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排序方式: 共有10000条查询结果,搜索用时 687 毫秒
931.
论述了在程序设计过程中 ,使用树形控件、SQL 语句、临时表等多种手段 ,达到多个关联数据库的数据由一个可视化树形结构控件显示的方法和技巧 相似文献
932.
On the basis of new concept using a solid disperse phase we have developed an efficient catalytic solid-phase-system for epoxidations of alkenes using urea–hydrogen peroxide (urea–H2O2) complex and cetylpyridinium dodecatungstate ((CetylPy)10[H2W12O42]) catalyst on fluorapatite (FAp). The recovered solid catalyst phase was reused to keep the catalytic activity after several times. In the conceptual idea it is a key point that in situ solid-phase-activation of the catalyst with urea–H2O2 proceeds to form microcrystals of the active species dispersed on the solid phase. The dispersion of the catalyst on FAp in the case of tungstic acid (H2WO4) was suggested by EPMA analysis. We proposed the peroxo type of species keeping the parent polyoxometalate framework as novel active species from FT-IR spectroscopic studies. FAp phase plays important roles of dispersing the active species on its surface to have high catalytic activity and of stabilizing the active species to lead to high reusability. 相似文献
933.
Harish Chander V ShankerD Haranath Suman DudejaPooja Sharma 《Materials Research Bulletin》2003,38(2):279-288
Synthesis of electroluminescent ZnS:Cu, Br phosphor by a number of routes has been presented along with their brightness-voltage, brightness-frequency, brightness-waveform and spectral energy distribution studies. The sample fired in N2 atmosphere with aluminum and bromine shows predominantly green emission with a peak around 530 nm whereas the sample prepared under H2S and HBr shows the broadest emission spectrum with multiple peaks. These peaks may arise out of different possible bands of copper, self-activated luminescence of ZnS and association of copper with some of the donor levels formed because of the higher reactivity of HBr. All the samples have been found to obey the relation B=B0 exp.(−b/V0.5) which has been discussed using bipolar tunnel emission model. The frequency variation of brightness is linear. Samples containing bromine show multiple secondary peaks indicating that bromine helps in formation of multiple shallow traps. 相似文献
934.
In this paper, a new approach for powder cold compaction simulations is presented. A density-dependent plastic model within
the framework of finite strain multiplicative hyperelastoplasticity is used to describe the highly nonlinear material behaviour;
the Coulomb dry friction model is used to capture friction effects at die-powder contact; and an Arbitrary Lagrangian–Eulerian
(ALE) formulation is used to avoid the (usual) excessive distortion of Lagrangian meshes caused by large mass fluxes. Several
representative examples, involving structured and unstructured meshes are simulated. The results obtained agree with the experimental
data and other numerical results reported in the literature. It is shown that, contrary to other Lagrangian and adaptive h-remeshing approaches recently reported for this type of problems, the present approach verifies the mass conservation principle
with very low relative errors (less than 1% in all ALE examples and exactly in the pure Lagrangian examples). Moreover, thanks
to the use of an ALE formulation and in contrast with other simulations, the presented density distributions do not present
spurious oscillations.
Received: 20 March 2002 / Accepted: 15 October 2002
The partial financial support of the Ministerio de Ciencia y Tecnología (grant number DPI 2001-2204) is gratefully acknowledged. 相似文献
935.
This paper reports a method to produce networks of crystalline gallium oxide comprised of one‐dimensional (1D) nanostructures. Because of the unique arrangement of wires, these crystalline networks are termed as ‘nanowebs’. Nanowebs are of great technological interest since they contain wire densities of the order of 109 cm–2. A possible mechanism for the fast self‐assembly of crystalline metal oxide nanowires involves multiple nucleation and coalescence via oxidation–reduction reactions at the molecular level. The preferential growth of nanowires parallel to the substrate enabled them to coalesce into regular polygonal networks. The individual segments of the polygonal network consist of both nanowires and nanotubules of β‐gallium oxide. Individual wire properties contribute to a nanoweb’s overall capacity and the implications for devices based on nanowebs are expected to be enormous. 相似文献
936.
对甲基丙烯酸三氟乙酰氧乙酯(TFAOEMA)的阴离子聚合及原予转移自由基聚合进行了研究。常用的阴离于引发剂如丁基锂、1,1-二苯基已基锂等很难引发TFAOEMA的阴离子聚合,而碱性较弱的引发剂如三乙基铝却容易引发,且产率较高。以氯化亚铜、五甲基二乙基三胺、溴代丙酸乙酯为引发体系的TFAOEMA的本体原子转移自由基聚合符合活性聚合特征。但在四氢呋喃为溶剂的原子转移自由基聚合中却存在活性中心失活现象。以末端含卤素的聚甲基丙烯酸甲酯为大分子引发剂,引发TFAOEMA的原子转移自由基聚合,得到了含氟双嵌段聚合物。 相似文献
937.
STUDY ON PHASE PERCEPTION IN SPEECH 总被引:4,自引:0,他引:4
Tong Ming Bian Zhengzhong Li Xiaohui Dai Qijun Chen Yanpu 《电子科学学刊(英文版)》2003,20(5):387-392
The perceptual effect of the phase information in speech has been studied by auditory subjective tests. On the condition that the phase spectrum in speech is changed while amplitude spectrum is unchanged, the tests show that: (1) If the envelop of the reconstructed speech signal is unchanged, there is indistinctive auditory perception between the original speech and the reconstructed speech; (2) The auditory perception effect of the reconstructed speech mainly lies on the amplitude of the derivative of the additive phase; (3) td is the maximum relative time shift between different frequency components of the reconstructed speech signal. The speech quality is excellent while td <10ms; good while 10ms< td <20ms; common while 20ms< td <35ms, and poor while td >35ms. 相似文献
938.
939.
940.