/MgO ratio facilitated the densification of Si3N4 ceramics while a high Y2O3/MgO ratio benefited the phase transformation of Si3N4 ceramics. Best mechanical properties (flexural strength of 875 MPa, and fracture toughness of 8.25 MPa·m1/2, respectively) and optimal thermal conductivity of 98.04W/(m·K) were achieved in the sample fabricated with Y2O3/MgO ratio of 3:4 by sintering at 1900°C for 4 h. 相似文献
945.
Surya Prakasarao Chodisetti V. K. Malik B. Venkata Manoj Kumar 《International Journal of Applied Ceramic Technology》2022,19(3):1367-1378
Highly dense electrically conductive silicon carbide (SiC)–(0, 10, 20, and 30 vol%) titanium boride (TiB2) composites with 10 vol% of Y2O3–AlN additives were fabricated at a relatively low temperature of 1800°C by spark plasma sintering in nitrogen atmosphere. Phase analysis of sintered composites reveals suppressed β→α phase transformation due to low sintering temperature, nitride additives, and nitrogen sintering atmosphere. With increase in TiB2 content, hardness increased from 20.6 to 23.7 GPa and fracture toughness increased from 3.6 to 5.5 MPa m1/2. The electrical conductivity increased to a remarkable 2.72 × 103 (Ω cm)–1 for SiC–30 vol% TiB2 composites due to large amount of conductive reinforcement, additive composition, and sintering in nitrogen atmosphere. The successful electrical discharge machining illustrates potential of the sintered SiC–TiB2 composites toward extending the application regime of conventional SiC-based ceramics. 相似文献
946.
Jian Zhao Linkun Shi Malin Liu Jiaxing Chang Youlin Shao Bing Liu Rongzheng Liu 《International Journal of Applied Ceramic Technology》2022,19(5):2514-2522
Dense sintering of SiC nanopowder under low temperature and pressure remains a big challenge, because of the great resistance caused by the severe agglomeration of nanopowder. A novel sintering strategy is proposed to prepare SiC composite ceramics by sintering the mixture of SiC nanopowder and SiC micron powder at low temperature and pressure. The SiC micron powder was in the size of 100 µm with little sintering activity, which was designed as a pressure conductor to promote the densification of SiC nanopowder. Experimental results showed that the SiC micron powder had a significant effect on increasing of the sintering density of nanopowder and improving the mechanical properties of SiC ceramics. An SiC composite ceramic with a relative density of 98%, a Vickers hardness of 22.6 GPa, and a fracture toughness of 5.43 MPa m1/2 could be sintered by spark plasma sintering under 1700°C and 30 MPa by adding 30 wt.% 100 µm SiC micron powder as reinforcements. 相似文献
947.
Ming Huang Zhihang Peng Wen Zhang Yang Xiang Feng Cao 《International Journal of Applied Ceramic Technology》2022,19(5):2916-2924
Fused silica ceramic has become one of the most widely used radome materials in the world since the 1970s. But its poor mechanical properties restricted its application to some extent. To improve the mechanical properties of the fused silica ceramic and keep its characteristic for radome materials, silicon nitride (Si3N4) whisker-reinforced fused silica ceramics were prepared by a slip-casting method in the work. The influence of Si3N4 whisker contents on the properties of the slurry was studied, indicating that the preferable pH values of the slurry were 4–6 and whisker contents were 10 wt.%. The flexural strength of as-prepared Si3N4w/SiO2 ceramic was about 74.35 MPa, exhibiting an increase of 7.75% over that of the pure silica sample. Its dielectric constant in the range from 8 to 12 GHz and tanδ under 10 GHz were, respectively, 3.37 and .0011. It is of great interest to find that Si3N4w/SiO2 has excellent oxidization resistance and its mass maintains even at 1270°C. 相似文献
948.
949.
采用OM、EBSD、XRD分析研究了含Cu低温加热取向硅钢组织、织构的演变特征,研究结果表明:热轧板中存在铁素体层和珠光体层彼此交替的带状组织,且显微组织在厚度方向上分布不均匀,热轧板中{001}〈110〉、{112}〈110〉织构以及{110}〈001〉织构在板厚方向上分布不均匀;经过冷轧后,铁素体晶粒被严重拉长,形成了沿轧向伸长的纤维状组织,冷轧板织构类型主要是α织构和γ织构;脱碳时基体发生回复再结晶,显微组织为单一的铁素体等轴晶粒,织构主要为γ织构;二次冷轧板经渗氮后织构仅从强度上有所降低,其织构类型变化不明显。成品二次再结晶组织发展比较完善,晶粒尺寸约为10~20 mm。织构类型为锋锐的Goss织构。成品磁感B800达到了1.926 T,铁损P1.7/50为1.047 W/kg。 相似文献
950.