泥浆制备中工艺改造的研究

根据室条件下粉磨试验结果，发现球磨过程中筛上料变化存在的突变范围，提出两次加料一次加水可改变泥浆颗粒分布，并找出适宜的加料种类与时间。另外给予测粒度分布提供了宝贵的试验基础数据。     

Direct preparation of particles from liquid suspension for ESEM or SEM analysis

A simplified method for the preparation of particles from liquid suspensions has been developed. Particles are deposited directly on carbon planchets for rapid analysis by environmental scanning electron microscopy or by conventional scanning electron microscopy after an additional drying step. This is accomplished by filtering the liquid through thin carbon planchets. Three different grades of graphite were investigated for their suitability as the source material for these planchets. The high quality isomolded graphite is recommended for the filtration and direct observation of particles by electron microscopy. This technique is demonstrated for particles in hydraulic fluid and aquatic suspended particulate material from a natural water source.     

稀疏气泡流动的粒子跟踪测速技术研究

采用动态阈值技术实现了对气泡图像的正确分割，利用灰度加权方法提高了气泡颗粒的定位精度。根据稀疏气泡流动图像的特点，提出了一种新的基于相关的粒子跟踪测速算法（2-HPTV）。通过进行两时刻中围绕待研究气泡所取的两个小的诊断窗口的相关运算，成功实现了气泡颗粒的轨迹追踪。实验表明本文算法较传统的PIV技术在测速精度上有很大程度的提高，与4帧粒子跟踪测速算法相比，降低了对摄像机帧频的要求，具有较强的实用性。     

A polydispersed particle system representation of the porosity for non-saturated cementitious materials

In this paper, the porosity of cementitious materials is described in terms of pore size distribution by means of a 3-dimensional overlapping sphere system with polydispersivity in size. On the basis of results established by Lu and Torquato [B. Lu, S. Torquato, Nearest-surface distribution functions for polydispersed particle systems, Phys. Rev. A 45(8) (1992) 5530-5544] and Torquato [S. Torquato, Random Heterogeneous Media: Microstructure and Macroscopic Properties. Springer-Verlag: New York, 2001] providing relations for nearest-neighbor distribution functions, the volume fraction of pores having a radius larger than a prescribed value is explicitly expressed. By adopting an appropriate size distribution function for the sphere system, it is shown that the pore size distribution of cementitious materials as detected for instance by mercury intrusion porosimetry (MIP), which generally points out several pore classes, can be well approached. On the basis of this porosity representation, the evaluation of the capillary pressure in function of the saturation degree is provided. The model is then applied to the simulation of the saturation degree versus relative humidity adsorption curves. The impact of the pore size distribution, the temperature and the thickness of the adsorbed water layer on these parameters are assessed and analyzed for three model materials having different pore characteristics.     

Feasibility study on the use of polyallyldiglycol-carbonate cell dishes in TUNEL assay for alpha particle radiobiological experiments

In the present work, we have studied the feasibility of a method based on polyallyldiglycol-carbonate (PADC) films to investigate the effects of alpha particles on HeLa cervix cancer cells. Thin PADC films with thickness of about 20 μm were prepared from commercially available CR-39 films by chemical etching to fabricate custom-made petri dishes for cell culture, which could accurately record alpha particle hit positions. A special method involving “base tracks” for aligning the images of cell nuclei and alpha particle hits has been proposed, so that alpha particle transversals of cell nuclei can be visually counted. Radiobiological experiments were carried out to induce DNA damages, with the TdT-mediated dUTP Nick-End Labeling (TUNEL) fluorescence method employed to detect DNA strand breaks. The staining results were investigated by flow cytometer. The preliminary results showed that more strand breaks occurred in cells hit by alpha particles with lower energies. Moreover, large TUNEL positive signals were obtained even with small percentages of cells irradiated and TUNEL signals were also obtained from non-targeted cells. These provided evidence for the bystander effect.     

Solid State Concepts to Understand Catalysis Using Nanoscale Metallic Particles

New advances in theoretical background and recent experimental results concerning nanometer scale metallic clusters are presented. We will begin by a presentation of the advantages and the limitations of synchrotron radiation techniques to characterise nanometer scale entities. Then, through a review of recent papers, we try to make a link between metallic surfaces and nanometer scale monometallic clusters in the case of the interaction with a small molecule, namely NO.     

热流量计的原理

根据工业及家庭供暖的要求，设计并研制成一种新型的热流量计，它采用方便而新颖的采集信息方式，并使用CPU精确实时的进行控制和运算，保证了热流量计的精确、实时和“分户计量”。     

高速钢高温形变诱发析出的研究

本文探讨了高速钢在高温形变过程中碳化物析出的行为及奥氏体组织状态对析出的影响。用透射电镜和扫描电镜分析了不同热处理状态奥氏体的组织结构,分析了高温形变过程中碳化物析出的部位,颗粒尺寸及形态。试验表明, 碳化物主要在奥氏体的缺陷处呈点状和点列状析出,大小为20mμ。处于回复状态的奥氏体缺陷诱发碳化物析出,析出碳化物钉札缺陷阻止再结晶进行。当再结晶驱动力较大时,由于动态再结晶充分发展,使缺陷大量消除,碳化物析出显著地减少。     

湖泊藻类叶绿素-α和悬浮物浓度的高光谱定量遥感模型研究

本文利用地物光谱仪对太湖水体进行了光谱测量和同步采样分析，对获得的数据尝试用光谱分离法进行分析，从中分离出蓝藻和悬浮物的特征波峰，建立波峰高度与同步水质采样得到的叶绿素-α浓度和悬浮物浓度的对应关系，得出其遥感定量反演算法，并实际应用在OMIS成像光谱仪图像上．     

用激光粒度分析仪测定二氧化锆粒度

介绍以六偏磷酸钠作为分散剂，采用激光粒度分析仪测量二氧化锆粒度的一种新方法。该方法的测量范围为0．05～300μm。